Direct comparison of the performance of CZT detectors contacted with various metals

Cadmium Zinc Telluride (CZT) achieves excellent spatial resolution and good energy resolution over the broad energy range from several keV into the MeV energy range. In this paper we present the results of a systematic study of the performance of CZT detectors manufacturered by Orbotech (before IMARAD) depending on surface preparation, contact materials and contact deposition. The standard Orbotech detectors have the dimension of 2.0 x 2.0 x 0.5 cm. They have a pixellated In anode with 8 x 8 pixels and a monolithic In cathode. Using the same CZT substrates several times, we have made a direct comparison of the performance of different contact materials by replacing the cathode and/or the anode contacts with several high-workfunction metals. We present the performance of the detectors and conclude with an overview over our ongoing detector optimization.Comment: 8 pages, 5 figures, to appear in the proceedings of the conference 5922, "Hard X-Ray and Gamma-Ray Detector Physics VII" on the "Optics & Photonics 2005" SPIE Symposium, July 31- August 4, 2005, San Diego, C

Evaluation of Bovine Embryo Biopsy Techniques according to Their Ability to Preserve Embryo Viability

The purpose of this research was to evaluate three embryo biopsy techniques used for preimplantation genetic diagnosis (PGD) in cattle and to recommend the least invasive one for current use, especially when PGD is followed by embryo cryopreservation. Three hundred bovine embryos were biopsied by either one of the needle, aspiration or microblade method, and then checked for viability by freezing/thawing and transplantation to recipient cows. The number of pregnancies obtained after the transfer of biopsied frozen/thawed embryos was assessed 30 days later using ultrasounds. The results were significantly different between the three biopsy methods: the pregnancy rate was of 57% in cows that received embryos biopsied by needle, 43% in cows that received embryos biopsied by aspiration, and 31% in cows that received embryos biopsied by microblade. Choosing an adequate biopsy method is therefore of great importance in embryos that will undergo subsequent cryopreservation, as it significantly influences their viability after thawing

Thick CZT Detectors for Space-Borne X-ray Astronomy

Cadmium Zinc Telluride (CZT) detectors are having a major impact on the field of hard X-ray astronomy. Without the need for cryogenic cooling they achieve good spatial and energy resolutions over the broad energy range from 10 keV to 600 keV. In this paper, we briefly review the historical development of detectors used in X-ray astronomy. Subsequently, we present an evaluation of CZT detectors from the company Imarad. The standard 2x2x0.5 cm detectors, contacted with 8x8 In pixels and an In cathode, exhibit FWHM energy resolutions of 7 keV at 59 keV, and 10 keV at 662 keV. A direct measurement of the 662 keV photopeak efficiency gives 67%. We have started a detailed study of the performance of Imarad detectors depending on surface preparation, contact materials, contact deposition, post-deposition detector annealing, and detector passivation techniques. We present first results from contacting detectors with Cr, Ag, Au, and Pt.Comment: Invited Contribution to the 49th International Symposium on Optical Science and Technology (SPIE), August 2004, Denver, CO, SPIE, 49, 5540, 13.01. (2004

FeCr₂S₄ in magnetic fields: possible evidence for a multiferroic ground state.

We report on neutron diffraction, thermal expansion, magnetostriction, dielectric, and specific heat measurements on polycrystalline FeCr2S4 in external magnetic fields. The ferrimagnetic ordering temperatures TC ≈ 170 K and the transition at TOO ≈ 10 K, which has been associated with orbital ordering, are only weakly shifted in magnetic fields up to 9 T. The cubic lattice parameter is found to decrease when entering the state below TOO. The magnetic moments of the Cr- and Fe-ions are reduced from the spin-only values throughout the magnetically ordered regime, but approach the spin-only values for fields >5.5 T. Thermal expansion in magnetic fields and magnetostriction experiments indicate a contraction of the sample below about 60 K. Below TOO this contraction is followed by a moderate expansion of the sample for fields larger than ~4.5 T. The transition at TOO is accompanied by an anomaly in the dielectric constant. The dielectric constant depends on both the strength and orientation of the external magnetic field with respect to the applied electric field for T < TOO. A linear correlation of the magnetic-field-induced change of the dielectric constant and the magnetic-field dependent magnetization is observed. This behaviour is consistent with the existence of a ferroelectric polarization and a multiferroic ground state below 10 K

Detailed Studies of Pixelated CZT Detectors Grown with the Modified Horizontal Bridgman Method

The detector material Cadmium Zinc Telluride (CZT), known for its high resolution over a broad energy range, is produced mainly by two methods: the Modified High-Pressure Bridgman (MHB) and the High-Pressure Bridgman (HPB) process. This study is based on MHB CZT substrates from the company Orbotech Medical Solutions Ltd. with a detector size of 2.0x2.0x0.5 cm^3, 8x8 pixels and a pitch of 2.46 mm. Former studies have emphasized only on the cathode material showing that high-work-function improve the energy resolution at lower energies. Therfore, we studied the influence of the anode material while keeping the cathode material constant. We used four different materials: Indium, Titanium, Chromium and Gold with work-functions between 4.1 eV and 5.1 eV. The low work-function materials Indium and Titanium achieved the best performance with energy resolutions: 2.0 keV (at 59 keV) and 1.9 keV (at 122 keV) for Titanium; 2.1 keV (at 59 keV) and 2.9 keV (at 122 keV) for Indium. These detectors are very competitive compared with the more expensive ones based on HPB material if one takes the large pixel pitch of 2.46 mm into account. We present a detailed comparison of our detector response with 3-D simulations, from which we determined the mobility-lifetime-products for electrons and holes. Finally, we evaluated the temperature dependency of the detector performance and mobility-lifetime-products, which is important for many applications. With decreasing temperature down to -30C the breakdown voltage increases and the electron mobility-lifetime-product decreases by about 30% over a range from 20C to -30C. This causes the energy resolution to deteriorate, but the concomitantly increasing breakdown voltage makes it possible to increase the applied bias voltage and restore the full performance.Comment: Accepted for publication in Astroparticle Physics, 25 pages, 13 figure

Research on environmental impact assessment of flame oxyacetylene welding processes

This paper presents the factors that may cause pollution of the work environment when working with the oxyacetylene flame welding process. Experiments were performed using an oven that allows the analysis of all gases resulted in the welding process, but also enables their monitoring using a video camera, and the resulting film was processed in that the frames for each second of experimentation were extracted. The materials used in the experiments were S235JR steel as the base material, and as filler materials, E70S. In order to assess the impact on the work environment of this welding process, the pollution coefficient CP was defined based on the equation of the material balance

Results of LLNL investigation of NYCT data sets

Upon examination we have concluded that none of the alarms indicate the presence of a real threat. A brief history and results from our examination of the NYCT ASP occupancy data sets dated from 2007-05-14 19:11:07 to 2007-06-20 15:46:15 are presented in this letter report. When the ASP data collection campaign at NYCT was completed, rather than being shut down, the Canberra ASP annunciator box was unplugged leaving the data acquisition system running. By the time it was discovered that the ASP was still acquiring data about 15,000 occupancies had been recorded. Among these were about 500 alarms (classified by the ASP analysis system as either Threat Alarms or Suspect Alarms). At your request, these alarms have been investigated. Our conclusion is that none of the alarm data sets indicate the presence of a real threat (within statistics). The data sets (ICD1 and ICD2 files with concurrent JPEG pictures) were delivered to LLNL on a removable hard drive labeled FOUO. The contents of the data disk amounted to 53.39 GB of data requiring over two days for the standard LLNL virus checking software to scan before work could really get started. Our first step was to walk through the directory structure of the disk and create a database of occupancies. For each occupancy, the database was populated with the occupancy date and time, occupancy number, file path to the ICD1 data and the alarm ('No Alarm', 'Suspect Alarm' or 'Threat Alarm') from the ICD2 file along with some other incidental data. In an attempt to get a global understanding of what was going on, we investigated the occupancy information. The occupancy date/time and alarm type were binned into one-hour counts. These data are shown in Figures 1 and 2