102 research outputs found
Fault Signature Identification for BLDC motor Drive System -A Statistical Signal Fusion Approach
A hybrid approach based on multirate signal processing and sensory data
fusion is proposed for the condition monitoring and identification of fault
signal signatures used in the Flight ECS (Engine Control System) unit. Though
motor current signature analysis (MCSA) is widely used for fault detection
now-a-days, the proposed hybrid method qualifies as one of the most powerful
online/offline techniques for diagnosing the process faults. Existing
approaches have some drawbacks that can degrade the performance and accuracy of
a process-diagnosis system. In particular, it is very difficult to detect
random stochastic noise due to the nonlinear behavior of valve controller.
Using only Short Time Fourier Transform (STFT), frequency leakage and the small
amplitude of the current components related to the fault can be observed, but
the fault due to the controller behavior cannot be observed. Therefore, a
framework of advanced multirate signal and data-processing aided with sensor
fusion algorithms is proposed in this article and satisfactory results are
obtained. For implementing the system, a DSP-based BLDC motor controller with
three-phase inverter module (TMS 320F2812) is used and the performance of the
proposed method is validated on real time data.Comment: 7 Pages, 7 figure
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A New Route to Highly Stretchable and Soft Inorganic–Organic Hybrid Elastomers Using Polydimethylsiloxane as Crosslinker of Epoxidized Natural Rubber
Sulfur or peroxide crosslinking is the most common and conventional method to develop elastomeric materials. A new approach to crosslink epoxidized natural rubber (ENR) by aminopropyl terminated polydimethylsiloxane (AT-PDMS) is described, intending to develop a new kind of hybrid organic–inorganic elastomers. The curing reaction is accelerated by using hydroquinone as a catalyst. The formation of the hybrid structure is evident from the appearance of two glass transition temperatures, at −1 and −120 °C, for the ENR and PDMS phases, respectively. The curing reaction is found to be of first order with respect to amine concentration with the estimated activation energy of ≈62 kJ mol−1. Comparing the mechanical properties to a typical ENR-sulfur system leads to the conclusion that the ENR/AT-PDMS hybrid structure is highly stretchable and soft, as demonstrated by its relatively higher strain at failure (up to ≈630%), and lower hardness and modulus values. The higher stretchability and soft nature of the material are achieved by introducing flexible PDMS chains during the curing process resulting to a hybrid elastomer networks. This kind of soft but robust materials can find several applications in diverse fields, such as soft robotics, flexible, and stretchable electronics
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Synthesis and characterization of poly(1,2,3-triazole)s with inherent high sulfur content for optical applications
The synthesis of solution-processable sulfur-containing polytriazoles for optoelectronic applications is a relatively less explored domain in polymer research. The synthesis of novel bifunctional (DA) and trifunctional (TA) azido-monomers with inherent high sulfur content and of organo-soluble high refractive index poly(1,2,3-triazole)s using the azido-monomers via Cu(I) assisted click polymerization reactions are reported in this work. The azido-monomers were synthesized by the conversion of previously reported amine-functionalized compounds to azides using azidotrimethylsilane in a polar aprotic solvent. Dialkyne monomers were also synthesized and reacted with the azides to prepare a series of five linear and two hyperbranched poly(1,2,3-triazole)s. Fourier transform infrared spectroscopy, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and thermogravimetric analysis were used to characterize the synthesized polymers. It was also demonstrated that the use of the trifunctional azide in optimized conditions resulted in increased solubility of an otherwise insoluble linear poly(1,2,3-triazole). The optical characterization of the polymers was carried out on thin polymer films with thickness in the nanometer range, which were successfully prepared by spin-coating on silicon wafers. It was found that the increase in the sulfur and aromatic content in the polymer backbone successfully increased the refractive index of the polymers up to 1.743 at 589 nm
Electronic Structure Prediction of Multi-million Atom Systems Through Uncertainty Quantification Enabled Transfer Learning
The ground state electron density - obtainable using Kohn-Sham Density
Functional Theory (KS-DFT) simulations - contains a wealth of material
information, making its prediction via machine learning (ML) models attractive.
However, the computational expense of KS-DFT scales cubically with system size
which tends to stymie training data generation, making it difficult to develop
quantifiably accurate ML models that are applicable across many scales and
system configurations. Here, we address these fundamental challenges using
Bayesian neural networks and employ transfer learning to leverage the
multi-scale nature of the training data. Our ML models employ descriptors
involving simple scalar products, comprehensively sample system configurations
through thermalization, and quantify uncertainty in electron density
predictions. We show that our models incur significantly lower data generation
costs while allowing confident - and when verifiable, accurate - predictions
for a wide variety of bulk systems well beyond training, including systems with
defects, different alloy compositions, and at unprecedented, multi-million-atom
scales
Distribution of hepatitis B virus genotypes: Phylogenetic analysis and virological characteristics of Genotype C circulating among HBV carriers in Kolkata, Eastern India
Aim: To evaluate the genotype distribution of hepatitis B virus (HBV) in Eastern India and to clarify the phylogenetic origin and virological characteristics of the recently identified genotype C in this region. Methods: Genotype determination, T1762/A1764 mutation in the basal core promoter (BCP) and A1896 mutation in the precore region of 230 subjects were determined by restriction fragment length polymorphism method (RFLP) and the result was confirmed by direct sequencing. Results: The predominant genotypes D (HBV/D) and A (HBV/A) were detected in 131/230 (57%) and 57/230 (25%) samples. In addition, genotype C (HBV/C) was detected in 42/230 (18%) isolates. Surface gene region was sequenced from 45 isolates (27 HBV/C, 9 HBV/A and 9 HBV/D). Phylogenetic analysis revealed that all of the HBV/C sequences clustered with South East Asian subgenotype (HBV/Cs). The sequence data showed remarkable similarity with a Thai strain (AF068756) (99.5% ± 0.4% nucleotide identities) in 90% of the genotype C strains analyzed. T1762/A1764 mutation in BCP region, associated with high ALT was significantly higher in HBeAg negative isolates than HBeAg positive isolates. Frequency of A1896 mutation leading to HBeAg negativity was low. Conclusion: The present study reports the genotypic distribution and the characteristics of partial genome sequences of HBV/C isolates from Eastern India. Low genetic diversity and confinement of HBV/C in Eastern India possibly indicate a recent, limited, spread in this region. Genotype C with T1762/A1764 mutation has been reported to increase the risk for hepatocellular carcinoma; therefore genotype C carriers in Eastern India should be carefully monitored
A Follow-Up Study on the Efficacy of the Homeopathic Remedy Arsenicum album in Volunteers Living in High Risk Arsenic Contaminated Areas
In continuation of our short-term pilot studies reported earlier, results on certain toxicity biomarkers in volunteers who continued to take the potentized Arsenicum album 200C till 2 years are presented. Out of some 130 “verum”-fed volunteers of pilot study, 96 continued to take the remedy till 6 months, 65 till 1 year and 15 among them continued till 2 years. They provided samples of their urine and blood at 6 months, 1 year and finally at 2 years. None out of 17 who received “placebo” turned up for providing blood or urine at these longer intervals. Standard methodologies were used for determination of arsenic content in blood and urine, and for measurement of toxicity biomarkers like acid and alkaline phosphatases, alanine and aspartate amino transferases, lipid peroxidation and reduced glutathione and anti-nuclear antibody titers. Most of the volunteers reported status quo maintained after the improvement they achieved within the first 3 months of homeopathic treatment, in respect of their general health and spirit, and appetite and sleep. A few with skin symptoms and burning sensation, however, improved further. This was supported by the data of toxicity biomarkers, levels of all of which remained fairly within normal range. Therefore, administration of Arsenicum album 200C considerably ameliorates symptoms of arsenic toxicity on a long-term basis, and can be recommended for interim use, particularly in high risk remote villages lacking modern medical and arsenic free drinking water facilities. Similar studies by others are encouraged
SYNTHESIS & IN-VITRO PROTEIN DENATURATION SCREENING OF 2-[(1, 5-DISUBSTITUTEDPHENYL-4,5-DIHYDRO-1H-PYRAZOL-3-YL)OXY]BENZOIC ACID DERIVATIVES
Abstract
Novel 2-[(1,5-diphenyl-4,5-dihydro-1H-pyrazol-3-yl)oxy]benzoic acid (2a) & 2-[5-(2-hydroxyphenyl)-1-Phenyl-4,5-dihydro-1H-pyrazol-3-yl]benzoic acid (2b) were produced and examined for their in-vitro protein denaturation activities. It was discovered that compound 2b showed promise and had more potency than acetylsalicylic acid (NSAID) in inhibiting denaturation of bovine serum albumin. Docking research also supports this. The compound 2b has the highest docking scores with COX1(PDB ID 3N8Z), COX2 (PDB ID 4PH9), and TNF (PDB ID 2AZ5), respectively, of Etotal -233.75, -256.48, and -255.83. TLC and elemental tests were used to determine the compounds' purity. All of the generated molecules' analytical and spectral data (1H NMR, FTIR, and MS) were entirely consistent with the proposed structures
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