186 research outputs found
Development of mercuric iodide uncooled x ray detectors and spectrometers
The results obtained in the development of miniature, lowpower, light weight mercuric iodide, HgI2, x ray spectrometers for future space missions are summarized. It was demonstrated that HgI2 detectors can be employed in a high resolution x ray spectrometer, operating in a scanning electron microscope. Also, the development of HgI2 x ray detectors to augment alpha backscattering spectrometers is discussed. These combination instruments allow for the identification of all chemical elements, with the possible exception of hydrogen, and their respective concentrations. Additionally, further investigations of questions regarding radiation damage effects in the HgI2 x ray detectors are reported
Double-Layer Silicon PIN Photodiode X-Ray Detector for a Future X-ray Timing Mission
A double-layer silicon detector consisting of two 500micron-thick silicon PIN
photodiodes with independent readouts was mounted in a vacuum chamber and
tested with X-ray sources. The detector is sensitive from 1-30 keV with an
effective area of 6 mm^2. The detector performs best at -35 C with an energy
resolution of 220 eV (FWHM, full width at half maximum) at 5.9 keV, and is able
to operate at room temperature, +25 C, with moderate resolution around 760 eV
(FWHM). The response of the top layer sensor is highly uniform across the
sensitive area. This large-format silicon detector is appropriate for future
X-ray timing missions.Comment: 10 pages, 5 figures, NIM A to appea
Mercuric Iodide Anticoincidence Shield for Gamma-Ray Spectrometer
A film-growth process was developed for polycrystalline mercuric iodide that creates cost-effective, large-area detectors for high-energy charged-particle detection. A material, called a barrier film, is introduced onto the substrate before the normal mercuric iodide film growth process. The barrier film improves the quality of the normal film grown and enhances the adhesion between the film and the substrate. The films grown using this improved technique were found to have adequate signal-to-noise properties so that individual high-energy charged -particle interactions could be distinguished from noise, and thus, could be used to provide an anticoincidence veto function as desired
New concepts for HgI2 scintillator gamma ray spectroscopy
The primary goals of this project are development of the technology for HgI2 photodetectors (PD's), development of a HgI2/scintillator gamma detector, development of electronics, and development of a prototype gamma spectrometer. Work on the HgI2 PD's involved HgI2 purification and crystal growth, detector surface and electrical contact studies, PD structure optimization, encapsulation and packaging, and testing. Work on the HgI2/scintillator gamma detector involved a study of the optical - mechanical coupling for the optimization of CsI(Tl)/HgI2 gamma ray detectors and determination of the relationship between resolution versus scintillator type and size. The development of the electronics focused on low noise amplification circuits using different preamp input FET's and the use of a coincidence technique to maximize the signal, minimize the noise contribution in the gamma spectra, and improve the overall system resolution
Miniaturization in x ray and gamma ray spectroscopy
The paper presents advances in two new sensor technologies and a miniaturized associated electronics technology which, when combined, can allow for very significant miniaturization and for the reduction of weight and power consumption in x-ray and gamma-ray spectroscopy systems: (1) Mercuric iodide (HgI2) x-ray technology, which allows for the first time the construction of truly portable, high-energy resolution, non-cryogenic x-ray fluorescence (XRF) elemental analyzer systems, with parameters approaching those of laboratory quality cryogenic instruments; (2) the silicon avalanche photodiode (APD), which is a solid-state light sensitive device with internal amplification, capable of uniquely replacing the vacuum photomultiplier tube in scintillation gamma-ray spectrometer applications, and offering substantial improvements in size, ruggedness, low power operation and energy resolution; and (3) miniaturized (hybridized) low noise, low power amplification and processing electronics, which take full advantage of the favorable properties of these new sensors and allow for the design and fabrication of advanced, highly miniaturized x-ray and gamma-ray spectroscopy systems. The paper also presents experimental results and examples of spectrometric systems currently under construction. The directions for future developments are discussed
Performance and durability of HgI_2 X-ray detectors for space missions
Considerable progress has been achieved in HgI_2 detector fabrication technology and amplification electronics. An energy resolution of 198 eV (full width at half maximum) has been obtained for the Mn K_α line of 5.9 keV in a practical X-ray probe without the use of cryogenic cooling. Detectors prepared with Parylene-C encapsulation have demonstrated perfect reliability in two-year tests under high vacuum and temperature and bias cycling. Other HgI_2 detectors have been used to demonstrate proton-radiation-damage resistance to levels of 10^(12) protons/cm^2 at 10.7 MeV. It is concluded that HgI_2 detectors are suitable for the ordinary requirements of energy dispersive detectors in X-ray spectroscopy systems
Advances in the development of encapsulants for mercuric iodide X-ray detectors
Advances in the development of protective impermeable encapsulants with high transparency to ultra-low-energy X-rays for use on HgI_2 X-ray detectors are reported. Various X-ray fluorescence spectra from coated detectors are presented. The X-ray absorption in the encapsulants has been analyzed using characteristic radiation from various elements. Results suggest that low-energy cutoffs for the detectors are not determined solely by the encapsulating coatings presently employed but are also influenced by the front electrode and surface effects, which can affect the local electric field or the surface recombination velocity. An energy resolution of 182 eV (FWHM) has been achieved for Ni L lines at 850 eV. Improved detector sensitivity to X-ray energies under 700 eV is demonstrated
Low Energy X-Ray Spectra Measured with a Mercuric Iodide Energy Dispersive Spectrometer in a Scanning Electron Microscope
A mercuric iodide energy dispersive x-ray
spectrometer, with Peltier cooling provided for the
detector and input field effect transistor, has been
developed and tested in a scanning electron microscope.
X-ray spectra were obtained with the 15 keV electron
beam. An energy resolution of 225 eV (FWHM) for Mn-Kα
at 5.9 keV and 195 eV (FWHM) for Mg-K line at 1.25 keV
has been measured. Overall system noise level was 175
eV (FWHM). The detector system characterization with a
carbon target demonstrated good energy sensitivity at
low energies and lack of significant spectral artifacts
at higher energies
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APPROACHING CRYOGENIC GE PERFORMANCE WITH PELTIER COOLED CDTE
A new class of hand-held, portable spectrometers based on large area (lcm2) CdTe detectors of thickness up to 3mm has been demonstrated to produce energy resolution of between 0.3 and 0.5% FWHM at 662 keV. The system uses a charge loss correction circuit for improved efficiency, and detector temperature stabilization to ensure consistent operation of the detector during field measurements over a wide range of ambient temperature. The system can operate continuously for up to 8hrs on rechargeable batteries. The signal output from the charge loss corrector is compatible with most analog and digital spectroscopy amplifiers and multi channel analyzers. Using a detector measuring 11.2 by 9.1 by 2.13 mm3, we have recently been able to obtain the first wide-range plutonium gamma-ray isotopic analysis with other than a cryogenically cooled germanium spectrometer. The CdTe spectrometer is capable of measuring small plutonium reference samples in about one hour, covering the range from low to high burnup. The isotopic analysis software used to obtain these results was FRAM, Version 4 from LANL. The new spectrometer is expected to be useful for low-grade assay, as well as for some in-situ plutonium gamma-ray isotopics in lieu of cryogenically cooled Ge
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Large area silicon drift detectors for x-rays -- New results
Large area silicon drift detectors, consisting of 8 mm and 12 mm diameter hexagons, were fabricated on 0.35 mm thick high resistivity n-type silicon. An external FET and a low-noise charge sensitive preamplifier were used for testing the prototype detectors. The detector performance was measured in the range 75 to 25 C using Peltier cooling, and from 0.125 to 6 {micro}s amplifier shaping time. Measured energy resolutions were 159 eV FWHM and 263 eV FWHM for the 0.5 cm{sup 2} and 1 cm{sup 2} detectors, respectively (at 5.9 keV, {minus}75 C, 6 {micro}s shaping time). The uniformity of the detector response over the entire active area (measured using 560 nm light) was < 0.5%
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