3,925 research outputs found
Calibration approach to electron probe microanalysis: A study with PWA-1480, a nickel base superalloy
The utility of an indirect calibration approach in electron probe microanalysis is explored. The methodology developed is based on establishing a functional relationship between the uncorrected k-ratios and the corresponding concentrations obtained using one of the ZAF correction schemes, for all the desired elements in the concentration range of interest. In cases where a very large number of analyses are desired, such a technique significantly reduces the total time required for the microprobe analysis without any significant loss of precision in the data. A typical application of the method in the concentration mapping of the transverse cross-section of a dendrite in directionally solidified PWA-1480, a nickel-based superalloy, is described
Macrosegregation during plane front directional solidification of Csl-1 wt. percent Tll alloy
Macrosegregation produced during vertical Bridgeman directional solidification of Csl-1 wt. pct. Tll in crucibles of varying diameter, from 0.5 to 2.0 cm, was examined. Gravity driven convection is present in the melt even in the smallest crucible diameter of 0.5 cm. Observed solutal profiles are in agreement with the analytical boundary layer model of Favier which describes macrosegregation in the presence of convection. The scintillation efficiency of Csl decreases along the specimen length as the thallium iodide content of the alloy increases
Robust procedure for creating and characterizing the atomic structure of scanning tunneling microscope tips
Scanning tunneling microscopes (STM) are used extensively for studying and
manipulating matter at the atomic scale. In spite of the critical role of the
STM tip, the control of the atomic-scale shape of STM tips remains a poorly
solved problem. Here, we present a method for preparing tips {\it in-situ} and
for ensuring the crystalline structure and reproducibly preparing tip structure
up to the second atomic layer. We demonstrate a controlled evolution of such
tips starting from undefined tip shapes.Comment: 12 pages preprint-style; 5 figure
Floating phase in a dissipative Josephson junction array
We consider dissipative quantum phase transitions in Josephson junction
arrays and show that the disordered phase in this extended system can be viewed
as an unusual floating phase in which the states of local -dimensional
elements (single Josephson junctions) can slide past each other despite
arbitrary range spatial couplings among them. The unusual character of the
metal-superconductor quantum critical point can be tested by measurements of
the current voltage characteristic. This may be the simplest and most natural
example of a floating phase.Comment: 4 pages, RevTex4. The revised version contains higher order
renormalization group equations and the corresponding phase diagra
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