793 research outputs found
A New Phenomenon: Sub-Tg, Solid-State, Plasticity-Induced Bonding in Polymers
Polymer self-adhesion due to the interdiffusion of macromolecules has been an
active area of research for several decades [70, 43, 62, 42, 72, 73, 41]. Here,
we report a new phenomenon of sub-Tg, solid-state, plasticity-induced bonding;
where amorphous polymeric films were bonded together in a period of time on the
order of a second in the solid-state at ambient temperatures nearly 60 K below
their glass transition temperature (Tg) by subjecting them to active plastic
deformation. Despite the glassy regime, the bulk plastic deformation triggered
the requisite molecular mobility of the polymer chains, causing
interpenetration across the interfaces held in contact. Quantitative levels of
adhesion and the morphologies of the fractured interfaces validated the sub-Tg,
plasticity-induced, molecular mobilization causing bonding. No-bonding outcomes
(i) during the compression of films in a near hydrostatic setting (which
inhibited plastic flow) and (ii) between an 'elastic' and a 'plastic' film
further established the explicit role of plastic deformation in this newly
reported sub-Tg solid-state bonding
Enhancing the Performance of the T-Peel Test for Thin and Flexible Adhered Laminates
Symmetrically bonded thin and flexible T-peel specimens, when tested on
vertical travel machines, can be subject to significant gravitational loading;
with the associated asymmetry and mixed-mode failure during peeling. This can
cause erroneously high experimental peel forces to be recorded which leads to
uncertainty in estimating interfacial fracture toughness and failure mode. To
overcome these issues, a mechanical test fixture has been designed for use with
vertical test machines, that supports the unpeeled portion of the test specimen
and suppresses parasitic loads due to gravity from affecting the peel test. The
mechanism, driven by the test machine cross-head, moves at one-half of the
velocity of the cross-head such that the unpeeled portion always lies in the
plane of the instantaneous center of motion. Several specimens such as bonded
polymeric films, laminates, and commercial tapes were tested with and without
the fixture, and the importance of the proposed T-peel procedure has been
demonstrated
A dynamics-driven approach to precision machines design for micro-manufacturing and its implementation perspectives
Precision machines are essential elements in fabricating high quality micro products or micro features and directly affect the machining accuracy, repeatability and efficiency. There are a number of literatures on the design of industrial machine elements and a couple of precision machines commercially available. However, few researchers have systematically addressed the design of precision machines from the dynamics point of view. In this paper, the design issues of precision machines are presented with particular emphasis on the dynamics aspects as the major factors affecting the performance of the precision machines and machining processes. This paper begins with a brief review of the design principles of precision machines with emphasis on machining dynamics. Then design processes of precision machines are discussed, and followed by a practical modelling and simulation approaches. Two case studies are provided including the design and analysis of a fast tool servo system and a 5-axis bench-top micro-milling machine respectively. The design and analysis used in the two case studies are formulated based on the design methodology and guidelines
Elemental Analysis of OAK and Hickory Charcoal Using Neutron Activation Analysis
One-cm cubes of heartwood of white oak and shagbark hickory wood and charcoat were analyzed for selected inorganic elements using neutron activation analysis. A multi-element survey procedure with short (30-sec) and long (24-h) irradiation exposures was developed for use with the University of Missouri Research Reactor Facility. Output of this facility is 10 Megawatts, generating a flux of 1 x 1014 neutrons/cm2/sec. Matched wood samples were converted into charcoat utilizing (1) commercial process in a Missouri-type kiln, and (2) laboratory charring using specified time/temperature schedules.Inorganic concentrations of Al, Ba, Br, Ca, Ce, Co, Cr, Eu, Fe, K, Mg, Mn, Na, Rb, and Zn were found to increase with charring temperature as a result of the reduced charcoal yield. The elements measured accounted for some 60% of the ash content, which was also shown to increase in inverse proportion to the charcoal yield
Centrifugal LabTube platform for fully automated DNA purification and LAMP amplification based on an integrated, low-cost heating system
This paper introduces a disposable battery-driven heating system for loop-mediated isothermal DNA amplification (LAMP) inside a centrifugally-driven DNA purification platform (LabTube). We demonstrate LabTube-based fully automated DNA purification of as low as 100 cell-equivalents of verotoxin-producing Escherichia coli (VTEC) in water, milk and apple juice in a laboratory centrifuge, followed by integrated and automated LAMP amplification with a reduction of hands-on time from 45 to 1 min. The heating system consists of two parallel SMD thick film resistors and a NTC as heating and temperature sensing elements. They are driven by a 3 V battery and controlled by a microcontroller. The LAMP reagents are stored in the elution chamber and the amplification starts immediately after the eluate is purged into the chamber. The LabTube, including a microcontroller-based heating system, demonstrates contamination-free and automated sample-to-answer nucleic acid testing within a laboratory centrifuge. The heating system can be easily parallelized within one LabTube and it is deployable for a variety of heating and electrical applications
Results from the Project 8 phase-1 cyclotron radiation emission spectroscopy detector
The Project 8 collaboration seeks to measure the absolute neutrino mass scale
by means of precision spectroscopy of the beta decay of tritium. Our technique,
cyclotron radiation emission spectroscopy, measures the frequency of the
radiation emitted by electrons produced by decays in an ambient magnetic field.
Because the cyclotron frequency is inversely proportional to the electron's
Lorentz factor, this is also a measurement of the electron's energy. In order
to demonstrate the viability of this technique, we have assembled and
successfully operated a prototype system, which uses a rectangular waveguide to
collect the cyclotron radiation from internal conversion electrons emitted from
a gaseous Kr source. Here we present the main design aspects of the
first phase prototype, which was operated during parts of 2014 and 2015. We
will also discuss the procedures used to analyze these data, along with the
features which have been observed and the performance achieved to date.Comment: 3 pages; 2 figures; Proceedings of Neutrino 2016, XXVII International
Conference on Neutrino Physics and Astrophysics, 4-9 July 2016, London, U
Project 8 Phase III Design Concept
We present a working concept for Phase III of the Project 8 experiment,
aiming to achieve a neutrino mass sensitivity of ( C.L.)
using a large volume of molecular tritium and a phased antenna array. The
detection system is discussed in detail.Comment: 3 pages, 3 figures, Proceedings of Neutrino 2016, XXVII International
Conference on Neutrino Physics and Astrophysics, 4-9 July 2016, London, U
A novel cardioport for beating-heart, image-guided intracardiac surgery
Objective
Intracardiac beating-heart procedures require the introduction and exchange of complex instruments and devices. To prevent potential complications such as air embolism and bleeding, a universal cardioport was designed and tested.
Methods
The design consists of a port body and a series of interchangeable sleeves. The port uses a fluid purging system to remove air from the instrument before insertion into the heart, and a valve system minimizes blood loss during instrument changes.
Results
The cardioport was tested ex vivo and in vivo in pigs (n = 5). Beating-heart procedures, such as septal defect closure and mitral valve repair, were modeled. Ex vivo trials (n = 150) were performed, and no air emboli were introduced using the port. In comparison, air emboli were detected in 40% to 85% of the cases without the use of the port-based purging system. Port operation revealed excellent ergonomics and minimal blood loss.
Conclusions
A novel cardioport system designed to prevent air entry and blood loss from transcardiac instrument introduction was shown to be an enabling platform for intracardiac beating-heart surgery. The port system improves safety and facilitates further development of complex instruments and devices for transcardiac beating-heart surgery.Center for Integration of Medicine and Innovative Technology (Award 07-026)National Institutes of Health (U.S.) (National Heart, Lung, and Blood Institute Award 5R01HL073647)Massachusetts Technology Transfer Cente
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