Utilization of Some Fruits and Vegetables By-Products to Produce High Dietary Fiber Jam

The present study aimed to investigate the chemical composition, antioxidant activity, total phenolic compounds and ?-carotene of carrot peels, apple pomace, banana peels and mandarin peels and their quality in preparing jam. Mandarin and banana peels characterized by its higher crude fiber (12.16 and 5.25%) and vitamin C (68 and 16.6 mg/100g) compared to carrot peels (3.91%) and apple pomace (3.65%). Banana peels contained higher amount of magnesium, potassium, calcium and iron compared to other peels samples. Therefore, jam of banana peels characterized by its higher content in magnesium (758 mg/100g), potassium (779 mg/100g), calcium (191 mg/100g) and iron (59.15 mg/100g). Jam of apple pomace characterized by its higher phosphorus contents (220 mg/100g) followed by jam of banana peels (138 mg/100g), mandarin peels (128 mg/100g) and carrot peels (53 mg/100g). Jam of carrot peels characterized by its higher phenolics content as gallic acid equivalent (87.4 mg/100g) followed by jams of apple pomace (82.5 mg/100g), banana peels (42.7 mg/100g) and mandarin peels (34.6 mg/100g). The same trend was observed in total flavonoids as catechen equivalent (mg CAT/100g) in jams of carrot peels, apple pomace, banana peels and mandarin peels, where they were 35.9, 30.1, 23.5 and 21.7, respectively. Furthermore, jam of carrot peels had higher antioxidant activity, where its DPPH radical, had lower DPPH based IC50 (1.8 ?g/ml) while jam of apple pomace, banana peels and mandarin peels had higher DPPH based IC50 reached to 2.04, 2.21 and 3.34 µg/ml, respectively. The same trend was observed for the ?-carotene radical in tested jam samples. Hunter color parameter showed that jam of mandarin peels had highest lightness (L* = 39.8), followed by jam of carrot peels (29.46), apple pomace (18.27) and banana peels (15.19). Therefore, jam of banana peels was darker than other tested peels samples. Sensory evaluation showed that jam of apple pomace characterized by its higher taste and odor, followed by jam of mandarin peels, banana peels and carrot peels. Color of tested jam of carrot, banana or mandarin peels was darker than apple pomace jam. Also, jam of apple pomace gave higher scores in appearance and overall acceptability. Keywords: Jam – Peels – antioxidant activity – Total phenolics– Total Flavonoid

Excess Spin and the Dynamics of Antiferromagnetic Ferritin

Temperature-dependent magnetization measurements on a series of synthetic ferritin proteins containing from 100 to 3000 Fe(III) ions are used to determine the uncompensated moment of these antiferromagnetic particles. The results are compared with recent theories of macroscopic quantum coherence which explicitly include the effect of this excess moment. The scaling of the excess moment with protein size is consistent with a simple model of finite size effects and sublattice noncompensation.Comment: 4 pages, 3 Postsript figures, 1 table. Submitted to PR

Statistical inference for the Nadarajah-Haghighi distribution based on ranked set sampling with applications

In this article, the maximum likelihood and Bayes inference methods are discussed for determining the two unknown parameters and specific lifetime parameters of the Nadarajah-Haghighi distribution, such as the survival and hazard rate functions, with the inclusion of ranked set sampling and simple random sampling. The estimated confidence intervals for the two parameters and any function of them are developed based on the Fisher-information matrix. Metropolis-Hastings algorithm and Lindley-approximation are used for generating the Bayes estimates and related highest posterior density credible ranges for the unknown parameters and reliability parameters under the presumption of conjugate gamma priors. A Monte-Carlo simulation study and a real-life data set have been used to assess the efficacy of the proposed methods

Estimation in Step-Stress Accelerated Life Tests for Weibull Distribution with Progressive First-Failure Censoring

Abstract: Based on progressive first-failure censoring, step-stress partially accelerated life tests are considered when the lifetime of a product follows Weibull distribution. The maximum likelihood estimates (MLEs) are obtained for the distribution parameters and the acceleration factor. In addition, asymptotic variance and covariance matrix of the estimators are given. Furthermore, confidence intervals of the estimators are presented. The optimal stress change time for the step-stress partially accelerated life test is determined by minimizing the asymptotic variance of MLEs of the model parameters and the acceleration factor. Simulation results are carried out to study the precision of the MLEs for the parameters involved

Validated stability indicating liquid chromatographic determination of ebastine in pharmaceuticals after pre column derivatization: Application to tablets and content uniformity testing

An accurate, simple, sensitive and selective reversed phase liquid chromatographic method has been developed for the determination of ebastine in its pharmaceutical preparations. The proposed method depends on the complexation ability of the studied drug with Zn2+ ions. Reversed phase chromatography was conducted using an ODS C18 (150 × 4.6 mm id) stainless steel column at ambient temperature with UV-detection at 260 nm. A mobile phase containing 0.025%w/v Zn2+ in a mixture of (acetonitril/methanol; 1/4) and Britton Robinson buffer (65:35, v/v) adjusted to pH 4.2, has been used for the determination of ebastine at a flow rate of 1 ml/min. The calibration curve was rectilinear over the concentration range of 0.3 - 6.0 μg/ml with a detection limit (LOD) of 0.13 μg/ml, and quantification limit (LOQ) of 0.26 μg/ml. The proposed method was successfully applied for the analysis of ebastine in its dosage forms, the obtained results were favorably compared with those obtained by a comparison method. Furthermore, content uniformity testing of the studied pharmaceutical formulations was also conducted. The composition of the complex as well as its stability constant was also investigated. Moreover, the proposed method was found to be a stability indicating one and was utilized to investigate the kinetics of alkaline and ultraviolet induced degradation of the drug. The first-order rate constant and half life of the degradation products were calculated

Validated stability-indicating spectrofluorimetric methods for the determination of ebastine in pharmaceutical preparations

Two sensitive, selective, economic, and validated spectrofluorimetric methods were developed for the determination of ebastine (EBS) in pharmaceutical preparations depending on reaction with its tertiary amino group. Method I involves condensation of the drug with mixed anhydrides (citric and acetic anhydrides) producing a product with intense fluorescence, which was measured at 496 nm after excitation at 388 nm

Evaluation of color change in CAD-On restorations using different core/veneer thickness ratios and different veneer translucencies

Statement of problem: The introduction of partially stabilized zirconium dioxide to the dental field created a path for development of new designs and applications, but still, a minimum framework thickness of 0.5 mmwith the remaining thickness of the restoration used for building the ceramic veneer was always recommended. This might have possibly affected the final shade of the restorartion due to the whitish color of Y-TZP. Purpose: This in vitro study was designed to evaluate the color reproduction ability of CAD-veneered zirconia restorations through the effect of different core-veneer thickness ratios and different translucencies of the Cad-on veneering material. Methods: Sixty CAD-On restorations were constructed and classified into 3 groups (n ¼ 20) of different core/veneer thickness ratios (0.5:1 mm, 0.7:0.8 mm, 1:0.5 mm). Each group was subdivided into 2 subgroups (n ¼ 10) according to the CAD-On veneer translucency (High Translucency HT, Low Translucency LT). Cad-On restorations were constructed using the CEREC InLab CAD/CAM System. Color change (DE) between groups of the CAD-On restorations was measured using Vita EasyShade Compact. All data was statistically analyzed and presented as mean and standard deviation values. Repeated measurements of data were analyzed with analysis of variance (ANOVA) for significant differences. Results: There was significant difference (P \u3c 0.05) for varrying the core/veneer thickness ratio over (DE) while both the veneer translucency and interaction between the core/veneer thickness ratio and veneer transluency had no significant effect. Conclusion: There was a visually perceptible color change for all core/veneer thickness ratios and all veneer translucencies, but they were all in the clinically acceptable range

Migration and employment in the construction sector: Critical factors in Egyptian development

The migration of construction workers is having a strong effect on the construction sector and on the economy as a whole. There are costs and benefits to this migration. And there are policy implications that must be clearly understood so that the benefits can be made to outweigh the costs