887 research outputs found

    Residual stresses of AlSi10Mg fabricated by selective laser melting (SLM)

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    The aim of the paper is the residual stress analysis of AlSi10Mg material fabricated by selective laser melting (SLM). The SLM technique allows to product of complex geometries based on three-dimensional model, in which stiffness and porosity can be precisely designed for specific uses. As the studied material, there were chosen solid samples built in two different directions: parallel (P-L) and perpendicular (P-R) to the tested surface and cellular lattice built in perpendicular direction, as well. In the paper, for the complex characterization of obtained materials, the phase analysis, residual stress and texture studies were performed. The classical non-destructive sin2ψ method was used to measure the residual stress measurements. The final products, both solid sample and cellular lattice, have a homogeneous phase composition and consist of solid solution Al(Si) (Fm-3m) type, Si (Fd-3m) and Mg2Si (Pnma). The obtained values of the crystallite size are in a range of 1000 Å for Al(Si), 130-180 Å for Si phase. For Mg2Si phase, the crystallite sizes depend on sintering process, they are 800 Å for solid samples and 107 Å for cellular lattice. The residual stress results have the compressive character and they are in a range from –5 to –15 MPa

    Modelling, manufacturability and compression properties of the CpTi grade 2 cellular lattice with radial gradient TPMS architecture

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    In the present study, a titanium cellular lattice structure with a mathematical designed porosity gradient was successfully fabricated using the selective laser melting method. The samples with smooth gradient transition of porosity of between 60% and 80% were received for different elementary cell geometries. Elementary cells belong to the triply periodic minimal surfaces family (G, D, I2Y, IWP). Each sample was subjected to a comprehensive analysis including: dimensional metrology and assessment of material defects (X-ray micro-tomography), surface morphology tests (scanning electron microscopy) and mechanical properties (universal testing machine). It has been shown that a cellular lattice with high dimensional accuracy (+0.16/–0.08 mm) and full dense struts can be obtained. According to the assumption, the gradient increases the strength of the cellular lattice samples. The highest increase in plateau stress between the samples with and without gradient was found for the I2Y series (about 185%). Furthermore, it was found that the stress-strain response of the samples depends not only on total porosity, but also on the 3D geometry of the cellular lattice. The stress-strain curves for G, IWP and I2Y samples are smooth and exhibit three characteristic regions: linear elasticity, plateau region and densification region. The size of regions depends on the geometric features of the cellular lattice. For series D, in the plateau region, the fluctuations in stress value are clearly visible. The smoothest stress-strain curve can be noted for the G series, which combined with good mechanical properties (the plateau stress and energy absorbed, at respectively 25.5 and 43.2 MPa, and 46.3J and 59.5J for Gyr_80 and Gyr_6080, which corresponds to a strain of almost 65% and 50%) positively affects the applicability of cellular structures with such geometry

    The manufacturability and compression properties of the Schwarz Diamond type Ti6Al4V cellular lattice fabricated by selective laser melting

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    Selective laser melting technology makes it possible to produce 3D cellular lattice structures with controlled porosity. The paper reflects to machining and examination of structures with predefined distribution, shape and size of the pores. In the study, the porous structures of Ti6Al4V were investigated. The tests were carried out using structures of spatial architecture of Schwarz D TPMS geometry with a total porosity of 60% and 80% and various pore sizes. Dimensional accuracy of additively manufactured structures was measured in relation to the 3D model. Geometry of the final structure differed from the CAD model in the range ± 0.3 mm. The surfacemorphology and porosity of the solid struts were also checked. Themechanical properties of the structures were determined in a static compression test

    Morphology and surface topography of Ti6Al4V lattice structure fabricated by selective laser sintering

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    Construction of metallic implants with a porous structure that mimics the biomechanical properties of bone is one of the challenges of orthopedic regenerative medicine. The selective laser sintering technique (SLS) allows the production of complex geometries based on three-dimensional model, which offers the prospect of preparing porous metal implants, in which stiffness and porosity can be precisely adjusted to the individual needs of the patient. This requires an interdisciplinary approach to design, manufacturing and testing of porous structures manufactured by selective sintering. An important link in this process is the ability to assess the surface topography of the struts of porous structure. The paper presents a qualitative assessment of the surface morphology based on SEM studies and methodology that allows for quantitative assessment of stereometric structure based on micro-tomographic measurements

    Photoacoustic Tomography of a Rat Cerebral Cortex in vivo with Au Nanocages as an Optical Contrast Agent

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    Poly(ethylene glycol)-coated Au nanocages have been evaluated as a potential near-infrared (NIR) contrast agent for photoacoustic tomography (PAT). Previously, Au nanoshells were found to be an effective NIR contrast agent for PAT; however, Au nanocages with their more compact sizes (100 nm for Au nanoshells) and larger optical absorption cross sections should be better suited for in vivo applications. We sequentially injected Au nanocages into the circulatory system of a rat in three administrations and in vivo PAT was conducted immediately prior to the first injection and continued until 5 h after the final injection. A gradual enhancement of the optical absorption in the cerebral cortex, by up to 81%, was observed over the course of the experiment

    Photoacoustic tomography with novel optical contrast agents based on gold nanocages or nanoparticles containing near-infrared dyes

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    Poly(ethylene glycol)-coated Au nanocages have been evaluated as a potential near-infrared (NIR) contrast agent for photoacoustic tomography (PAT). Previously, Au nanoshells were found to be an effective NIR contrast agent for PAT; however, Au nanocages, with their more compact sizes (100 nm for Au nanoshells) and larger optical absorption cross-sections, should be better suited for in vivo applications. In this study, we tested Au nanocages as a contrast agent for PAT. The result suggests that Au nanocages are promising contrast agents for our applications. We also present PAT results when novel, dye-containing nanoparticles are used as contrast agents

    Synthesis and Application of Carbon–Iron Oxide Microspheres’ Black Pigments in Electrophoretic Displays

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    Carbon–iron oxide microspheres’ black pigments (CIOMBs) had been prepared via ultrasonic spray pyrolysis of aqueous solutions containing ferrous chloride and glucose. Due to the presence of carbon, CIOMBs not only exhibited remarkably acid resistance, but also could be well dispersed in both polar solvents and nonpolar solvent. Finally, dispersions of hollow CIOMBs in tetrachloroethylene had successfully been applied in electrophoretic displays
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