122 research outputs found

    The dependence of cylindrical resonator natural frequencies on the fluid density

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    The article examines the dependence of cylindrical resonator natural frequencies (sensitive element) on the density (mass) of different fluids flowing through it. The cylindrical resonators are being widely applied in automatic control systems of technological processes as oscillating transducer density meter. The article presents the experimental results that prove the dependence of natural frequencies and vibration amplitude on the fluid density

    Effect of silver additive on physicochemical properties of hydroxyapatite applied to reconstructive surgery

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    The effect of silver adding to hydroxyapatite (HA) in its solubility in physiological solution and biological activity was investigated. Samples of HA containing silver (AgHA) obtained by liquid-phase method in the conditions of microwave exposure. Solubility (CCa2+·103, mol/l) of the powders AgHA was determined by chemical methods according trilonometric titration of the calcium ions in physiological solution at 25 and 37 °C. To investigate the biological activity of the samples, a series of experiments on the formation of the calcium-phosphate layer on the surface of the SBF-solution at 37 °C for 28 days. Electronic micrographs of samples taken at the end of each 7 days of the experiment, indicate the formation of calcium-phosphate layer (CPL) in the samples, the kinetics of which is shown as a function of cumulative concentrations of calcium and magnesium ions from time

    Resource conservation program in terms of Vostokgazprom environmental policy

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    The article examines a number of key areas of environmental policy of Vostokgazprom. The Associated Petroleum Gas program is an important step within the resource conservation and environmental protection framework. In addition, the company undertakes the extensive work on emergency response programs, and carries out continuous protection of the subsurface and control over environmental safety in all production sites. Vostokgazprom continuously modernizes the basic industrial facilities and invests money in new projects. The study analyzes the steps being taken by the company within the energy saving policy that leads to significant costs cut

    Estimating gold-ore mineralization potential within Topolninsk ore field (Gorny Altai)

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    Based on the results of ore and near-ore metasomatite composition analysis, the factors and indicators of gold-ore mineralization potential were proposed. Integration of the obtained data made it possible to outline magmatic, structural, and lithological factors, as well as direct and indirect indicators of gold-ore mineralization. Applying multidimensional analysis inherent to geochemical data, the spatial structure was investigated, as well as the potential mineralization was identified. Based on the developed and newly-identified mineralization, small (up to medium-sized) mineable gold-ore deposits in skarns characterized by complex geological setting was identified

    Synthesis and investigation of physico-chemical, antibacterial, biomymetic properties of silver and zinc containing hydroxyapatite

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    In the work we carried out microwave synthesis of modified hydroxyapatites (HA) with different content of ions. A solid solution based on HA remains a single-phase sample when the calcium ions are substituted by silver and zinc ions up to 5 % by weight (0.5 mole fraction). The microstructure parameters, morphology and the particle powders size were studied by X-ray diffraction analysis, IR spectroscopy, and scanning electron microscopy (SEM). It is shown that the modification of НA by silver (AgHA) and zinc (ZnHA) ions increases the size of its particles, the degree of crystallinity, and the pore sizes of the samples while reducing their specific surface and uniformity of their forms. Elemental analysis and distribution of elements over the surface of HA, AgHA, and ZnHA powders were performed by X-ray spectral microanalysis (RSMA). The ratio of Ca/P is within the range of 1.66-1.77 and corresponds to the ratio of Ca/P in stoichiometric HA and the HA entering bone tissue. The ability of AgHA- and ZnHA-substrates to form on their surface a calcium-phosphate layer from the simulated body fluid (SBF) at 37 °C is determined. This ability decreases in the order: in ZnHА it is less than in AgHА, but greater than in HА. The antibacterial activity of the samples was analyzed. The AgHA sample has both bactericidal and persistent bacteriostatic properties in the case of direct contact with Escherichia coli cells

    Structural-phase state and surface properties of composite materials based on polylactide and hydroxyapatite

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    The phase composition and unit cell parameters were determined for composites based on polylactide and hydroxyapatite with the polylactide/hydroxyapatite weight ratios of 90/10, 80/20, 70/30, and 60/40. As the polylactide content of the composites is increased, they become less hydrophilic, and the surface energy σS-G increases from 29.13 to 74.35 mJ m–2. The sample with the component weight ratio of 70/30 is characterized by the maximal roughness, and the Ca2+ and Mg2+ ions from simulated body fluid are actively adsorbed onto its surface, as proved by SEM examination of the composites

    Preparation of composite materials based on hydroxyapatite and lactide and glycolide copolymer

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    Composite materials for the restoration of bone tissues based on hydroxyapatite and a copolymer of lactide and glycolide were obtained. The composition of materials at different stages of production is estimated by X-Ray diffraction method. It has been established that during the production of materials a new phase of chlorine-substituted hydroxyapatite (Ca9.7(P6O23.81)Cl2.35(OH)2.01) was formed, which promoted an increase of hydroxyapatite solubility in the composition of materials. The quantitative estimation of micro- and macroporosity of materials is given. It was found that the use of sodium chloride as the pore-forming agent delivers porosity of the composites required for use as bone substitutes
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