66 research outputs found

    Asymptotic equivalence of discretely observed diffusion processes and their Euler scheme: small variance case

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    This paper establishes the global asymptotic equivalence, in the sense of the Le Cam Δ\Delta-distance, between scalar diffusion models with unknown drift function and small variance on the one side, and nonparametric autoregressive models on the other side. The time horizon TT is kept fixed and both the cases of discrete and continuous observation of the path are treated. We allow non constant diffusion coefficient, bounded but possibly tending to zero. The asymptotic equivalences are established by constructing explicit equivalence mappings.Comment: 21 page

    Microstructured catalytic hollow fiber reactor for methane steam reforming

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    Microstructured alumina hollow fibers, which contain a plurality of radial microchannels with significant openings on the inner surface, have been fabricated in this study and used to develop an efficient catalytic hollow fiber reactor. Apart from low mass-transfer resistance, a unique structure of this type facilitates the incorporation of Ni-based catalysts, which can be with or without the aged secondary support, SBA-15. In contrast to a fixed bed reactor, the catalytic hollow fiber reactor shows similar methane conversion, with a gas hourly space velocity that is approximately 6.5 times higher, a significantly greater CO2 selectivity, and better productivity rates. These results demonstrate the advantages of dispersing the catalyst inside the microstructured hollow fiber as well as the potential to reduce the required quantity of catalyst

    Fluidic bus system for chemical process engineering in the laboratory and for small-scale production

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    Within the framework of a BMBF-funded project, five research institutes are developing a standardized system for the combination of microstructured devices and laboratory equipment of various suppliers thus leading to the building of chemical plants. The concept is based upon the bus system and simultaneously handles a number of tasks such as mechanical stability, fluidic flow and signal transmission. A key feature of the backbone interface developed is its open architecture. It does not rely on standardized connections thus allowing the combination of devices from various suppliers. The interface shows robustness, withstands high pressures and temperatures while thermal cross-talk is minimized through the use of different materials. Its application in chemical synthesis has shown truly promising results
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