128 research outputs found

    The Internal Relationship, Linguistic and Theological, Between the Gospel of John and the Epistles of John

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    The intrinsic value of a paper such as the one here presented, lies not so much in the impression made by the finished product as in the profitable textual study which it entails. The task of digging deep into the language and theology of four books of the New Testament has been a pleasant one. In addition to the joy of working with the original Greek of the sacred New Testament, of making careful literal translations and thorough exegetical studies, there has been the added satisfaction of unfolding cumulative doctrinal evidence overwhelming in its depth and extent

    Session F-4: Developing Parametric Equations Using Mathematical Modeling

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    Designing project to develop student understanding of parametric equations and two modeling situations in which they are applied. No previous knowledge of parametrics is required by the students. The project requires two days of class time, with the remaining work done outside of class. This project is intended to be given three days into a unit on vectors

    Analysis of Minerals Using Linearly Polarized Infrared Microspectroscopy

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    This is an extended abstract of a paper presented at Microscopy and Microanalysis 2009 in Richmond, Virginia, USA, July 26 – July 30, 2009

    The Use of Raman Spectroscopy for the Identification of Forensically Relevant Body Fluid Stains

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    Raman spectroscopy is fast becoming a popular technique in the forensic science discipline, and more recently its focus has turned to biological samples. This study reveals the ability of Raman spectroscopy to identify some forensically relevant body fluids, both individually and within mixed samples, that can be crucial in some forensic investigations. This study also further demonstrates the capabilities of Raman as a means for human blood identification in simulated crime scene samples to include bloodstains on a variety of fabrics, at varying dilutions, following laundering, and with the use of various blood-enhancement reagents. The impact of washing and blood-enhancement reagents reveals the importance of the choice of method and its bearing on subsequent Raman analysis

    Collecting Quality Infrared Spectra from Microscopic Samples of Suspicious Powders in a Sealed Cell

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    The infrared (IR) microspectroscopical analysis of samples within a sealed-cell containing barium fluoride is a critical need when identifying toxic agents or suspicious powders of unidentified composition. The dispersive nature of barium fluoride is well understood and experimental conditions can be easily adjusted during reflection–absorption measurements to account for differences in focus between the visible and IR regions of the spectrum. In most instances, the ability to collect a viable spectrum is possible when using the sealed cell regardless of whether visible or IR focus is optimized. However, when IR focus is optimized, it is possible to collect useful data from even smaller samples. This is important when a minimal sample is available for analysis or the desire to minimize risk of sample exposure is important. While the use of barium fluoride introduces dispersion effects that are unavoidable, it is possible to adjust instrument settings when collecting IR spectra in the reflection–absorption mode to compensate for dispersion and minimize impact on the quality of the sample spectrum

    The Potential Interference of Body Products and Substrates to the Identification of Ignitable Liquid Residues on Worn Clothing

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    The question of whether deposits on clothing as well as their chemical composition are being mistaken for ignitable fluids is a concern for forensic analysts. Body products and oil secretions can have similar chemical profiles to ignitable liquid residues (ILRs) as a result of comparable chemical compounds that may be found in both sources. This study investigated whether substrates of unworn and worn clothing, with endogenous body secretions and body products could interfere with ILR analysis. Sample extraction was completed by passive headspace concentration with activated charcoal strips (ACS) and desorption with carbon disulfide followed by analysis with gas chromatography-mass spectrometry (GC–MS). Results showed that some body products produce similar patterns to heavy petroleum distillates and most clothing contained components that are commonly found in ignitable liquids. It was concluded that the clothing, body products and compounds released by the body all contribute to the GC–MS profile of worn clothing. These components can mimic or mask the presence of ILRs, however educated and experienced analysts would likely be able to differentiate these substrate patterns from ILRs

    Is Forensic Science in Danger of Extinction?

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    Observations of modern day forensic science has prompted asking the question of whether this field is in danger of extinction. Although there have undoubtedly been meaningful advancements in analytical capabilities, we have overlooked several unintended practical and philosophical consequences. This article addresses three main areas of concern: the declining role of the generalist in an era of increased specialization, the role of education in preparing the next generation of forensic scientists, and the implementation of advanced instrumentation with a focus on statistical significance and field deployable instrumentation

    Morphologically-directed Raman Spectroscopy for Forensic Soil Analysis

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    Morphologically-directed Raman spectroscopy (MDRS) is a novel yet reliable analytical technique that can be used for a variety of forensic applications, enabling scientists to gain more information from samples than they obtain using more traditional methods. In soil forensics, MDRS delivers particle size distribution and microscopic morphological characteristics for the particles present, and at the same time allows secure mineral identification. In this article, we explore the benefits of utilizing soil in forensic investigations, and demonstrate the value of applying MDRS. Two case studies illustrate the real-life potential and applications of this technology

    Morphologically Directed Raman Spectroscopic Analysis of Forensic Samples

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    Morphologically directed Raman spectroscopy (MDRS) is a novel and reliable tool that would enable criminalists to obtain more discriminatory information from forensic samples than their current capabilities. MDRS combines automated particle imaging and Raman spectroscopy into one instrument. Particle imaging is performed to determine particle size and shape distributions of components in a blended sample. Particle size is an important physical property of particulate samples and can be used in conjunction with Raman spectroscopy in the analysis of a range of samples of forensic interest, including illicit and counterfeit drugs, soils, gunshot residue (GSR), and white powders. Although measurement of particle size distributions is routinely carried out across a wide range of industries and is often a critical parameter in the manufacture and analysis of many products and substances, it is not widely used in the forensic sciences. Raman spectroscopy is used in forensic science to determine the molecular chemistry of materials because it is rapid, reliable, allows for analysis without contacting the sample, is nondestructive, and enables detection at low concentrations. Combining these two analytical techniques into a single platform allows the individual components present within a blend or mixture to be independently characterized and compared
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