13,375 research outputs found
X-ray powder diffraction of high-absorption materials at the XRD1 beamline off the best conditions: Application to (Gd,Nd)5Si4 compounds
Representative compounds of the new family of magnetic materials Gd5-xNdxSi4
were analyzed by X-ray diffraction at the XRD1 beamline at LNLS. To reduce
X-ray absorption, thin layers of the powder samples were mounted outside the
capillaries and measured in Debye-Scherrer geometry as usual. The X-ray
diffraction analyses and the magnetometry results indicate that the behavior of
the magnetic transition temperature as a function of Nd content may be directly
related to the average of the four smallest interatomic distances between
different rare earth sites of the majority phase of each compound. The quality
and consistency of the results show that the XRD1 beamline is able to perform
satisfactory X-ray diffraction experiments on high-absorption materials even
off the best conditions.Comment: 12 pages, 3 figures, 3 table
Mechanisms of direct reactions with halo nuclei
Halo nuclei are exotic nuclei which exhibit a strongly clusterised structure:
they can be seen as one or two valence nucleons loosely bound to a core. Being
observed at the ridge of the valley of stability, halo nuclei are studied
mostly through reactions. In this contribution the reaction models most
commonly used to analyse experimental data are reviewed and compared to one
another. A reaction observable built on the ratio of two angular distributions
is then presented. This ratio enables removing most of the sensitivity to the
reaction mechanism, which emphasises the effects of nuclear structure on the
reaction.Comment: Invited talk given by Pierre Capel at the "10th International
Conference on Clustering Aspects of Nuclear Structure and Dynamics"
(Cluster12), Debrecen, Hungary, 24-28 September 2012. To appear in the
Cluster12 Proceedings in the Open Access Journal of Physics: Conference
Series (JPCS). (5 pages, 3 figures
Nonlinear dynamics of relativistic charged particle beams
The idea behind this work is to analyze the transversal dynamics of a relativistic charged particle beam. The beam is azimuthally symmetric, focused by a constant magnetic field and supposed to be initially cold. While mismatched, nonrelativistic, and homogeneous beams oscillate with an invariant cold density profile, it is shown that relativistic homogeneous beams progressively heat and lose an important amount of constituents during its magnetic confinement. This heating process starts with phase-space wave-breaking, a mechanism observed before in initially inhomogeneous beams. The results have been obtained with full self-consistent N-particle beam numerical simulations
Synthesis and properties of Co-doped titanate nanotubes and their optical sensitization with methylene blue
Here we report on a novel chemical route to synthesize homogenous cobalt
doped titanate nanotubes (CoTNT), using an amorphous Co-doped precursor. The
influence of the synthesis temperature, autoclave dwell time and metal doping
on the structural and microstructural as well as on the optical properties of
the synthesized titanate nanotubes is studied and discussed. The optical band
gaps of the CoTNT samples are red shifted in comparison with the values
determined for the undoped samples, such red shifts bringing the absorption
edge of the CoTNT samples into the visible region. CoTNT materials also
demonstrate particular high adsorption ability for methylene blue, the amount
of the adsorbed dye being higher than the one predictable for a monolayer
formation. This suggests the possibility of intercalation of the dye molecule
between the TiO6 layers of the TNT structure. It is also shown that the
methylene blue sensitized Co-doped nanostructures are highly stable under UV
radiation and present a strong and broad absorption in the visible region.Comment: 31 pages, 3 tables, 7 figure
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