Tensile-Shear Fatigue Behavior of Aluminum and Magnesium Lap-Joints obtained by Ultrasonic Welding and Adhesive Bonding

n/

Fatigue analysis of adhesive joints with laser treated substrates

Abstract Recent literature works focused on the analysis of laser irradiation on the strength of adhesive joints under quasi-static loading conditions. It has been demonstrated that laser surface preparation allows to remove impurity and weak boundary layers from the mating substrates and, depending on the energy density, it is also able to modify surface morphology promoting mechanical interlocking. In previous works, the authors assessed the effect of Yb-fiber laser ablation over the quasi-static strength and toughness, of aluminum and stainless steel adhesively bonded joints. The experimental results demonstrated the ability of laser irradiation to improve the mechanical properties of the joints. The aim of this work is to extend the scope of previous investigations to fatigue loading. Double Cantilever Beam (DCB) samples with laser treated aluminum substrates have been bonded with a two component epoxy adhesive. For comparison standard degreasing and grit blasting have been also deployed for samples preparation. The results have been compared in terms of cycles to failure and the fracture surfaces have been analyzed by means of Scanning Electron Microscopy (SEM) in order to investigate the mechanism of failure

Engineering design in food-packaging industry: the case study of a tuna canning machine

Abstract Food packaging industry requires machines able to perform different tasks and carry out several functions. Machine modularization allows to feed customer's needs creating a set of equipment with different features and technology. Module derivation is particularly important at the conceptual phase where main decisions are taken and where the degree of freedom are higher, avoiding subsequent costly modification. This study aims at investigating the adoption of engineering design process for the development of a tuna canning machine, deriving main modules for a definition of a product platform. The possibility to have a modular framework in this type of products allows to satisfy constraints coming from different markets and applications (i.e., product quality, adaptability, upgradability, assemblability, compliance with standards where the machine is installed, etc.). Modules were derived based on state-of-art approaches used for product development (i.e., functional analysis, module derivation and morphological matrix) and two examples (i.e., Cutter and Compactor & Shaper modules) were detailed to explain the developed design solutions. Results highlight how different design options can be adopted to overcome several issues (i.e., assemblability, upgradability) and fulfill requirements of different markets (i.e., product quality and aesthetic)

numerical and experimental validation of a non standard specimen for uniaxial tensile test

Abstract Material testing is a fundamental activity for the characterization of materials mechanical properties and for the certification of product quality. With concepts such as Smart Factories and Industry 4.0 coming to the fore, testing and measurement is moving away from laboratories and closer to the production floor: MaCh 3D is a miniaturized tensile testing machine developed for products and materials certification directly on the production site. The heart of the technology is the specimen with non-conventional geometry for tensile tests developed so as to be easily installed on the machine. The objective of this work is to illustrate the process of determining the geometry of specimen and fixtures by numerical analysis and their experimental validation, comparing the results with those obtained from specimens according to ASTM D638 standard, ASTM International, (1999)

fracture toughness of structural adhesives for the automotive industry

Abstract Adhesive bonding is currently employed by automotive manufacturers to complement (or replace) welding in joining dissimilar materials. In order to reduce the impact on the existing manufacturing infrastructures, structural adhesives are deployed in the body shop but hardening is accomplished in the paint cure oven. Various adhesive formulations have been specifically developed for the implementation in the automotive manufacturing chain. However, it is very important to assess the mechanical behaviour of the joints which results from the peculiar curing strategy. In the present work, automotive grade single component epoxy and two component epoxy modified acrylic adhesives were evaluated. T-joints were fabricated using a cold rolled galvanized steel (FeP04) employed in the production of car body parts. The fracture toughness of the joints was determined using the test protocol proposed by the European Structural Integrity Society (ESIS). Optical microscopy was employed to ascertain the mechanisms of failure. The results indicated that both adhesives were able to provide a fairly good mechanical response with minimum preparation of the mating substrates. Moreover, the obtained values of fracture toughness were shown to be essentially independent of the adhesive layer thickness

Preparation and characterization of innovative poly(butylene adipate terephthalate)-based biocomposites for agri-food packaging application

The present work reports on the preparation and subsequent mechanical, morphological and thermal characterization of composites based on poly(butylene adipate terephthalate) (PBAT), reinforced with micro-particles of inorganic bioabsorbable calcium-phosphate glass (CPG) at different contents up to 40 wt%. The PBAT-CPG composites were prepared by solvent casting. The resulting composite pellets were used for the injection molding of model 1BA specimens, according to standard UNI EN ISO 527. PBAT-CPG composites displayed an effective increase of the Young's modulus (E) up to 82% with respect to the pristine polymer, while showing a reduction of the yield stress (σy) up to 20%, of the stress at break (σB) up to 46%, of the strain at break (εB) up to 57% and of the toughness (T) up to 72%. The values of E, σy and σB were also compared and validated with theoretical values calculated using Kerner’s and Pukanszky’s models. Scanning electron microscopy (SEM) images display homogeneous dispersion and distribution of the filler particles in the polymer matrix with no aggregates or phase separation that would cause a deterioration of the material properties. Infrared (IR) spectroscopy did not show structural variations of the polymer matrix due to the CPG presence. The oxygen permeability in PBAT-based samples assumes significantly lower values when benchmarked with the permeability of low-density polyethylene (LDPE). Among the different composites, a decrease in oxygen permeability is observed as the CPG concentration increases. Regarding water vapor permeability, PBAT-based samples show a lower barrier effect than PE: in particular, permeability to water vapor assumes an increasing trend as the quantity of filler increases. The tuneable degradability of the final composite materials was defined by the disintegration degree (DD) determination under composting conditions in a laboratory-scale reactor. The developed materials prove to be valid biodegradable and eco-friendly alternatives to traditional thermoplastic polymers, such as LDPE, and can be applied in many fields, especially in package and mulch film applications

Preparation and characterization of innovative poly(butylene adipate terephthalate)‐based biocomposites for agri‐food packaging application

The present work reports on the preparation and subsequent mechanical, morphological and thermal characterization of composites based on poly(butylene adipate terephthalate) (PBAT), reinforced with micro-particles of inorganic bioabsorbable calcium-phosphate glass (CPG) at different contents up to 40 wt%. The PBAT-CPG composites were prepared by solvent casting. The resulting composite pellets were used for the injection molding of model 1BA specimens, according to standard UNI EN ISO 527. PBAT-CPG composites displayed an effective increase of the Young's modulus (E) up to 82% compared to the pristine polymer, while showing a reduction of the yield stress (σy) up to 20%, of the stress at break (σB) up to 46%, of the strain at break (εB) up to 57% and of the toughness (T) up to 72%. The values of E, σy and σB were also compared and validated with theoretical values calculated using Kerner's and Pukanszky's models. Scanning electron microscopy (SEM) images display homogeneous dispersion and distribution of the filler particles in the polymer matrix with no aggregates or phase separation that would cause a deterioration of the material properties. Infrared (IR) spectroscopy did not show structural variations of the polymer matrix due to the CPG presence. The oxygen permeability in PBAT-based samples assumes significantly lower values when benchmarked with the permeability of low-density polyethylene (LDPE). Among the different composites, a decrease in oxygen permeability is observed as the CPG concentration increases. Regarding water vapor permeability, PBAT-based samples show a lower barrier effect than polyethylene (PE): in particular, permeability to water vapor assumes an increasing trend as the quantity of filler increases. The tuneable degradation of the final composite materials was defined by the disintegration degree (DD) determination under composting conditions in a laboratory-scale reactor. The developed materials prove to be valid biodegradable and eco-friendly alternatives to traditional thermoplastic polymers, such as LDPE, and can be applied in many fields, especially in package and mulch film applications

Acute Tubular Necrosis Following Interferon-Based Therapy for Hepatitis C: Case Study with Literature Review

Background/Aims: Interferon treatment of malignant or viral diseases can be accompanied by various side-effects including nephro-toxicity. Methods: We report on a 68-year-old Caucasian male who received dual therapy with pegylated interferon 2a plus ribavirin for chronic hepatitis C. Results: After three months of antiviral therapy, the patient developed acute kidney failure (serum creatinine up to 6 mg/dL) with mild proteinuria (500 mg daily) and haematuria. Immediate immunosuppressive therapy with high-dose intravenous steroids did not improve kidney function. Kidney biopsy was consistent with acute tubular necrosis without glomerular abnormalities. He started long-term peritoneal dialysis (four regular exchanges) to provide both dialysis adequacy and ascites removal. Kidney function gradually improved over the following months (serum creatinine around 2 mg/dL) and peritoneal dialysis was continued with two exchanges daily. The temporal relationship between the administration of the drug and the occurrence of nephro-toxicity, and the absence of other obvious reasons for acute tubular necrosis support a causative role for pegylated interferon; benefit on kidney disease was noted after withdrawal of antiviral agents. An extensive review of the literature on acute tubular necrosis associated with interferon-based therapy, based on in vitro data and earlier case-reports, has been made. The proposed pathogenic mechanisms are reviewed. Conclusions: Our case emphasizes the importance of monitoring renal function during treatment of chronic hepatitis C with antiviral combination therapy as treatment may precipitate kidney damage at tubular level