Effect of light curing tip distance and resin shade on microhardness of a hybrid resin composite Efeito da distância da ponta do aparelho de fotoativação e da cor na microdureza superficial de um compósito híbrido

Resin composite shades and resin composite polymerization performed with a distanced light tip are factors that can affect polymerization effectiveness. Thisin vitro study aimed to evaluate the influence of curing tip distance and resin shade on the microhardness of a hybrid resin composite (Z250 - 3M ESPE). Forty-five resin composite specimens were randomly prepared and divided into nine experimental groups (n = 5): three curing tip distances (2 mm, 4 mm, and 8 mm) and three resin shades (A1, A3.5, and C2). All samples were polymerized with a continuous output at 550 mW/cm². After 24 hours, Knoop microhardness measurements were obtained on the top and bottom surfaces of the sample, with a load of 25 grams for 10 seconds. Five indentations were performed on each surface of each sample. Results showed that bottom surface samples light-cured at 2 mm and 4 mm presented significantly higher hardness values than samples light-cured at 8 mm. The resin shade A1 presented higher hardness values and was statistically different from C2. The resin shade A3.5 did not present statistical differences from A1 and C2. For the top surface, there were no statistical differences among the curing tip distances. For all experimental conditions, the top surface showed higher hardness values than the bottom surface. It was concluded that light curing tip distance and resin shade are important factors to be considered for obtaining adequate polymerization.<br>A cor do compósito e a polimerização realizada com a ponta do aparelho de fotoativação distante da superfície do compósito são fatores que podem afetar a efetividade de polimerização. Assim, o objetivo deste estudo in vitro foi avaliar a influência desses fatores na microdureza superficial de um compósito híbrido (Z250 - 3M ESPE). Quarenta e cinco espécimes de compósito foram aleatoriamente preparados de acordo com os nove grupos experimentais (n = 5): três distâncias de fotoativação (2 mm, 4 mm e 8 mm) e três cores de compósito (A1, A3,5 e C2). Todas as amostras foram fotoativadas com aparelho de fotoativação ajustado com intensidade contínua de 550 mW/cm². Após 24 horas, dez medidas de dureza Knoop foram obtidas nas superfícies de topo e fundo de cada amostra, com carga de 25 gramas por um tempo de 10 segundos. Resultados mostraram que, para a superfície de fundo, os grupos com a fotoativação realizada com distância de 2 e 4 mm apresentaram maiores médias do que os grupos com distância de 8 mm, e os grupos de cor A1 apresentaram maiores médias e com diferenças estatísticas que os grupos de cor C2, e o grupo A3,5 não apresentou diferenças estatísticas quando comparado aos outros grupos. Para a superfície de topo, não houve diferenças estatísticas significantes para os fatores estudados. Para todas as condições experimentais, a superfície de fundo apresentou médias de durezas estatisticamente menores do que as da superfície de topo. Pode-se concluir que os fatores cor do compósito e distância de polimerização são importantes fatores a serem considerados para a obtenção de adequada polimerização

Effects of food-simulating liquids on surface properties of giomer restoratives

10.2341/11-419-LOperative Dentistry376665-67

Influence of different light-curing units on the surface roughness of restorative materials: in situ study

The aim of this study was to evaluate the influence of different light sources (LED and Halogen lamp) on the roughness (superficial) of composite resin (Filtek Z250, Filtek P60, Charisma and Durafill) varying post-irradiation times, in an in situ experiment. For this purpose, 80 specimens were made in polyurethane moulds. Ten volunteers without medicament use and good oral condition were selected and from them study moulds were obtained. A palatal intra-oral acrylic resin appliance was made for each of the subjects of the experiment. In each appliance, two specimens of each material were fixed (LED/Halogen lamp - control group). Roughness tests were performed immediately and 30 days after initial light-curing. Statistical analysis was performed using ANOVA. Statistically significant difference was observed only between post-irradiation times, where the 30th day showed the highest roughness values. It be concluded that roughness was influenced only by post-irradiation times, presenting the 30- days period inferior behavior

Composite depth of cure using four polymerization techniques

The light-curing technique is relevant to reduce the degree of polymerization shrinkage, improving clinical and esthetic success of composite resin restorations. OBJECTIVE: To evaluate in vitro the effect of four light-curing techniques on depth of cure of a composite resin. MATERIAL AND METHODS: Ten specimens of a composite resin were made in cylindrical cavities prepared in PVC plates (3.0 X 7.0 mm) for each light-curing technique. Four photoactivation methods were investigated: stepped, ramped, pulse-delay and traditional. Specimens were longitudinally sectioned and polished for microhardness measurements (kg/mm²), which were made at 0.1, 1.0, 2.0 and 4.0 mm from the irradiated surface. Data were subjected to ANOVA and Tukey's test. RESULTS: The effect of factors studied (curing method and distance from the surface) and the interaction of these factors was statistically significant (p<0.05). The traditional method of cure provided higher microhardness values (69.6 ± 2.5) than the stepped (63.5 ± 3.1) and pulsed (63.9 ± 3.2) methods at all depths evaluated, but it did not differ from the ramped method (66.7± 4.4) at 0.1 and 1.0 mm of depth. CONCLUSION: All techniques employed provided satisfactory cure of the composite resin up to the depth of 2.0 mm from the irradiated surface