227 research outputs found
Application of Slow-Scan Charge-Coupled Device (CCD) Cameras to On-Line Microscope Control
Autotuning methods for transmission electron microscopy are reviewed, and a distinction is drawn between predictive and non-predictive methods. The predictive methods make better use of the input data and therefore need fewer images to carry out complete autotuning. They typically require high quality of input data, which can be best provided by cooled slow-scan charge-coupled device (CCD) cameras. Two predictive methods are considered in more detail. These are the tilt-induced image shift (TIS) method of Koster, van der Mast and de Ruijter, and a new automated diffractogram analysis (ADA) method, which is introduced in this paper. The ADA method is shown to be capable of accurately aligning, stigmating and focussing a TEM in less than 30 seconds using just three high resolution images, and of automatically calibrating all the needed microscope parameters
Breeding Quality Protein Maize (QPM): Protocols for Developing QPM Cultivars
This manual is intended for maize breeders who would like to start developing quality protein maize (QPM) cultivars. It is a compilation and consolidation of several breeding protocols successfully used at CIMMYT over two decades of QPM development and breeding. A brief background and the basic theory of QPM genetics are explained, leading up to detailed methods and procedures of QPM development.Zea mays, Plant breeding, Breeding methods, Genetic resources, Protein quality, Protein content, Application methods, Lysine, Tryptophan, Food composition, Crop Production/Industries, F30, Q04,
Atomic Configuration of Nitrogen Doped Single-Walled Carbon Nanotubes
Having access to the chemical environment at the atomic level of a dopant in
a nanostructure is crucial for the understanding of its properties. We have
performed atomically-resolved electron energy-loss spectroscopy to detect
individual nitrogen dopants in single-walled carbon nanotubes and compared with
first principles calculations. We demonstrate that nitrogen doping occurs as
single atoms in different bonding configurations: graphitic-like and
pyrrolic-like substitutional nitrogen neighbouring local lattice distortion
such as Stone-Thrower-Wales defects. The stability under the electron beam of
these nanotubes has been studied in two extreme cases of nitrogen incorporation
content and configuration. These findings provide key information for the
applications of these nanostructures.Comment: 25 pages, 13 figure
Mejoramiento de ma�z con calidad de prote�na (QPM): Protocolos para generar variedades QPM
Zea mays, fitomejoramiento, m�todos fitot�cnicos, recursos gen�ticos, calidad de prote�na, contenido de prote�na, m�todos de aplicaci�n, lisina, tript�fano, componentes de los alimentos, Crop Production/Industries, F30, Q04,
Spectroscopic imaging of single atoms within a bulk solid
The ability to localize, identify and measure the electronic environment of
individual atoms will provide fundamental insights into many issues in
materials science, physics and nanotechnology. We demonstrate, using an
aberration-corrected scanning transmission microscope, the spectroscopic
imaging of single La atoms inside CaTiO3. Dynamical simulations confirm that
the spectroscopic information is spatially confined around the scattering atom.
Furthermore we show how the depth of the atom within the crystal may be
estimated.Comment: 4 pages and 3 figures. Accepted in Phys.Rev.Let
Effects of epitaxial strain on the growth mechanism of YBa2Cu3O7-x thin films in [YBa2Cu3O7-x / PrBa2Cu3O7-x] superlattices
We report on the growth mechanism of YBa2Cu3O7-x (YBCO). Our study is based
on the analysis of ultrathin, YBa2Cu3O7-x layers in c-axis oriented YBa2Cu3O7-x
/ PrBa2Cu3O7-x superlattices. We have found that the release of epitaxial
strain in very thin YBCO layers triggers a change in the dimensionality of the
growth mode. Ultrathin, epitaxially strained, YBCO layers with thickness below
3 unit cells grow in a block by block two dimensional mode coherent over large
lateral distances. Meanwhile, when thickness increases, and the strain relaxes,
layer growth turns into three dimensional, resulting in rougher layers and
interfaces.Comment: 10 pages + 9 figures, accepted in Phys. Rev.
Graphene re-knits its holes
Nano-holes, etched under an electron beam at room temperature in singlelayer
graphene sheets as a result of their interaction with metalimpurities, are
shown to heal spontaneously by filling up with either non-hexagon,
graphene-like, or perfect hexagon 2D structures. Scanning transmission electron
microscopy was employed to capture the healing process and study atom-by-atom
the re-grown structure. A combination of these nano-scale etching and
re-knitting processes could lead to new graphene tailoring approaches.Comment: 11 pages, 4 figure
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