302 research outputs found
Synchrotron X-ray Diffraction Study of BaFe2As2 and CaFe2As2 at High Pressures up to 56 GPa: Ambient and Low-Temperatures Down to 33 K
We report high pressure powder synchrotron x-ray diffraction studies on
MFe2As2 (M=Ba, Ca) over a range of temperatures and pressures up to about 56
GPa using a membrane diamond anvil cell. A phase transition to a collapsed
tetragonal phase is observed in both compounds upon compression. However, at
300 (33) K in the Ba-compound the transition occurs at 26 (29) GPa, which is a
much higher pressure than 1.7 (0.3) GPa at 300 (40) K in the Ca-compound, due
to its larger volume. It is important to note that the transition in both
compounds occurs when they are compressed to almost the same value of the unit
cell volume and attain similar ct/at ratios. We also show that the FeAs4
tetrahedra are much less compressible and more distorted in the collapsed
tetragonal phase than their nearly regular shape in the ambient pressure phase.
We present a detailed analysis of the pressure dependence of the structures as
well as equation of states in these important BaFe2As2 and CaFe2As2 compounds.Comment: 26 pages, 12 figure
Assessment of stock state for walleye pollock in the Okhotsk Sea in the spring 2013
Results of the trawl and ichthyoplankton surveys conducted in the northern Okhotsk Sea in the spring of 2013 are presented. In comparison with 2012, the abundance of walleye pollock decreased in 1.8 times and its biomass - in 1.4 times. Number of the 1+ pollock is assessed in 1.6·109 ind., so the 2012 year-class is weak. The size structure is distinguished by 3 modes formed by strong year-classes: 17-23 cm (2+), 30-36 cm (5+), and 37-53 cm (mature fish). Spawning stock of pollock in the northern Okhotsk Sea is assessed as 6.649 million t that is considered as a medium value
Observation of the second harmonic in superconducting current-phase relation of Nb/Au/(001)YBa2Cu3Ox heterojunctions
The superconducting current-phase relation (CPR) of Nb/Au/(001)YBa2Cu3Ox
heterojunctions prepared on epitaxial c-axis oriented YBa2Cu3Ox thin films has
been measured in a single-junction interferometer. For the first time, the
second harmonic of the CPR of such junctions has been observed. The appearance
of the second harmonic and the relative sign of the first and second harmonics
of the CPR can be explained assuming, that the macroscopic pairing symmetry of
our YBa2Cu3Ox thin films is of the d+s typeComment: 11 pages, 4 figure
Electronic and magnetic structure of epitaxial NiO/FeO(001) heterostructures grown on MgO(001) and Nb-doped SrTiO(001)
We study the underlying chemical, electronic and magnetic properties of a
number of magnetite based thin films. The main focus is placed onto
NiO/FeO(001) bilayers grown on MgO(001) and Nb-SrTiO(001)
substrates. We compare the results with those obtained on pure FeO(001)
thin films. It is found that the magnetite layers are oxidized and Fe
dominates at the surfaces due to maghemite (-FeO) formation,
which decreases with increasing magnetite layer thickness. From a layer
thickness of around 20 nm on the cationic distribution is close to that of
stoichiometric FeO. At the interface between NiO and FeO we
find the Ni to be in a divalent valence state, with unambiguous spectral
features in the Ni 2p core level x-ray photoelectron spectra typical for NiO.
The formation of a significant NiFeO interlayer can be excluded by
means of XMCD. Magneto optical Kerr effect measurements reveal significant
higher coercive fields compared to magnetite thin films grown on MgO(001), and
a 45 rotated magnetic easy axis. We discuss the spin magnetic moments
of the magnetite layers and find that the moment increases with increasing thin
film thickness. At low thickness the NiO/FeO films grown on
Nb-SrTiO exhibits a significantly decreased spin magnetic moments. A
thickness of 20 nm or above leads to spin magnetic moments close to that of
bulk magnetite
Magnetic anisotropy in strained manganite films and bicrystal junctions
Transport and magnetic properties of LSMO manganite thin films and bicrystal
junctions were investigated. Manganite films were epitaxially grown on STO,
LAO, NGO and LSAT substrates and their magnetic anisotropy were determined by
two techniques of magnetic resonance spectroscopy. Compare with cubic
substrates a small (about 0.3 persentage), the anisotropy of the orthorhombic
NGO substrate leads to a uniaxial anisotropy of the magnetic properties of the
films in the plane of the substrate. Samples with different tilt of
crystallographic basal planes of manganite as well as bicrystal junctions with
rotation of the crystallographic axes (RB - junction) and with tilting of basal
planes (TB - junction) were investigated. It was found that on vicinal NGO
substrates the value of magnetic anisotropy could be varied by changing the
substrate inclination angle from 0 to 25 degrees. Measurement of magnetic
anisotropy of manganite bicrystal junction demonstrated the presence of two
ferromagnetically ordered spin subsystems for both types of bicrystal
boundaries RB and TB. The magnitude of the magnetoresistance for TB - junctions
increased with decreasing temperature and with the misorientation angle even
misorientation of easy axes in the parts of junction does not change. Analysis
of the voltage dependencies of bicrystal junction conductivity show that the
low value of the magnetoresistance for the LSMO bicrystal junctions can be
caused by two scattering mechanisms with the spin- flip of spin - polarized
carriers due to the strong electron - electron interactions in a disordered
layer at the bicrystal boundary at low temperatures and the spin-flip by anti
ferromagnetic magnons at high temperatures.Comment: 26 pages, 10 figure
Raman spectra of lead chalcogenide single crystals
Raman spectra of single crystals of lead chalcogenides (PbTe, PbSe, PbS) were studied at room temperature and ambient pressure. The structure of spectra for all compounds is rather similar showing the bands in one-and two-phonon range. Possible spectra identification is discussed
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