Energy-resolved neutron imaging for reconstruction of strain introduced by cold working

Energy-resolved neutron transmission imaging is used to reconstruct maps of residual strains in drilled and cold-expanded holes in 5-mm and 6.4-mm-thick aluminum plates. The possibility of measuring the positions of Bragg edges in the transmission spectrum in each 55 × 55 µm2 pixel is utilized in the reconstruction of the strain distribution within the entire imaged area of the sample, all from a single measurement. Although the reconstructed strain is averaged through the sample thickness, this technique reveals strain asymmetries within the sample and thus provides information complementary to other well-established non-destructive testing methods

Characterization and application of Bragg-edge transmission imaging for strain measurement and crystallographic analysis on the IMAT beamline

This paper presents a series of experiments to characterize the performance of the new IMAT beamline at the ISIS pulsed neutron source and provides examples to showcase the potential applications of Bragg-edge transmission imaging on the instrument. The characterization includes determination of the IMAT spectral and spatial resolutions through calibration measurements, and also determination of the precision and the accuracy of Bragg-edge analysis for lattice parameters of ceramics, metals and textured engineering alloys through high-temperature measurements. A novel Bragg-edge analysis method based on the cross-correlation of different Bragg edges has been developed to provide an estimate of the change in lattice parameter, which is especially useful for measurements of textured samples. Three different applications of the Bragg-edge transmission imaging technique are presented, including strain mapping, texture mapping and obtaining crystallographic information, i.e. the dependence on temperature of the Debye–Waller factor. The experimental results demonstrate the ability of the IMAT beamline to provide accurate strain measurements with uncertainties as low as 90 µ[epsilon] with reasonable measurement time, while characteristic materials parameters can be mapped across the sample with a spatial resolution of 300–600 µm for a strain map and down to ∼90 µm for a texture map

A new thermography using inelastic scattering analysis of wavelength-resolved neutron transmission imaging

Abstract Thermography using energy-dependent neutron transmission imaging can non-invasively and non-destructively visualize a real-space distribution of interior temperatures of a material in a container. Previously, resonance absorption broadening analysis and Bragg-edge shift analysis using energy-resolved neutron transmission have been developed, however some issues remain, e.g., imaging efficiency, substance limitation and temperature sensitivity. For this reason, we propose a new neutron thermography using the temperature dependence of inelastic scattering of cold neutrons. This method has some advantages, for example, the imaging efficiency is high because cold neutrons are measured with moderate wavelength resolution, and light elements can be analysed in principle. We investigated the feasibility of this new neutron thermography at pulsed neutron time-of-flight imaging instruments at ISIS in the United Kingdom and HUNS in Japan. A Rietveld-type transmission spectrum analysis program (RITS) was employed to refine temperature and atomic displacement parameters from the inelastic scattering cross-section analysis. Finally, we demonstrated interior thermography of an α-Fe sample of 10 mm thickness inside a vacuum chamber by using a neutron time-of-flight imaging detector at the compact accelerator-driven pulsed neutron source HUNS

Characterization and application of Bragg-edge transmission imaging for strain measurement and crystallographic analysis on the IMAT beamline

This paper presents a series of experiments to characterize the performance of the new IMAT beamline at the ISIS pulsed neutron source and provides examples to showcase the potential applications of Bragg-edge transmission imaging on the instrument. The characterization includes determination of the IMAT spectral and spatial resolutions through calibration measurements, and also determination of the precision and the accuracy of Bragg-edge analysis for lattice parameters of ceramics, metals and textured engineering alloys through high-temperature measurements. A novel Bragg-edge analysis method based on the cross-correlation of different Bragg edges has been developed to provide an estimate of the change in lattice parameter, which is especially useful for measurements of textured samples. Three different applications of the Bragg-edge transmission imaging technique are presented, including strain mapping, texture mapping and obtaining crystallographic information, i.e. the dependence on temperature of the Debye–Waller factor. The experimental results demonstrate the ability of the IMAT beamline to provide accurate strain measurements with uncertainties as low as 90 µ[epsilon] with reasonable measurement time, while characteristic materials parameters can be mapped across the sample with a spatial resolution of 300–600 µm for a strain map and down to ∼90 µm for a texture map

Exploring 3D X-Ray Diffraction Method to Validate Approaches in Materials Modelling

Cyclic high temperature deformation, which is a precursor to creep-fatigue damage is one of the main life limiting factors in thermal power plants. Microstructurally informed models such as crystal plasticity have shown great promise in predicting cyclic plasticity and creep deformation; however, further validation of predicted meso-scale deformation is required to ensure accurate damage calculations. Here, a novel 3D X-ray diffraction (3DXRD) experiment was performed to resolve and investigate the response of individual grains within a polycrystalline material under loading at elevated temperature. Specimens were made from 316H stainless steel, which is an alloy commonly used for critical structural components in thermal power generation plants. The 3DXRD experiments were conducted at the UK national synchrotron facility, Diamond Light Source. The measurements provided positions, strain tensors, and orientations of individual grains within a gauge volume. The data generated from 3DXRD was used both as an input and for the validation of a crystal plasticity finite element model (CPFE). The results provided demonstrate the importance of microstructural information in materials modelling.<br/

Mapping residual strain induced by cold working and by laser shock peening using neutron transmission spectroscopy

This paper presents 2D mapping of residual strains, induced by cold expansion and laser shock peening processing of aluminium alloy samples, by using Bragg edge neutron transmission. Neutron transmission uses information contained in the neutron beam transmitted through a sample. It is shown that neutron transmission strain mapping with high spatial resolution can provide important insights into the distribution of residual strains associated with processing of materials. The residual strain field around a cold-expanded hole can be revealed in detail, as can be the residual strain profile associated with laser peening. Results are correlated with measurements obtained by conventional neutron diffraction and incremental hole drilling. The residual strain variation around the cold-expanded hole and the depth of compressive residual strain generated by the peening process were captured with high spatial resolution, showing the advantages of neutron transmission over other well-established strain measurement methods by non-destructively generating a map of residual strains over a large area