3,833 research outputs found

    (Methanol-κO){1-[2-(piperazin-4-ium-1-yl-κN 1)ethyl­imino­methyl-κN]naphthalen-2-olato-κO}bis­(thio­cyanato-κN)nickel(II) methanol monosolvate

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    In the title solvated complex, [Ni(C17H21N3O)(NCS)2(CH3OH)]·CH3OH, the Ni2+ ion is coordinated by one phenolate O, one imine N, and one amine N atom of the tridentate Schiff base ligand, two thio­cyanate N atoms and one methanol O atom, resulting in a distorted cis-NiO2N4 octa­hedral geometry. The chelate ring formed by the phenolate O and imine N atoms approximates to an envelope with the Ni atom as the flap, whereas the chelate ring formed by the two N atoms is twisted about the C—C bond. In the crystal, the components are linked by O—H⋯O, N—H⋯O, N—H⋯S, and O—H⋯S hydrogen bonds

    Ferromagnetic and insulating behavior in both half magnetic levitation and non-levitation LK-99 like samples

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    Finding materials exhibiting superconductivity at room temperature has long been one of the ultimate goals in physics and material science. Recently, room-temperature superconducting properties have been claimed in a copper substituted lead phosphate apatite (Pb10−x_{10-x}Cux_x(PO4_4)6_6O, or called LK-99) [1-3]. Using a similar approach, we have prepared LK-99 like samples and confirmed the half-levitation behaviors in some small specimens under the influence of a magnet at room temperature. To examine the magnetic properties of our samples, we have performed systematic magnetization measurements on the as-grown LK-99-like samples, including the half-levitated and non-levitated samples. The magnetization measurements show the coexistence of soft-ferromagnetic and diamagnetic signals in both half-levitated and non-levitated samples. The electrical transport measurements on the as-grown LK-99-like samples including both half-levitated and non-levitated samples show an insulating behavior characterized by the increasing resistivity with the decreasing temperature

    Hot deformation behavior of the fine-grain W-25Cu alloy

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    Practical formula to calculate tension of vertical cable with hinged-fixed conditions based on vibration method

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    Vertical cables are widely used in the tied-arch bridges and suspension bridges as the vital components to transfer load. It is very important to accurately estimate the cable tensions in the cable supported bridges during both construction and in-service stages. Vibration method is the most widely used method for in-situ measurement of cable tensions. But for the cables with hinged-fixed boundary conditions, no analytical formulas can be used to describe the relationship between the frequencies and the cable tension. According to the general solution of the vibration equation and based on its numerical computational results, practical formula to calculate tensions of vertical cables by multiple natural frequencies satisfying hinged-fixed boundary conditions is proposed in this paper. The expression of the practical formula is the same as the solution derived from an axially loaded beam with simple supported ends and can use the first 10 order frequencies to calculate the cable tension conveniently and accurately. Error analysis showed that when using the fundamental frequency to estimate cable force, the estimated tension errors of the cables with its dimensionless parameter ξ≥ 2.8 are less than 2 %. It contained nearly all of the vertical cables used in bridge engineering. In addition, with multiple natural frequencies being measured, bending stiffness of the cable can be identified by using the formulas presented in this paper with an iterative method. At last, the practical formula in this paper is verified to have high precision with several numerical examples, and can be conveniently applied to field test for cable-supported bridges

    The Implementation of a Vulnerability Topology Analysis Method for ICS

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    Nowadays Industrial Control System (ICS) is becoming more and more important in significant fields. However, the using of the general facilities in these systems makes lots of security issues exposed. Because there are a number of differences between the original IT systems and ICSs. At the same time, the traditional vulnerability scan technology lacks the ability to recognize the interactions between vulnerabilities in the network. ICSs are always in a high risk state. So, this paper focuses on the vertex polymerization of the topological vulnerability analysis. We realized a topological analysis method oriented ICSs on the basis of achievements at home and abroad. The result shows that this method can solve the problem of the complex fragility correlation among industrial control networks

    Measurement-induced disturbance and thermal negativity of qutrit-qubit mixed spin chain

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    We investigate the quantum correlation in a qutrit-qubit mixed spin chain based on measurement-induced disturbance (MID) [S. Luo, Phys. Rev. A, 77, (2008) 022301]. We also compare MID and thermal entanglement measured by negativity and illustrate their different characteristics.Comment: 1 text and 3 eps figures;accepted by solid state communication

    Buyang Huanwu Decoction for Healthcare: Evidence-Based Theoretical Interpretations of Treating Different Diseases with the Same Method and Target of Vascularity

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    Buyang Huanwu Decoction (BHD) is a famous herbal prescription that has been used to treat stroke for centuries. Recent studies reported that the use of BHD had been extended to treat various kinds of disorders according to the TCM syndrome theory of Treating Different Diseases with the Same Method (TDDSM). Here, an overview of systematic reviews (SRs) of BHD for healthcare was conducted to interpret the TCM theory of TDDSM and its target of vascularity in an evidence-based manner. Literature searches were carried out in 5 databases to search SRs of BHD for any indication up to August 2013. Thirteen eligible SRs were identified which reported a wide range of vascular conditions. Based on the Overview Quality Assessment Questionnaire scores, the quality of included SRs was varied, with an average score of 4 points. We found that there is premature evidence for the use of BHD for healthcare, whereas BHD was well tolerable in all patients. BHD can be used to treat many disorders with the same therapeutic principle of invigorating Qi to activate blood circulation, which is essentially a manifestation of the TDDSM and is likely to account for targeting the specific pathogenesis of vascular diseases
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