3,069 research outputs found

    Dense and accurate motion and strain estimation in high resolution speckle images using an image-adaptive approach

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    Digital image processing methods represent a viable and well acknowledged alternative to strain gauges and interferometric techniques for determining full-field displacements and strains in materials under stress. This paper presents an image adaptive technique for dense motion and strain estimation using high-resolution speckle images that show the analyzed material in its original and deformed states. The algorithm starts by dividing the speckle image showing the original state into irregular cells taking into consideration both spatial and gradient image information present. Subsequently the Newton-Raphson digital image correlation technique is applied to calculate the corresponding motion for each cell. Adaptive spatial regularization in the form of the Geman-McClure robust spatial estimator is employed to increase the spatial consistency of the motion components of a cell with respect to the components of neighbouring cells. To obtain the final strain information, local least-squares fitting using a linear displacement model is performed on the horizontal and vertical displacement fields. To evaluate the presented image partitioning and strain estimation techniques two numerical and two real experiments are employed. The numerical experiments simulate the deformation of a specimen with constant strain across the surface as well as small rigid-body rotations present while real experiments consist specimens that undergo uniaxial stress. The results indicate very good accuracy of the recovered strains as well as better rotation insensitivity compared to classical techniques

    Large enhancement of the thermopower in Nax_xCoO2_2 at high Na doping

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    Research on the oxide perovskites has uncovered electronic properties that are strikingly enhanced compared with those in conventional metals. Examples are the high critical temperatures of the cuprate superconductors and the colossal magnetoresistance in the manganites. The conducting layered cobaltate NaxCoO2\rm Na_xCoO_2 displays several interesting electronic phases as xx is varied including water-induced superconductivity and an insulating state that is destroyed by field. Initial measurements showed that, in the as-grown composition, NaxCoO2\rm Na_xCoO_2 displays moderately large thermopower SS and conductivity Ļƒ\sigma. However, the prospects for thermoelectric cooling applications faded when the figure of merit ZZ was found to be small at this composition (0.6<x<<x<0.7). Here we report that, in the poorly-explored high-doping region x>x>0.75, SS undergoes an even steeper enhancement. At the critical doping xpāˆ¼x_p\sim 0.85, ZZ (at 80 K) reaches values āˆ¼\sim40 times larger than in the as-grown crystals. We discuss prospects for low-temperature thermoelectric applications.Comment: 6 pages, 7 figure

    Formation and evolution of epitaxial Co5Ge7Co5Ge7 film on Ge (001) surface by solid-state reaction in an in situ ultrahigh-vacuum transmission electron microscope

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    A thin metallic cobalt (Co) layer was deposited on a single-crystal Ge (001) surface at room temperature by the electron-beam evaporation of a pure Co metal source in an ultrahigh-vacuum transmission electron microscope. The formation and epitaxial growth of a cobalt germanide Co5Ge7Co5Ge7 phase on the Ge (001) surface was studied in situ by gradually heating the sample from room temperature to āˆ¼ 350ā€‚Ā°Cāˆ¼350Ā°C. The occurrence of an epitaxial hexagonal-close-packed Co and the reaction between Co and Ge were observed at āˆ¼ 225ā€‚Ā°Cāˆ¼225Ā°C. After annealing at āˆ¼ 300ā€‚Ā°Cāˆ¼300Ā°C for 26.5 h, a continuous epitaxial Co5Ge7Co5Ge7 film formed on the Ge (001) substrate. With further annealing at a higher temperature, the continuous Co5Ge7Co5Ge7 layer broke up and formed three-dimensional islands in order to relieve the strain energy in the epitaxial Co5Ge7Co5Ge7 layer. Two epitaxial relationships between Co5Ge7Co5Ge7 and Ge, i.e., Co5Ge7āŒ©110āŒŖ(001)//GeāŒ©100āŒŖ(001)Co5Ge7āŒ©110āŒŖ(001)āˆ•āˆ•GeāŒ©100āŒŖ(001) and Co5Ge7āŒ©001āŒŖ(110)//GeāŒ©100āŒŖ(001)Co5Ge7āŒ©001āŒŖ(110)āˆ•āˆ•GeāŒ©100āŒŖ(001) were found by electron diffraction.Peer Reviewedhttp://deepblue.lib.umich.edu/bitstream/2027.42/87837/2/211909_1.pd

    Magnetic and Metal-Insulator Transitions in beta-Na0.5CoO2 and gamma-K0.5CoO2 -NMR and Neutron Diffraction Studies-

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    Co-oxides beta-Na0.5CoO2 and gamma-K0.5CoO2 have been prepared by the Na de-intercalation from alpha-NaCoO2 and by the floating-zone method, respectively. It has been found that successive phase transitions take place at temperatures Tc1 and Tc2 in both systems. The appearance of the internal magnetic field at Tc1 with decreasing temperature T indicates that the antiferromagnetic order exists at T < Tc1, as in gamma-Na0.5CoO2. For beta-Na0.5CoO2, the transition temperatures and the NMR parameters determined from the data taken for magnetically ordered state are similar to those of gamma-Na0.5CoO2, indicating that the difference of the stacking ways of the CoO2 layers between these systems do not significantly affect their physical properties. For gamma-K0.5CoO2, the quantitative difference of the physical quantities are found from those of beta- and gamma-Na0.5CoO2. The difference between the values of Tci (i = 1 and 2) of these systems might be explained by considering the distance between CoO2 layers.Comment: 8 pages, 14 figures, 1 Tabl

    Precise Control of Band Filling in NaxCoO2

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    Electronic properties of the sodium cobaltate NaxCoO2 are systematically studied through a precise control of band filling. Resistivity, magnetic susceptibility and specific heat measurements are carried out on a series of high-quality polycrystalline samples prepared at 200 C with Na content in a wide range of 0.35 =< x =< 0.70. It is found that dramatic changes in electronic properties take place at a critical Na concentration x* that lies between 0.58 and 0.59, which separates a Pauli paramagnetic and a Curie-Weiss metals. It is suggested that at x* the Fermi level touches the bottom of the a1g band at the gamma point, leading to a crucial change in the density of states across x* and the emergence of a small electron pocket around the gamma point for x > x*.Comment: 4 pages, 5 figures, submitted to J. Phys. Soc. Jp

    NMR studies of Successive Phase Transitions in Na0.5CoO2 and K0.5CoO2

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    59Co- and 23Na-NMR measurements have been carried out on polycrystalline and c-axis aligned samples of Na0.5CoO2, which exhibits successive transitions at temperatures T = 87 K (= Tc1) and T = 53 K (= Tc2). 59Co-NMR has also been carried out on c-axis aligned crystallites of K0.5CoO2 with similar successive transitions at Tc1 ~ 60 K and Tc2 ~ 20 K. For Na0.5CoO2, two sets of three NMR lines of 23Na nuclei explained by considering the quadrupolar frequencies nuQ ~1.32 and 1.40 MHz have been observed above Tc1, as is expected from the crystalline structure. Rather complicated but characteristic variation of the 23Na-NMR spectra has been observed with varying T through the transition temperatures, and the internal fields at two crystallographically distinct Na sites are discussed on the basis of the magnetic structures reported previously. The internal fields at two distinct Co sites observed below Tc1 and the 591/T1-T curves of Na0.5CoO2 and K0.5CoO2 are also discussed in a comparative way.Comment: 7 pages, 10 figures, submitted to J. Phys. Soc. Jpn, correction is made in right colum of p6 (35th line) as K0.5CoO2-->Na0.5CoO

    Thermal and Electrical Properties of gamma-NaxCoO2 (0.70 < x < 0.78)

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    We have performed specific heat and electric resistivity measurements of Nax_{x}CoO2_{2} (x=0.70x=0.70-0.78). Two anomalies have been observed in the specific heat data for x=0.78x=0.78, corresponding to magnetic transitions at Tc=22T_{c}=22 K and Tkā‰ƒ9T_{k}\simeq 9 K reported previously. In the electrical resistivity, a steep decrease at TcT_{c} and a bending-like variation at TbT_{b}(=120K for x=0.78x=0.78) have been observed. Moreover, we have investigated the xx-dependence of these parameters in detail. The physical properties of this system are very sensitive to xx, and the inconsistent results of previous reports can be explained by a small difference in xx. Furthermore, for a higher xx value, a phase separation into Na-rich and Na-poor domains occurs as we previously proposed, while for a lower xx value, from characteristic behaviors of the specific heat and the electrical resistivity at the low-temperature region, the system is expected to be in the vicinity of the magnetic instability which virtually exists below x=0.70x=0.70.Comment: 4 pages (3 figures included) and an extra figure (gif), to be published in J. Phys. Soc. Jpn. 73 (9) with possible minor revision

    Determination of overlap in lidar systems

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    The overlap profile, also known as crossover function or geometric form factor, is often a source of uncertainty for lidar measurements. This paper describes a method for measuring the overlap by presenting the lidar with a virtual cloud through the use of an imaging system. Results show good agreement with horizontal hard target lidar measurements and with geometric overlap calculated for the ideal aberration-free case

    Association of body mass index, metabolic health status and clinical outcomes in acute myocardial infarction patients: a national registry-based study

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    INTRODUCTION: Obesity is an important risk factor for acute myocardial infarction (AMI), but the interplay between metabolic health and obesity on AMI mortality has been controversial. In this study, we aimed to elucidate the risk of short- and long-term all-cause mortality by obesity and metabolic health in AMI patients using data from a multi-ethnic national AMI registry. METHODS: A total of 73,382 AMI patients from the national Singapore Myocardial Infarction Registry (SMIR) were included. These patients were classified into four groups based on the presence or absence of metabolic diseases, diabetes mellitus, hyperlipidaemia, and hypertension, and obesity: (1) metabolically-healthy-normal-weight (MHN); (2) metabolically-healthy-obese (MHO); (3) metabolically-unhealthy-normal-weight (MUN); and (4) metabolically-unhealthy-obese (MUO). RESULTS: MHO patients had reduced unadjusted risk of all-cause in-hospital, 30-day, 1-year, 2-year, and 5-year mortality following the initial MI event. However, after adjusting for potential confounders, the protective effect from MHO on post-AMI mortality was lost. Furthermore, there was no reduced risk of recurrent MI or stroke within 1-year from onset of AMI by the MHO status. However, the risk of 1-year mortality was higher in female and Malay AMI patients with MHO compared to MHN even after adjusting for confounders. CONCLUSION: In AMI patients with or without metabolic diseases, the presence of obesity did not affect mortality. The exception to this finding were female and Malay MHO who had worse long-term AMI mortality outcomes when compared to MHN suggesting that the presence of obesity in female and Malay patients may confer worsened outcomes
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