19 research outputs found
1-(1-Benzofuran-2-yl)-3-(4-chlorophenyl)prop-2-en-1-one
In the title compound, C17H11ClO2, the benzofuran ring system is almost planar (r.m.s. deviation = 0.011 Å) and forms a dihedral angle of 10.53 (6)° with the chlorophenyl ring. No significant intermolecular interactions are observed
N-[3-(4-Fluorobenzyl)-2,4-dioxo-1,3-diazaspiro[4.5]dec-8-yl]-2-methylbenzenesulfonamide
In the title compound, C22H24FN3O4S, the cyclohexane ring adopts a chair conformation and the five-membered ring is essentially planar, with a maximum deviation of 0.040 (2) Å. The dihedral angles between the five-membered ring and the tolyl and fluorobenzene rings are 56.74 (12) and 89.88 (12)°, respectively. The two terminal benzene rings make a dihedral angle of 63.53 (12)°. The crystal structure displays intermolecular C—H⋯O and N—H⋯O hydrogen bonds. An intramolecular C—H⋯O hydrogen bond also occurs
N-{3-[2-(4-Fluorophenoxy)ethyl]-2,4-dioxo-1,3-diazaspiro[4.5]decan-7-yl}-4-methoxybenzenesulfonamide
In the title compound, C23H26FN3O6S, the two terminal aromatic rings form a dihedral angle of 49.26 (12)°. The cyclohexane ring adopts a chair conformation and the five-membered ring is essentially planar, with a maximum deviation from planarity of 0.0456 (19) Å. The dihedral angles between the five-membered ring and the methoxybenzene and fluorobenzene rings are 33.56 (11) and 81.94 (12)°, respectively. The crystal structure displays N—H⋯O hydrogen bonds as well as weak intermolecular C—H⋯O interactions
N-{3-[2-(4-Fluorophenoxy)ethyl]-2,4-dioxo-1,3-diazaspiro[4.5]decan-7-yl}-4-methylbenzamide
In the title compound, C24H26FN3O4, the two aromatic rings form a dihedral angle of 88.81 (15)°. The cyclohexane ring adopts a chair conformation and the five-membered ring is essentially planar, with a maximum deviation from planarity of 0.041 (2) Å. The crystal structure displays intermolecular C—H⋯O and N—H⋯O hydrogen bonds
3-[2-(2,6-Dichloroanilino)benzyl]-4-[(4-methoxybenzylidene)amino]-1H-1,2,4-triazole-5(4H)-thione
In the title compound, C23H19Cl2N5OS, the triazole ring makes dihedral angles of 24.81 (18), 69.94 (19) and 35.68 (18)° with the dichlorophenyl, benzene and methoxyphenyl rings, respectively. An intramolecular N—H⋯N hydrogen bond occurs. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur. In addition, there are weak C—H⋯π interactions involving the dichlorophenyl and triazole rings
4-Decylphenyl 4-benzyloxy-3-methylbenzoate
In the title compound, C31H38O3, the central benzene ring makes dihedral angles of 66.06 (9) and 65.21 (8)°, respectively, with the benzyl and 4-decylphenyl rings
Crystal structure of (7-fluoro-2-oxo-2H-chromen-4-yl)methyl morpholine-4-carbodithioate
In the title compound, C15H14FNO3S2, the 2H-chromene ring system is close to being planar (r.m.s. deviation = 0.024 angstrom) and the morpholine ring adopts a chair conformation. The dihedral angle between the 2H-chromene ring system and the morpholine ring (all atoms) is 88.21 (11)degrees. In the crystal, inversion dimers linked by pairs of very weak C-H center dot center dot center dot F hydrogen bonds generate R-2(2)(8) loops; C-H center dot center dot center dot O hydrogen bonds connect the dimers into 010] chains. Weak aromatic pi-pi stacking interactions between the pyran rings of the chromene systems centroid-centroid distance = 3.6940 (16) angstrom] are also observed
Crystal structure of (2E)-1-(5-bromothiophen-2-yl)-3-(2-chlorophenyl)prop-2-en-1-one
In the title compound, C13H8BrClOS, the thienyl ring is not coplanar with the benzene ring, their planes forming a dihedral angle of 13.2 (4)degrees. In the crystal, molecules stack along the a axis, with the interplanar separation between thienyl rings and between benzene rings being 3.925 (6) angstrom. The sample is an inversion twin
(Z)-2-(4-Methoxyanilino)-1,4-Diphenylbut-2-Ene-1,4-Dione
In the mol\-ecule of the title compound, C\sb 23H\sb 19NO\sb 3, the mean plane of the meth\-oxy\-phenyl ring makes dihedral angles of 51.63(8) and 50.86(8)\circ with the terminal phenyl rings. An intra\-molecular N—-H⋅sO hydrogen bond occurs. The crystal structure features C—-H⋅sO hydrogen bonds
1-(6-Chloro-1-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-3-(2-chlorophenyl)urea
In the title compound, C14H11Cl2N5O, the plane of the 1H-imidazo[4,5-c]pyridine ring system [r.m.s. deviation = 0.087 (19) Å] makes a dihedral angle of 4.87 (10)° with the terminal phenyl ring. An intramolecular N—H...N hydrogen bond stabilizes the molecular conformation. In the crystal, N—H...O hydrogen bonds link the molecules into inversion dimers. These dimers are connected by π–π interactions between imidazole rings [shortest centroid–centroid distance = 3.4443 (14) Å]