29 research outputs found

    Twist glass transition in regioregulated poly(3-alkylthiophenes)s

    Full text link
    The molecular structure and dynamics of regioregulated poly(3-butylthiophene) (P3BT), poly(3-hexylthiophene)(P3HT), and poly(3-dodecylthiophene) (P3DDT) were investigated using Fourier transform infrared absorption (FTIR), solid state 13^{13}C nuclear magnetic resonance (NMR), and differential scanning calorimetry (DSC) measurements. In the DSC measurements, the endothermic peak was obtained around 340 K in P3BT, and assigned to enthalpy relaxation that originated from the glass transition of the thiophene ring twist in crystalline phase from results of FTIR, 13^{13}C cross-polarization and magic-angle spinning (CPMAS) NMR, 13^{13}C spin-lattice relaxation time measurements, and centerband-only detection of exchange (CODEX) measurements. We defined this transition as {\it twist-glass transition}, which is analogous to the plastic crystal - glassy crystal transition.Comment: 9 pages, 10 figures, 2 tables. Phys.Rev.B, in pres

    First results of material charging in the space environment

    Get PDF
    A satellite experiment, designed to measure potential charging of typical thermal control materials at near geosynchronous altitude, was flown as part of the SCATHA program. Direct observations of charging of typical satellite materials in a natural charging event ( 5 keV) are presented. The results show some features which differ significantly from previous laboratory simulations of the environment

    Ueber das Photographiren auf trocknen Collodiumplatten.

    No full text
    n/

    Zur Erzeugung von Jodidbeschlägen

    No full text

    Solarthermie 2000. Teilprogramm 2: Musterstatiken fuer tragende Aufstellkonstruktionen von thermischen Solaranlagen auf Flachdaechern Abschlussbericht

    No full text
    The target of the project is, to lower the costs of the basic constructions and the costs of the static calculation. These costs categories develop when setting up collectors on flat roofs. Cost-optimized solutions are presented beginning with the attachment detail up to the carrying construction. A economical implementation enables. A substantial point of the project is the examination of the load assumptions, particularly the wind load. Result is a modular system, which gives a selection of attachment details depending upon available roof structure and a combination of different carrying constructions co-ordinated with most frequently occurring collector types enables. (orig.)Das Ziel des Projektes ist, sowohl die Kosten fuer die Unterkonstruktion als auch die Kosten fuer die statische Berechnung, die fuer eine Aufstaenderung von Kollektoren auf flachen Daechern notwendig sind, zu senken. Dazu werden kostenoptimierte Loesungen fuer Aufstaenderungssysteme vom Befestigungsdetail bis zur Tragkonstruktion vorgestellt, die eine kostenguenstige Realisierung ermoeglichen. Ein wesentlicher Bestandteil des Vorhabens ist die Ueberpruefung der Lastannahmen insbesondere der Windlast. Resultat ist ein modulares System, das, je nach vorliegender Dachkonstruktion, eine Auswahl von Befestigungsdetails vorgibt und eine Kombination verschiedener Tragkonstruktionen mit den gebraeuchlichsten Kollektortypen und -feldgroessen ermoeglicht. (orig.)Published in 2 separate volumesSIGLEAvailable from TIB Hannover: F01B1766(1): F01B1766(2) / FIZ - Fachinformationszzentrum Karlsruhe / TIB - Technische InformationsbibliothekBundesministerium fuer Bildung und Forschung, Berlin (Germany)DEGerman

    CEPPAD

    No full text
    The CEPPAD Experiment consists of four sensors for investigating energetic particle phenomena on the POLAR mission. These sensors provide 3-D proton and electron angular distributions in the energy range of 20 keV to 1 MeV, energetic proton and electron measurements extending to energies greater than 10 MEV, high angular and time resolution measurements in the loss-cone, and data on energetic neutral particles. All sensors operate in conjunction with special on-board data processing units which control sensor data acquisition modes while performing in-flight data processing, data compression, and telemetry formatting. Presented here is a CEPPAD system overview together with descriptions of the individual sensors, the in-flight data processing, and examples of sensor calibration data
    corecore