31 research outputs found

    Principles of non-contact A.C. Calorimetry

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    Thermophysikalische Eigenschaften und Glasbildung unterkuehlter metallischer Schmelzen Abschlussbericht

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    SIGLEAvailable from TIB Hannover: F01B137+a / FIZ - Fachinformationszzentrum Karlsruhe / TIB - Technische InformationsbibliothekBundesministerium fuer Bildung, Wissenschaft, Forschung und Technologie, Bonn (Germany)DEGerman

    Surface tension and viscosity of the Ni-based superalloys LEK94 and CMSX-10 measured by the Oscillating Drop Method on board a parabolic flight

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    The surface tension and viscosity of the Ni-based superalloys LEK94 and CMSX-10 were measured by the oscillating drop method in a containerless electromagnetic processing device on board a parabolic flight airplane. Surface oscillations were recorded by 150 and 200 Hz Frame rate digital cameras positioned in two perpendicular directions and by the inductive coupling between the oscillating sample surface and the oscillating circuit of the radio frequency heating and positioning generator. The surface tension as a function of temperature of LEK94 and CMSX-10 was obtained as r(T) = 1.73 � 4.51 9 10�4 [T—1656 K (1383 �C)] Nm�1 and r(T) = 1.71 � 5.80 9 10�4 [(T—1683 K (1410 �C)] Nm�1, respectively. The viscosity at the liquidus temperatures as 9.8 and 7.8 mPa.s, respectively. In addition, some basic thermophysical properties such as solidus and liquidus temperatures, densities at room temperature, and thermal expansion in the solid phase are reported

    Structural investigation of the stability in temperature of some high entropy alloys as a function of their electronic structure

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    International audienceHigh Entropy Alloys (HEA) can be classified in three domains according to their e/a and r values, with e/a, the number of itinerant valence electrons and r the average radius for a 12 nearest atoms neighborhood. The phase composition, thermal stability and possible phase transformations of a series of HEA alloys, CoCrzFeNi-XY (with X and Y = Al, Cu, Pd, Ru, Ti and z=0 or 1), selected according to their e/a ratio were investigated in cast conditions (T0), after 3 hours homogenization at 1100°C (T1) and after 3 hours annealing at 700°C (T3). It is observed that for the alloys from domain I which contains fcc structures, the microstructure transforms from multi-to almost single-phase under homogenization (T1). In domain III alloys contains cubic (bcc and/or B2) structures very small multi-structural changes are observed. Alloys in domain II have mixed structure, i.e. several different structures in the diffraction pattern, which changes during heat treatments
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