Influence of gas flow rate on liquid distribution in trickle-beds using perforated plates as liquid distributors

Two wire mesh tomography devices and a liquid collector were used to study the influence of the gas flow rate on liquid distribution when fluids distribution on top of the reactor is ensured by a perforated plate. In opposition to most of the studies realized by other authors, conditions in which the gas has a negative impact in liquid distribution were evidenced. Indeed, the obtained results show that the influence of gas flow rate depends on the quality of the initial distribution, as the gas forces the liquid to "respect" the distribution imposed at the top of the reactor. Finally, a comparison between the two measuring techniques shows the limitations of the liquid collector and the improper conclusions to which its use could lead

Liquid Distribution in Trickle-Bed Reactor

The aim of this study is to develop techniques to qualify the efficiency of liquid distribution in trickle-bed reactors, using cold mockups. The experimental setup consists mainly in a 0. 3-m-ID packed-bed column with three different plates used to vary the quality of inlet liquid distribution. Liquid distribution has been qualified using several techniques: global pressure drop measurements, global RTD (Residence-Time Distribution) of the liquid, local heat transfer probes, capacitance tomography, collector at the bottom of the reactor with nine equal zones. The bed pressure drop and the overall external liquid saturation decrease when the maldistribution increases; quantitative information is however difficult to obtain this way. Global RTD of the liquid allows quantifying of the average liquid distribution in the bed. The local thermal sensors give an indication of local liquid velocity and indicate possible local maldistribution of the liquid (scale mm) even when global distribution is good. Concerning the results obtained with the collector, a maldistribution index is defined, ranging from 0 (ideal distribution) to 1 (worst possible distribution), and the influence of the different operating parameters (gas and liquid velocities, particle shape) is discussed

Liquid Distribution in Trickle-Bed Reactor

International audienceThe aim of this study is to develop techniques to qualify the efficiency of liquid distribution in trickle-bed reactors, using cold mockups. The experimental setup consists mainly in a 0. 3-m-ID packed-bed column with three different plates used to vary the quality of inlet liquid distribution. Liquid distribution has been qualified using several techniques: global pressure drop measurements, global RTD (Residence-Time Distribution) of the liquid, local heat transfer probes, capacitance tomography, collector at the bottom of the reactor with nine equal zones. The bed pressure drop and the overall external liquid saturation decrease when the maldistribution increases; quantitative information is however difficult to obtain this way. Global RTD of the liquid allows quantifying of the average liquid distribution in the bed. The local thermal sensors give an indication of local liquid velocity and indicate possible local maldistribution of the liquid (scale mm) even when global distribution is good. Concerning the results obtained with the collector, a maldistribution index is defined, ranging from 0 (ideal distribution) to 1 (worst possible distribution), and the influence of the different operating parameters (gas and liquid velocities, particle shape) is discussed