Adhesive bonding of resin composite to various titanium surfaces using different metal conditioners and a surface modification system

OBJECTIVE: This study evaluated the effect of three metal conditioners on the shear bond strength (SBS) of a prosthetic composite material to cpTi grade I having three surface treatments. MATERIAL AND METHODS: One hundred sixty eight rivet-shaped specimens (8.0x2.0 mm) were cast and subjected to polishing (P) or sandblasting with either 50 mm (50SB) or 250 mm (250SB) Al(2)O(3). The metal conditioners Metal Photo Primer (MPP), Cesead II Opaque Primer (OP), Targis Link (TL), and one surface modification system Siloc (S), were applied to the specimen surfaces, which were covered with four 1-mm thick layers of resin composite. The resin layers were exposed to curing light for 90 s separately. Seven specimens from each experimental group were stored in water at 37ºC for 24 h while the other 7 specimens were subjected to 5,000 thermal cycles consisting of water baths at 4ºC and 60ºC (n=7). All specimens were subjected to SBS test (0.5 mm/min) until failure occurred, and further 28 specimens were analyzed using scanning electron microscope (SEM) and X-ray energy-dispersive spectroscopy (EDS). Data were analyzed by 3-way ANOVA followed by post-hoc Tukey's test (α=0.05). RESULTS: On 50SB surfaces, OP groups showed higher SBS means than MPP (P<0.05), while no significant difference was found among OP, S, and TL groups. On 250SB surfaces, OP and TL groups exhibited higher SBS than MPP and S (P<0.05). No significant difference in SBS was found between OP and TL groups nor between MPP and S groups. The use of conditioners on 250SB surfaces resulted in higher SBS means than the use of the same products on 50SB surfaces (P<0.05). CONCLUSION: Sandblasting associated with the use of metal conditioners improves SBS of resin composites to cpTi

Correlation between clinical performance and degree of conversion of resin cements: a literature review

AbstractResin-based cements have been frequently employed in clinical practice to lute indirect restorations. However, there are numerous factors that may compromise the clinical performance of those cements. The aim of this literature review is to present and discuss some of the clinical factors that may affect the performance of current resin-based luting systems. Resin cements may have three different curing mechanisms: chemical curing, photo curing or a combination of both. Chemically cured systems are recommended to be used under opaque or thick restorations, due to the reduced access of the light. Photo-cured cements are mainly indicated for translucent veneers, due to the possibility of light transmission through the restoration. Dual-cured are more versatile systems and, theoretically, can be used in either situation, since the presence of both curing mechanisms might guarantee a high degree of conversion (DC) under every condition. However, it has been demonstrated that clinical procedures and characteristics of the materials may have many different implications in the DC of currently available resin cements, affecting their mechanical properties, bond strength to the substrate and the esthetic results of the restoration. Factors such as curing mechanism, choice of adhesive system, indirect restorative material and light-curing device may affect the degree of conversion of the cement and, therefore, have an effect on the clinical performance of resin-based cements. Specific measures are to be taken to ensure a higher DC of the luting system to be used

Shrinkage Stress, Long-term Adaptation And Bond Strength Of Low-shrinkage Composite Resins

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Purpose: To evaluate the internal adaptation, bond strength, and polymerization stress of silorane- and methacrylate-based composite resins. Material and methods: Three methacrylate-based composite resins (Heliomolar; Tetric N-Ceram and Aelite LS) and one silorane-based composite resin (Filtek Silorane) were tested. Polymerization stress (n=5) was determined by the insertion of the composite resin between rods of polymethyl methacrylate. The ratio of the maximum force of contraction was recorded and the cross-sectional area of the rod was used to calculate the nominal stress. Bond strength was evaluated by microtensile bond test. Dentin surfaces of human third molars were bonded, sectioned, and stored for 24 h or 1 year in distilled water before the bond strength test. The ratio of maximum force and the adhered area was used for the bond strength calculation. For internal adaptation analysis, third molars received Class II cavities and were restored according to either an incremental oblique or bulk-filling technique. After being sectioned perpendicularly, impressions were taken and epoxy resin replicas were obtained of the internal surfaces of the restorations (after 24 h and 1 year of storage) to analyze gap formation using scanning electron microscopy. Results: Filtek Silorane showed the highest bond strength after one year of storage, the lowest formation of gaps, and polymerization stress similar to methacrylate-based materials. Conclusion: Silorane restorative material presented polymerization stress comparable to that of methacrylate-based composite resins, stable dentin bond strength after one year and better internal adaptation to the cavity walls, showing good alternative to traditional composite resins and promising longevity. (C) 2015 Elsevier Ltd. All rights reserved.65110Sao Paulo Research Foundation (FAPESP) [2009/51454-6]National Council for Scientific and Technological Development (CNPq), Brazil [305777-2010-6]Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq

Scan flip-flops with on-line testing ability with respect to input delay and crosstalk faults

We propose a possible modification to the internal structure of scan flip-flops, which allows the online detection of delay and crosstalk faults affecting their input. Our solution allows to obtain, together with the flip-flop output datum, an indication denoting whether or not the provided datum is incorrect, because of an input crosstalk or delay fault. The proposed solution features self-checking ability with respect to a wide set of possible internal faults, including node stuck-ats, transistor stuck-ons and stuck-opens, resistive bridgings, delays, transient and crosstalk faults

Effect of Curing Mode on Bond Strength of Self-Adhesive Resin Luting Cements to Dentin

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)In this study, the in vitro bond strength of dual-curing resin cements to indirect composite restorations when the cement was either light polymerized or allowed to only autopolymerize was evaluated. Occlusal dentin surfaces of 56 extracted human third molars were flattened to expose coronal dentin. Teeth were assigned to eight groups (n = 7) according to resin cement products and polymerization modes: conventional cement (Panavia F 2.0; Kuraray Medical) and self-adhesive cements [RelyX Unicem (3M ESPE), BisCem (Bisco), and G-Cem (GC Corp.)]. Cements were applied to prepolymerized resin discs (2-mm-thick Sinfony; 3M ESPE), which were subsequently bonded to the prepared dentin surfaces. The restored teeth were either light-polymerized through the overlying composite according to manufacturers' instructions or were allowed to only self-cure. After 24 h, the teeth and restorations were sectioned to obtain multiple bonded beams (1.0 mm(2)) and tested in tension at a crosshead speed of 0.5 mm/min until failure. Data (MPa) were analyzed by two-way ANOVA and Tukey test (alpha = 0.05). Light activation of some cement systems (G-Cem and Panavia F 2.0) increased the bond strength, while the curing mode did not affect the bond strength for some (RelyX Unicem and BisCem). The bond strength in the autopolymerized mode varied among products. In general, the use of self-adhesive resin cements did not provide significantly higher bond strengths than that of a conventional material, and two self-adhesive cements yielded significantly lower bond values (regardless of cure mode) than the other products. (C) 2010 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater 938: 122-127, 201093B1122127Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)FAPESP [07/53214-7

On-Chip Clock Faults' Detector

This paper proposes an on-chip detector for the on-line testing of faults affecting clock signals and making them change with incorrect duty-cycle. Our scheme is particularly suitable to be integrated within Systems-On-a-Chip (SOCs), in order to avoid their possible incorrect operation because of faults affecting clock signals, thus solving their extreme criticality in clock faults' testing. In particular, our detector is suitable to be applied to clock signals within each SOC digital core, to the clock signals at the interface between the diverse cores, as well as to those driving the DFT and BIST structures used to perform the SOC test. Our scheme features self-checking ability with respect to its possible internal faults belonging to a realistic set including stuck-ats, transistor stuck-ons, stuck-opens and resistive bridgings

Shrinkage Stress, Long-term Adaptation And Bond Strength Of Low-shrinkage Composite Resins

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)To evaluate the internal adaptation, bond strength, and polymerization stress of silorane- and methacrylate-based composite resins. Material and methods: Three methacrylate-based composite resins (Heliomolar; Tetric N-Ceram and Aelite LS) and one silorane-based composite resin (Filtek Silorane) were tested. Polymerization stress (n=5) was determined by the insertion of the composite resin between rods of polymethyl methacrylate. The ratio of the maximum force of contraction was recorded and the cross-sectional area of the rod was used to calculate the nominal stress. Bond strength was evaluated by microtensile bond test. Dentin surfaces of human third molars were bonded, sectioned, and stored for 24 h or 1 year in distilled water before the bond strength test. The ratio of maximum force and the adhered area was used for the bond strength calculation. For internal adaptation analysis, third molars received Class II cavities and were restored according to either an incremental oblique or bulk-filling technique. After being sectioned perpendicularly, impressions were taken and epoxy resin replicas were obtained of the internal surfaces of the restorations (after 24 h and 1 year of storage) to analyze gap formation using scanning electron microscopy. Results: Filtek Silorane showed the highest bond strength after one year of storage, the lowest formation of gaps, and polymerization stress similar to methacrylate-based materials. Conclusion: Silorane restorative material presented polymerization stress comparable to that of methacrylate-based composite resins, stable dentin bond strength after one year and better internal adaptation to the cavity walls, showing good alternative to traditional composite resins and promising longevity. (C) 2015 Elsevier Ltd. All rights reserved.65110Sao Paulo Research Foundation (FAPESP) [2009/51454-6]National Council for Scientific and Technological Development (CNPq), Brazil [305777-2010-6]Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq