8,447 research outputs found

    The Monumental Cemeteries of Northern Pictland

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    Peer reviewedPublisher PD

    A fluorometric method for the estimation of tryptophan

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    The various colorimetric methods now employed for the estimation of tryptophan are not specific for tryptophan but give colored products with many compounds containing the indole nucleus, including indole itself. In order to facilitate studies of the enzymatic synthesis of tryptophan from indole and serine by extracts of Neurospora (1), a search for a rapid, quantitative method for the estimation of tryptophan in the presence of indole was undertaken. Tauber (2) reported that tryptophan gives a green fluorescence when treated with 70 to 72 per cent perchloric acid at room temperature. Modification of this procedure has led to a method for the rapid estimation of tryptophan, without preliminary extraction of indole, in hydrolyzed or unhydrolyzed tryptophan-containing materials

    Tight-fill fruit packing /

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    C54

    Goal-setting And Achievement In Activity Tracking Apps: A Case Study Of MyFitnessPal

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    Activity tracking apps often make use of goals as one of their core motivational tools. There are two critical components to this tool: setting a goal, and subsequently achieving that goal. Despite its crucial role in how a number of prominent self-tracking apps function, there has been relatively little investigation of the goal-setting and achievement aspects of self-tracking apps. Here we explore this issue, investigating a particular goal setting and achievement process that is extensive, recorded, and crucial for both the app and its users' success: weight loss goals in MyFitnessPal. We present a large-scale study of 1.4 million users and weight loss goals, allowing for an unprecedented detailed view of how people set and achieve their goals. We find that, even for difficult long-term goals, behavior within the first 7 days predicts those who ultimately achieve their goals, that is, those who lose at least as much weight as they set out to, and those who do not. For instance, high amounts of early weight loss, which some researchers have classified as unsustainable, leads to higher goal achievement rates. We also show that early food intake, self-monitoring motivation, and attitude towards the goal are important factors. We then show that we can use our findings to predict goal achievement with an accuracy of 79% ROC AUC just 7 days after a goal is set. Finally, we discuss how our findings could inform steps to improve goal achievement in self-tracking apps

    Practical applications of small-angle neutron scattering.

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    Recent improvements in beam-line accessibility and technology have led to small-angle neutron scattering (SANS) becoming more frequently applied to materials problems. SANS has been used to study the assembly, dispersion, alignment and mixing of nanoscale condensed matter, as well as to characterise the internal structure of organic thin films, porous structures and inclusions within steel. Using time-resolved SANS, growth mechanisms in materials systems and soft matter phase transitions can also be explored. This review is intended for newcomers to SANS as well as experts. Therefore, the basic knowledge required for its use is first summarised. After this introduction, various examples are given of the types of soft and hard matter that have been studied by SANS. The information that can be extracted from the data is highlighted, alongside the methods used to obtain it. In addition to presenting the findings, explanations are provided on how the SANS measurements were optimised, such as the use of contrast variation to highlight specific parts of a structure. Emphasis is placed on the use of complementary techniques to improve data quality (e.g. using other scattering methods) and the accuracy of data analysis (e.g. using microscopy to separately determine shape and size). This is done with a view to providing guidance on how best to design and analyse future SANS measurements on materials not listed below

    Don\u27t Copy Me, Argentina: Constitutional Borrowing and Rhetorical Type

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    Part I of this Article concerns the relationship between rhetoric and law, outlining the classical distinction between the forensic and deliberative modes of rhetoric. Part II describes the basic vision of Juan Bautista Alberdi, the father of Argentine constitutionalism. Part III discusses how Alberdi’s proposed constitutional ideas, borrowed heavily from the Constitution of the United States, influenced the text of Argentina’s Constitution of 1853. Part IV examines the subsequent debate between Alberdi and his contemporary and associate, Domingo Faustino Sarmiento, to illustrate how their different rhetorical modes resulted in differing interpretations of the Argentine Constitution. Part V offers some thoughts on rhetorical problems inherent in the interpretation of borrowed constitutions. My stance, essentially Hegelian, is that the rhetorical muddles presented by borrowed constitutions are unavoidable, placing on borrowers and their descendants the added obligation to link the borrowed text to a surrounding culture of constitutionalism

    Upholding Longstanding Prohibitions on Firearm Possession Under Bruen

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    The Supreme Court’s decision in New York State Rifle & Pistol Association, Inc. v. Bruen has cast doubt on the constitutionality of federal firearms possession laws, such as the prohibition on felons possessing guns. This piece examines how one federal district court upheld a federal restriction on felon gun possession in the recent wake of the Bruen decision. In this article, Mitchell Gordon especially focuses on the historical facts and analysis that are now required under Bruen in order to uphold a governmental restriction on Second Amendment rights.https://scholarship.law.slu.edu/lawjournalonline/1117/thumbnail.jp

    Aspects of solute movement in the British uplands

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    The aim of this research is to determine the process by which runoff draining parts of the UK uplands becomes discoloured. Recent increases in colour are perceived as a problem due to the frequency with which EC surface water directives are breached, to the increased cost of meeting standards, to an increase in consumer complaints, and due to the possible deleterious health effects of consuming coloured potable water. The work was conducted over the last four years, largely in the Upper Burn and Nidd valleys, north Yorkshire, and at the University of Leeds. Existing knowledge on the chemical nature and environmental genesis of coloured water is reviewed, and related to the chemical nature of coloured waters examined in this study. Analysis of water quality archives and direct monitoring of selected catchments was conducted enabling the spatial and temporal distribution of coloured waters to be determined. A tentative process theory was produced, and tested by controlled laboratory investigations. Coloured runoff is derived from Winter Hill soil, raw acid oligo-fibrous peat, and is most intense from areas with slopes < 5% and high drainage densities. The seasonal pattern of colour is highly regular, and is a product of rainfall and soil moisture deficit. Colour is strongly associated with discharge, and demonstrates the operation of a catchment flushing mechanism. Runoff is discoloured in a three phase process; colour production, solubilisation and removal. Colour is a product of organic decomposition, dependent upon microbiological activity, moisture deficit, temperature and peat structure. Solubilisation of colour is dependent upon solution pH, temperature, the chemical structure of organic molecules and the availability of iron. The removal of decomposition products, as colour, is strongly dependent on the moisture status of peat, and its ability to rewet after drying. The implications of these findings for future colour levels and for catchment and catchwater management are discussed
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