The effects of temperature and strain rate on yielding and springback behaviour of DP1000 dual phase steel

This study aims to investigate the effects of the temperature and strain rate on the yielding and springback behavior of DP1000 advanced high strength steel. For this purpose, material properties were defined using tensile tests at several temperatures (25 °C, 100 °C, 200 °C) and strain rates (0.0083 s -1 , 0.16 s -1 ). Yield loci were estimated by using Barlat-89 yield criteria. Springback behavior is specified by performing V bending tests. No significant effect was observed in the assessment of the effect of temperature on the yield locus and springback. Moreover, it was found that the increase in strain rate increased dramatically the yield locus and springback. © 2018 IOP Publishing Ltd

Strain rate sensitivity and strain hardening response of DP1000 dual phase steel

In this study, strain hardening and strain rate sensitivity behavior of commercial DP1000 dual phase steel have been examined in detail at temperatures of 25 °C, 100 °C, 200 °C and 300 °C, at strain rates of 0.0016 s -1 and 0.16 s -1 . As the strain rate has increased, the yield strength has increased but no significant change in tensile strength and strain hardening coefficient has been observed. As the temperature has increased, the yield and tensile strength has decreased in between 25 and 200 °C but it has showed an increase at 300 °C. The strain hardening coefficient has increased in parallel with temperature increase. It has been seen that the strain rate sensitivity has not been affected by temperature. No significant difference in the hardening rate has appeared in between 25 and 200 °C, but the highest value has been calculated at 300 °C. It has been determined that the fracture behavior has occurred earlier and load carrying capacity on necking has reduced with the increase of strain rate and not significantly affected by temperature. © 2018 EDP Sciences

Antibiotic and heavy metal resistant bacteria isolated from aegean sea water and sediment in Güllük Bay, Turkey Quantifying the resistance of identified bacteria species with potential for environmental remediation applications

Heavy metal and antibiotic-resistant bacteria have potential for environmental bioremediation applications. Resistant bacteria were investigated in sediment and seawater samples taken from the Aegean Sea, Turkey, between 2011 and 2013. Bioindicator bacteria in seawater samples were tested using the membrane filtration technique. The spread plate technique and VITEK® 2 Compact 30 micro identification system were used for heterotrophic aerobic bacteria in the samples. The minimum inhibition concentration method was used for heavy metal-resistant bacteria. Antibiotic-resistant bacteria were tested using the disk diffusion method. All bacteria isolated from sediment samples showed 100% resistance to rifampicin, sulfonamide, tetracycline and ampicillin. 98% of isolates were resistant against nitrofurantoin and oxytetracycline. Higher antibiotic and heavy metal resistance was recorded in bacteria isolated from sediment than seawater samples. The highest levels of bacterial metal resistance were recorded against copper (58.3%), zinc (33.8%), lead (32.1%), chromium (31%) and iron (25.2%). The results show that antibiotic and heavy metal resistance in bacteria from sediment and seawater can be observed as responses to environmental influences including pollution in marine areas. © 2020 Johnson Matthey.Türkiye Bilimsel ve Teknolojik Araştirma Kurumu: 110Y243 İÜ BAP Project/19347 Türkiye Bilimsel ve Teknolojik Araştirma KurumuThe authors wish to thank the Scientific and Technical Research Council of Turkey (TÜBITAK, project number: 110Y243, 2011) and Istanbul University Scientific Research Project Unit (İÜ BAP Project/19347) for their financial support

An annular CMUT array beamforming system for high-frequency side looking IVUS imaging

A CMUT annular array system for Side-Looking Intravascular Ultrasound (SL-IVUS) with fixed transmit and dynamic receive focusing capabilities has been developed. The system was experimentally characterized and validated through analytical models that simulate the beamformed transducer behavior. An 840 m diameter, 35MHz array was fabricated, characterized, and used in experiments. The array consists of curved 18m by 60m CMUT membranes that form 8 ring transducer elements with approximately equal areas. The beamforming system uses an IC chip consisting of 8 transimpedance amplifiers and delay elements for receive beamforming with adjustable delays between 2ns and 4ns, that are constant up to 50 MHz with close to unity gain. Transmit focusing is implemented with an FPGA controlled, high voltage pulser board that can generate adjustable electrical pulses with delays as small as 2ns. The system is characterized by measuring the radiation patterns of individual CMUT annular array elements as well as the unfocused and fixed transmit focused arrays. The results show predicted behavior including acoustic crosstalk effects at certain frequencies. For transmit-receive beamforming characterization, a 25m gold wire was imaged using 4 beamformed transmit elements and 4 beamformed receive elements with different delay values. The results show improved lateral resolution and lower side lobes with proper beamforming.Publisher's Versio

Evaluation of CMUT annular arrays for side-looking IVUS

Side-looking (SL) IVUS probes are extensively used for management of cardiovascular diseases. Currently SL-IVUS imaging probes use either a single rotating transducer element or solid-state arrays. Probes with single rotating piezoelectric transducer have simple front-end, but have fixed focused operation, and suffers from motion artifacts. Solid-state SL-IVUS imaging probes use piezoelectric transducer arrays and electronic beam-forming. Synthetic phased array processing of signals detected with small-sized elements in these arrays limits the SNR achievable with these probes. In this study, we explore a new SL-IVUS probe architecture employing rotating phased annular CMUT arrays. We tested and compared imaging performance of the existing and proposed probe configurations through simulated point spread functions. We also two fabricated sample annular array designs operating at 20-MHz and 50-MHz. Our experimental measurements on the 20-MHz array in oil shows 105% fractional bandwidth. The 50-MHz array with parylene coating shows approximately 40% fractional bandwidth measured in water. We also present imaging results acquired from wire-targets to test the experimental point-spread functions.IEEE Ultrasonics, Ferroelectrics, and Frequency Control SocietyPublisher's Versio

A tunable analog delay element for high-frequency dynamic beamforming

Implementing beamforming for high frequency arrays is challenging because of the accurate delay requirements at high frequencies. High frequency digital beamforming is not suitable for catheter based applications as a large number of cables is required between the array and the external beamformer. A possible solution is to perform analog beamforming on an integrated circuit adjacent or monolithically integrated to the imaging array. In this study, we introduce an improved voltage in voltage out low pass filter as an analog delay cell for high frequency dynamic beamformers. This circuit can generate three times more delay with a given bandwidth when compared to conventional low pass filters. Delay of the circuit is tunable and the gain of the cell is inherently very close to unity. The proposed delay cell operates single ended and therefore is more suitable for CMUT operation which generates single ended output. We designed a test beamformer for a 30MHz, equal area, annular array with 100% bandwidth using the proposed delay cell and the unit-delay focusing architecture. Required delays are implemented using a delay line made up of improved delay elements with tunable delays. To demonstrate functionality we designed and fabricated a custom front-end IC in a 0.5µm standard CMOS process. The IC chip consists of 8 transimpedance amplifiers, voltage-to-current converters, the analog dynamic beamformer, and two buffers. We present results of preliminary imaging experiments that demonstrate the focusing capability

Monolithic CMUT-on-CMOS integration for intravascular ultrasound applications

PubMed ID: 23443701work was supported by the National Institutes of Health under the grants HL082811 and EB010070One of the most important promises of capacitive micromachined ultrasonic transducer (CMUT) technology is integration with electronics. This approach is required to minimize the parasitic capacitances in the receive mode, especially in catheter-based volumetric imaging arrays, for which the elements must be small. Furthermore, optimization of the available silicon area and minimized number of connections occurs when the CMUTs are fabricated directly above the associated electronics. Here, we describe successful fabrication and performance evaluation of CMUT arrays for intravascular imaging on custom-designed CMOS receiver electronics from a commercial IC foundry. The CMUT-on-CMOS process starts with surface isolation and mechanical planarization of the CMOS electronics to reduce topography. The rest of the CMUT fabrication is achieved by modifying a low-temperature micromachining process through the addition of a single mask and developing a dry etching step to produce sloped sidewalls for simple and reliable CMUT-to-CMOS interconnection. This CMUT-to-CMOS interconnect method reduced the parasitic capacitance by a factor of 200 when compared with a standard wire-bonding method. Characterization experiments indicate that the CMUT-on-CMOS elements are uniform in frequency response and are similar to CMUTs simultaneously fabricated on standard silicon wafers without electronics integration. Experiments on a 1.6-mm-diameter dual-ring CMUT array with a center frequency of 15 MHz show that both the CMUTs and the integrated CMOS electronics are fully functional. The SNR measurements indicate that the performance is adequate for imaging chronic total occlusions located 1 cm from the CMUT array.Publisher's Versio

CMUT-based volumetric ultrasonic imaging array design for forward looking ICE and IVUS applications

Designing a mechanically flexible catheter based volumetric ultrasonic imaging device for intravascular and intracardiac imaging is challenging due to small transducer area and limited number of cables. With a few parallel channels, synthetic phased array processing is necessary to acquire data from a large number of transducer elements. This increases the data collection time and hence reduces frame rate and causes artifacts due to tissue-transducer motion. Some of these drawbacks can be resolved by different array designs offered by CMUT-on-CMOS approach. We recently implemented a 2.1-mm diameter single chip 10 MHz dual ring CMUT-on-CMOS array for forward looking ICE with 64-transmit and 56-receive elements along with associated electronics. These volumetric arrays have the small element size required by high operating frequencies and achieve sub mm resolution, but the system would be susceptible to motion artifacts. To enable real time imaging with high SNR, we designed novel arrays consisting of multiple defocused annular rings for transmit aperture and a single ring receive array. The annular transmit rings are utilized to act as a high power element by focusing to a virtual ring shaped line behind the aperture. In this case, image reconstruction is performed by only receive beamforming, reducing total required firing steps from 896 to 14 with a trade-off in image resolution. The SNR of system is improved more than 5 dB for the same frequency and frame rate as compared to the dual ring array, which can be utilized to achieve the same resolution by increasing the operating frequency.Publisher's Versio

Front-end CMOS electronics for monolithic integration with CMUT arrays: Circuit design and initial experimental results

This paper discusses design of CMOS-ASICs for monolithic integration of CMUT arrays by post-CMOS fabrication. We describe design strategies for monolithic integration and demonstrate the advantages of CMUT-on-CMOS approach. On the same wafer, separate sets of IC cells are designed to interface different types of CMUT arrays for IVUS and ICE applications. Circuit topologies include resistive feedback transimpedance amplifiers on the receiver side, along with multiplexers and buffers. Gains and bandwidths of receiving amplifiers are optimized separately to fit different array specifications such as number of elements, element size and operation bandwidth. To drive CMUTs a high voltage pulser array is designed in the same 3.3V unmodified CMOS technology by combining existing technological layers in an unconventional way. CMUT arrays are then built on top of the custom made 8" wafer containing these circuits fabricated in a 0.35µm standard CMOS process. We present initial characterization of the CMO electronics and pulse-echo measurements obtained post-CMOS fabricated CMUT elements.Publisher's Versio

Forward-looking IVUS imaging using a dual-annular ring CMUT array: Experimental results

This paper presents the experimental results on forward-looking Intravascular ultrasound (FL-IVUS) using dual-annular-ring CMUT arrays. The array has a diameter of 1mm including bondpads which consists of separate, concentric 24 transmit and 32 receive ring arrays built on the same silicon substrate. This configuration has the potential for Independent optimization of each array and uses the silicon area more effectively without any drawback. For imaging experiments, we designed and constructed a custom integrated circuit using a standard 0.5 mu m CMOS process for data acquisition. A sample pulse-echo signal received from the oil-air Interface (plane reflector) at 6mm had a center frequency of 11MHz with 95% fractional 6-dB bandwidth. The measured SNR of the echo was 24 dB with no averaging. B-scan image of a wire-phantom was generated to test the resolution.Publisher's Versio