348 research outputs found

    Morphology and Properties of Zn-Al-TiO2 Composite on Mild Steel

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    The influence of TiO2 composite and dispersed pure Al particle on zinc alloy electrodeposited on mild steel was studied from chloride bath solution.Microstructural and mechanical properties of the alloy were investigated. The structure, surface morphology, and surface topography of the deposited alloys were characterized by scanning electron microscopy (SEM) and atomic force microscope (AFM).In addition, hardness of the coated alloys was measured. It was found that the obtained Zn-Al-TiO2 alloyexhibited more preferred surface morphology and mechanical strength compared tothe substrate. The result shows the existence of interaction between TiO2 compounds and zinc alloy particulate. It also exhibited well bright dominate zinc coating on steel surface

    Structural and properties of Zn-Al2O3-SiC nano-composite coatings by direct electrolytic process

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    In this paper, Zn-SiC and Zn-Al2O3-SiC composite coating were fabricated by electrodeposition technique from sulfates bath. The resulting composite coating was carried out by adding Al2O3/SiC particulate to a zinc-containing bath. The properties of the composite coating were investigated by SEM equipped with EDS, XRD, and AFM. The electrochemical behavior of the coating alloy was evaluated in 3.65 % NaCl with linear polarization technique and mechanically examined by durascan microhardness tester. The morphology of the thermal treated coatings at 400 °C in 6 h was viewed with high optical microscope (OPM). The results show hardness, thermal stability, and anti-corrosion properties of Zn-Al2O3-SiC were improved significantly as against Zn- SiC coating matrixes. This was attributed to dispersive strengthening effect and grain induced effort of Al2O3/SiC particulate. The decrease in corrosion and thermal stability at 15 g/L of SiC concentration may be as a result of agglomeration and the superimposed particle in the plating bath

    Physio-Chemical and Mechanical Behaviour of(Pinussylvestris) as Binders on Foundry Core Strength

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    The mechanical potential of sand core binders made withPinussylvestris has been examined. Ota silica base sand bonded with 6% of cassava starch in admixed proportion of Pinussylvestris was tested for tensile, compressive strength and permeability to establish the binding efficiency. Tensile strength of the green baked core were oven baked at 50°C, 100°C, 150°C and 200°C.The cylindrically shaped permeability specimens were tested with permeability meter. Study revealed thatPinussylvestris showed an improve properties at 6% cassava starch at 200°C

    ZnO as corrosion inhibitor for dissolution of zinc electrodeposited mild steel in varying HCl concentration

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    The corrosion behavior of Zn electrodeposition on mild steel in varying 0.1 to 0.5 M of HCl with and without inhibitor was studied using weight loss measurement and optical microscope. The (OP) results revealed that the corrosion mechanism layers of the zinc plated mild steel without inhibitor has high content corrosivity related to the appearance of cracks due to the dissolution into the acidic medium. However, the zinc electrodeposition with ZnO as an inhibitor in the test medium shows a stable layer formation. The Zn coatings were found to contain an insoluble corrosion products, which act as a corrosion barrier that prevent corrosion from been attacked by the hydrogen presence

    Performance Evaluation of Zinc Deposited Mild Steel in Chloride Medium.

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    The effect of deposited mild steel under plating variable influence was investigated in a chloride medium. The results showed homogeneous layer with improved surface adhesion after deposition. The distance between the anode and the cathode on voltage, plating time and coating thickness were observed. The mild steel was deposited into solution of zinc bath for varying voltage between 0.6 v and 1.0v. It was discovered that the sample plated at 1.0v for 15 minutes gives the best plating surface finish. Analytical study using potentiastat/galvanostat, focused ion beam scanning electron microscopy (FIB-SEM), XRD and AFM were used to determine the surface characterization, topography and corrosion evaluation of the substrat

    Study of Al2O3/SiC particle loading on the microstructural strengthening characteristics of ZneAl2O3eSiC matrix composite coating

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    In this paper, the microstructure, and mechanical performance of ZneAl2O3eSiC film codeposited on mild steel substrate were produced by electrodeposition method. The structural characteristic of the composite coating was analyzed by scanning electron microscope (SEM) equipped with energy dispersive spectrometer (EDS), X-ray diffraction (XRD) and atomic force microscope (AFM). Mechanical examination was done using durascan hardness tester. The result showed that the influence of individual particle loading greatly alter the structural properties and hardness behavior. The increase in hardness is attributed to the perfect homogeneity and characteristics of the particulate which led to the formation of uniform distribution, coherent and interfacial precipitation within the zinc lattice
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