63 research outputs found
Visitor satisfaction in ICU and recovery waiting rooms in acute-care hospitals
Call number: LD2668 .T4 ARCH 1989 M57Master of ArchitectureArchitectur
Synthesis of a tetrasaccharide analogue related to the repeating unit of the antigen from Klebsiella type 2
434-43
Chemoselective hydration of glycosyl cyanides to C-glycosyl formamides using ruthenium complexes in aqueous media
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Implementation and results of an integrated data quality assurance protocol in a randomized controlled trial in Uttar Pradesh, India
Convergent synthesis of the tetrasaccharide repeating unit of the O-antigen of Shigella boydii type 9 Full Research Paper
Abstract A convenient synthesis of the tetrasaccharide repeating unit of the O-antigen of Shigella boydii type 9 has been achieved in excellent yield using a [2 + 2] block glycosylation strategy. TEMPO-mediated selective oxidation of the primary alcohol of the tetrasaccharide derivative 8 to the carboxylic group followed by deprotection of the functional groups furnished target tetrasaccharide 1 as its 4-methoxyphenyl glycoside in high yield
Environmentally benign preparation of benzylidene acetal of carbohydrate derivatives in PEG 600
Short synthesis of the common trisaccharide core of kankanose and kankanoside isolated from Cistanche tubulosa
A short synthetic approach was developed for the synthesis of a common trisaccharide core found in kankanose, kankanoside F, H1, H2, and I isolated from the medicinally active plant Cistanche tubulosa. All glycosylations were carried out under nonmetallic reaction conditions. Yields were very good in all intermediate steps
Convergent synthesis of the tetrasaccharide repeating unit of the cell wall lipopolysaccharide of Escherichia coli O40
A tetrasaccharide repeating unit corresponding to the cell-wall lipopolysaccharide of E. coli O40 was synthesized by using a convergent block glycosylation strategy. A disaccharide donor was coupled to a disaccharide acceptor by a stereoselective glycosylation. A 2-aminoethyl linker was chosen as the anomeric protecting group at the reducing end of the tetrasaccharide. All glycosylation steps are significantly high yielding and stereoselective
Reaction of glycal derivatives with alcohols in the presence of N-bromosuccinimide and diphenyldiselenide:Preparation of 2-deoxy-2- phenylselenyl glycosides
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