Probing microwave fields and enabling in-situ experiments in a transmission electron microscope.

A technique is presented whereby the performance of a microwave device is evaluated by mapping local field distributions using Lorentz transmission electron microscopy (L-TEM). We demonstrate the method by measuring the polarisation state of the electromagnetic fields produced by a microstrip waveguide as a function of its gigahertz operating frequency. The forward and backward propagating electromagnetic fields produced by the waveguide, in a specimen-free experiment, exert Lorentz forces on the propagating electron beam. Importantly, in addition to the mapping of dynamic fields, this novel method allows detection of effects of microwave fields on specimens, such as observing ferromagnetic materials at resonance

Magnetic levitation by rotation

A permanent magnet can be levitated simply by placing it in the vicinity of another permanent magnet that rotates in the order of 200 Hz. This surprising effect can be easily reproduced in the lab with off-the-shelf components. Here we investigate this novel type of magnetic levitation experimentally and clarify the underlying physics. Using a 19 mm diameter spherical NdFeB magnet as rotor magnet, we capture the detailed motion of levitating, spherical NdFeB magnets, denoted floater magnets. We find that as levitation occurs, the floater magnet frequency-locks with the rotor magnet, and, noticeably, that the magnetization of the floater is oriented close to the axis of rotation and towards the like pole of the rotor magnet. This is in contrast to what might be expected by the laws of magnetostatics as the floater is observed to align its magnetization essentially perpendicular to the magnetic field of the rotor. Moreover, we find that the size of the floater has a clear influence on the levitation: the smaller the floater, the higher the rotor speed necessary to achieve levitation, and the further away the levitation point shifts. We verify that magnetostatic interactions between the rotating magnets are responsible for creating the equilibrium position of the floater. Hence, this type of magnetic levitation does not rely on gravity as a balancing force to achieve an equilibrium position. Based on theoretical arguments and a numerical model, we show that a constant, vertical field and eddy-current enhanced damping is sufficient to produce levitation from rest. This enables a gyroscopically stabilised counter-intuitive steady-state moment orientation, and the resulting magnetostatically stable, mid-air equilibrium point. The numerical model display the same trends with respect to rotation speed and the floater magnet size as seen in the experiments.Comment: 15 pages, 6 figures, 10 videos + 8 pages supplementary material. Videos available at https://youtube.com/playlist?list=PLOfbFSFa_WoK4PgYQXhuNucS_WcIxXDE

The Application of Off-Axis Electron Holography to Electrically Biased Single GaN Nanowires for Electrical Resistivity Measurement

Extended abstract of a paper presented at Microscopy and Microanalysis 2013 in Indianapolis, Indiana, USA, August 4 – August 8, 2013.</jats:p

The colours of durum wheat: a review

Abstract. Pigments are essential to the life of all living organisms. Animals and plants have been the subjects of basic and applied research with the aim of determining the basis of the accumulation and physiological roles of pigments. In crop species, the edible organs show large variations in colour. In durumwheat grain, which is a staple food for humans, the colour is mainly due to two natural classes of pigment: carotenoids and anthocyanins. The carotenoids provide the yellow pigmentation of the durum wheat endosperm, and consequently of the semolina, which has important implications for the marketing of end products based on durumwheat. Anthocyanins accumulate in the aleurone or pericarp of durumwheat and provide the blue, purple and red colours of the grain. Both the carotenoids and the anthocyanins are known to provide benefits for human health, in terms of decreased risks of certain diseases. Therefore, accumulation of these pigments in the grain represents an important trait in breeding programs aimed at improving the nutritional value of durumwheat grain and its end products. This review focuses on the biochemical and genetic bases of pigment accumulation in durum wheat grain, and on the breeding strategies aimed at modifying grain colour

Metabolic Profiling of a Mapping Population Exposes New Insights in the Regulation of Seed Metabolism and Seed, Fruit, and Plant Relations

To investigate the regulation of seed metabolism and to estimate the degree of metabolic natural variability, metabolite profiling and network analysis were applied to a collection of 76 different homozygous tomato introgression lines (ILs) grown in the field in two consecutive harvest seasons. Factorial ANOVA confirmed the presence of 30 metabolite quantitative trait loci (mQTL). Amino acid contents displayed a high degree of variability across the population, with similar patterns across the two seasons, while sugars exhibited significant seasonal fluctuations. Upon integration of data for tomato pericarp metabolite profiling, factorial ANOVA identified the main factor for metabolic polymorphism to be the genotypic background rather than the environment or the tissue. Analysis of the coefficient of variance indicated greater phenotypic plasticity in the ILs than in the M82 tomato cultivar. Broad-sense estimate of heritability suggested that the mode of inheritance of metabolite traits in the seed differed from that in the fruit. Correlation-based metabolic network analysis comparing metabolite data for the seed with that for the pericarp showed that the seed network displayed tighter interdependence of metabolic processes than the fruit. Amino acids in the seed metabolic network were shown to play a central hub-like role in the topology of the network, maintaining high interactions with other metabolite categories, i.e., sugars and organic acids. Network analysis identified six exceptionally highly co-regulated amino acids, Gly, Ser, Thr, Ile, Val, and Pro. The strong interdependence of this group was confirmed by the mQTL mapping. Taken together these results (i) reflect the extensive redundancy of the regulation underlying seed metabolism, (ii) demonstrate the tight co-ordination of seed metabolism with respect to fruit metabolism, and (iii) emphasize the centrality of the amino acid module in the seed metabolic network. Finally, the study highlights the added value of integrating metabolic network analysis with mQTL mapping

Dipolar Magnetism in Ordered and Disordered Low-Dimensional Nanoparticle Assemblies

Magnetostatic (dipolar) interactions between nanoparticles promise to open new ways to design nanocrystalline magnetic materials and devices if the collective magnetic properties can be controlled at the nanoparticle level. Magnetic dipolar interactions are sufficiently strong to sustain magnetic order at ambient temperature in assemblies of closely-spaced nanoparticles with magnetic moments of ≥ 100 μB. Here we use electron holography with sub-particle resolution to reveal the correlation between particle arrangement and magnetic order in self-assembled 1D and quasi-2D arrangements of 15 nm cobalt nanoparticles. In the initial states, we observe dipolar ferromagnetism, antiferromagnetism and local flux closure, depending on the particle arrangement. Surprisingly, after magnetic saturation, measurements and numerical simulations show that overall ferromagnetic order exists in the present nanoparticle assemblies even when their arrangement is completely disordered. Such direct quantification of the correlation between topological and magnetic order is essential for the technological exploitation of magnetic quasi-2D nanoparticle assemblies