66 research outputs found
Asymptotic equivalence of discretely observed diffusion processes and their Euler scheme: small variance case
This paper establishes the global asymptotic equivalence, in the sense of the
Le Cam -distance, between scalar diffusion models with unknown drift
function and small variance on the one side, and nonparametric autoregressive
models on the other side. The time horizon is kept fixed and both the cases
of discrete and continuous observation of the path are treated. We allow non
constant diffusion coefficient, bounded but possibly tending to zero. The
asymptotic equivalences are established by constructing explicit equivalence
mappings.Comment: 21 page
Microstructured catalytic hollow fiber reactor for methane steam reforming
Microstructured alumina hollow fibers, which contain a plurality of radial microchannels with significant openings on the inner surface, have been fabricated in this study and used to develop an efficient catalytic hollow fiber reactor. Apart from low mass-transfer resistance, a unique structure of this type facilitates the incorporation of Ni-based catalysts, which can be with or without the aged secondary support, SBA-15. In contrast to a fixed bed reactor, the catalytic hollow fiber reactor shows similar methane conversion, with a gas hourly space velocity that is approximately 6.5 times higher, a significantly greater CO2 selectivity, and better productivity rates. These results demonstrate the advantages of dispersing the catalyst inside the microstructured hollow fiber as well as the potential to reduce the required quantity of catalyst
Fluidic bus system for chemical process engineering in the laboratory and for small-scale production
Within the framework of a BMBF-funded project, five research institutes are developing a standardized system for the combination of microstructured devices and laboratory equipment of various suppliers thus leading to the building of chemical plants. The concept is based upon the bus system and simultaneously handles a number of tasks such as mechanical stability, fluidic flow and signal transmission. A key feature of the backbone interface developed is its open architecture. It does not rely on standardized connections thus allowing the combination of devices from various suppliers. The interface shows robustness, withstands high pressures and temperatures while thermal cross-talk is minimized through the use of different materials. Its application in chemical synthesis has shown truly promising results
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