Elastic characterization of nanometer-thick polymeric film for astrophysics application with an experimental-numerical method

The x-ray detectors on board astrophysics space missions require optical blocking filters that are highly transparent to x-rays. The filter design typically consists of a polymeric film that is a few tens of nanometers thick coated with aluminium. Due to the large size of the filter membrane (from a few tens to a few hundred square centimeters) and the extreme aspect ratio, together with severe loading conditions during launch and different stoichiometries of the polymer that could change its mechanical properties, a characterization study of the employed material is needed. The plane strain bulge test is a well-accepted methodology for the mechanical testing of structures that are less than a micrometer thick, and especially for freestanding membranes. Unfortunately, testing such ultra-thin films is not a simple task due to residual stress and experimental uncertainty at very low pressure. In this work, the elastic properties of an extremely thin (between 45 and 415 nm) membrane made of bare polyimide and coated with aluminium were derived through adopting a combined experimental-numerical methodology based on the bulge test and numerical simulations

Thermalization of Mesh Reinforced Ultra-Thin Al-Coated Plastic Films: A Parametric Study Applied to the Athena X-IFU Instrument

The X-ray Integral Field Unit (X-IFU) is one of the two focal plane detectors of Athena, a large-class high energy astrophysics space mission approved by ESA in the Cosmic Vision 2015-2025 Science Program. The X-IFU consists of a large array of transition edge sensor micro-calorimeters that operate at similar to 100 mK inside a sophisticated cryostat. To prevent molecular contamination and to minimize photon shot noise on the sensitive X-IFU cryogenic detector array, a set of thermal filters (THFs) operating at different temperatures are needed. Since contamination already occurs below 300 K, the outer and more exposed THF must be kept at a higher temperature. To meet the low energy effective area requirements, the THFs are to be made of a thin polyimide film (45 nm) coated in aluminum (30 nm) and supported by a metallic mesh. Due to the small thickness and the low thermal conductance of the material, the membranes are prone to developing a radial temperature gradient due to radiative coupling with the environment. Considering the fragility of the membrane and the high reflectivity in IR energy domain, temperature measurements are difficult. In this work, a parametric numerical study is performed to retrieve the radial temperature profile of the larger and outer THF of the Athena X-IFU using a Finite Element Model approach. The effects on the radial temperature profile of different design parameters and boundary conditions are considered: (i) the mesh design and material, (ii) the plating material, (iii) the addition of a thick Y-cross applied over the mesh, (iv) an active heating heat flux injected on the center and (v) a Joule heating of the mesh. The outcomes of this study have guided the choice of the baseline strategy for the heating of the Athena X-IFU THFs, fulfilling the stringent thermal specifications of the instrument

Multi-technique investigation of silicon nitride/aluminum membranes as optical blocking filters for high-energy space missions

X-ray detectors for space astrophysics missions are susceptible to noise caused by photons with energies outside the operating energy range; for this reason, efficient external optical blocking filters are required to shield the detector from the out-ofband radiation. These filters play a crucial role in meeting the scientific requirements of the X-ray detectors, and their proper operation over the life of the mission is essential for the success of the experimental activity. We studied thin sandwich membranes made of silicon nitride and aluminum as optical blocking filters for high-energy detectors in space missions. Here, we report the results of a multitechnique characterization of SiN membranes with thicknesses in the range from 40 nm to 145 nm coated with few tens of nanometers of aluminum on both sides. In particular, we have measured the X-ray transmission at synchrotron radiation beamlines, the rejection of ultraviolet, visible, and near-infrared radiation, the amount of native oxide on the aluminum surfaces by X-ray photoelectron spectroscopy, the morphology of the sample surfaces by atomic force microscopy, and the aging effects under proton irradiation

The Athena X-ray Integral Field Unit: a consolidated design for the system requirement review of the preliminary definition phase

The Athena X-ray Integral Unit (X-IFU) is the high resolution X-ray spectrometer studied since 2015 for flying in the mid-30s on the Athena space X-ray Observatory. Athena is a versatile observatory designed to address the Hot and Energetic Universe science theme, as selected in November 2013 by the Survey Science Committee. Based on a large format array of Transition Edge Sensors (TES), X-IFU aims to provide spatially resolved X-ray spectroscopy, with a spectral resolution of 2.5 eV (up to 7 keV) over a hexagonal field of view of 5 arc minutes (equivalent diameter). The X-IFU entered its System Requirement Review (SRR) in June 2022, at about the same time when ESA called for an overall X-IFU redesign (including the X-IFU cryostat and the cooling chain), due to an unanticipated cost overrun of Athena. In this paper, after illustrating the breakthrough capabilities of the X-IFU, we describe the instrument as presented at its SRR (i.e. in the course of its preliminary definition phase, so-called B1), browsing through all the subsystems and associated requirements. We then show the instrument budgets, with a particular emphasis on the anticipated budgets of some of its key performance parameters, such as the instrument efficiency, spectral resolution, energy scale knowledge, count rate capability, non X-ray background and target of opportunity efficiency. Finally, we briefly discuss the ongoing key technology demonstration activities, the calibration and the activities foreseen in the X-IFU Instrument Science Center, touch on communication and outreach activities, the consortium organisation and the life cycle assessment of X-IFU aiming at minimising the environmental footprint, associated with the development of the instrument. Thanks to the studies conducted so far on X-IFU, it is expected that along the design-to-cost exercise requested by ESA, the X-IFU will maintain flagship capabilities in spatially resolved high resolution X-ray spectroscopy, enabling most of the original X-IFU related scientific objectives of the Athena mission to be retained. The X-IFU will be provided by an international consortium led by France, The Netherlands and Italy, with ESA member state contributions from Belgium, Czech Republic, Finland, Germany, Poland, Spain, Switzerland, with additional contributions from the United States and Japan.The French contribution to X-IFU is funded by CNES, CNRS and CEA. This work has been also supported by ASI (Italian Space Agency) through the Contract 2019-27-HH.0, and by the ESA (European Space Agency) Core Technology Program (CTP) Contract No. 4000114932/15/NL/BW and the AREMBES - ESA CTP No.4000116655/16/NL/BW. This publication is part of grant RTI2018-096686-B-C21 funded by MCIN/AEI/10.13039/501100011033 and by “ERDF A way of making Europe”. This publication is part of grant RTI2018-096686-B-C21 and PID2020-115325GB-C31 funded by MCIN/AEI/10.13039/501100011033

Filters design and characterization for LAD instrument onboard eXTP

The LAD (Large Area Detector) instrument, onboard the Sino-European mission eXTP (enhanced X-ray Timing and Polarimetry), will perform single-photon, high-resolution timing and energy measurements, in the energy range 2–30 keV, with a large collecting area. Its silicon drift detectors need shielding from NIR/Vis/UV light by astrophysical sources and the bright Earth, to avoid performance degradation. Filters made of an Al coated thin polyimide (PI) membrane will guarantee the needed out-of-band rejection while offering high X-ray transparency. They will be placed between the detectors and the capillary plate plate collimators, open to the external environment. The mission is now in phase B2 and a baseline design for the filters was produced. We describe the filter design and modeling activity, and report the characterization performed so far on X-ray transmission, pinhole and defects, thermo-vacuum cycling endurance, and bright Earth optical load shielding properties

The Athena X-ray Integral Field Unit: a consolidated design for the system requirement review of the preliminary definition phase

48 pages, 29 figures, submitted for publication in Experimental AstronomyThe Athena X-ray Integral Unit (X-IFU) is the high resolution X-ray spectrometer, studied since 2015 for flying in the mid-30s on the Athena space X-ray Observatory, a versatile observatory designed to address the Hot and Energetic Universe science theme, selected in November 2013 by the Survey Science Committee. Based on a large format array of Transition Edge Sensors (TES), it aims to provide spatially resolved X-ray spectroscopy, with a spectral resolution of 2.5 eV (up to 7 keV) over an hexagonal field of view of 5 arc minutes (equivalent diameter). The X-IFU entered its System Requirement Review (SRR) in June 2022, at about the same time when ESA called for an overall X-IFU redesign (including the X-IFU cryostat and the cooling chain), due to an unanticipated cost overrun of Athena. In this paper, after illustrating the breakthrough capabilities of the X-IFU, we describe the instrument as presented at its SRR, browsing through all the subsystems and associated requirements. We then show the instrument budgets, with a particular emphasis on the anticipated budgets of some of its key performance parameters. Finally we briefly discuss on the ongoing key technology demonstration activities, the calibration and the activities foreseen in the X-IFU Instrument Science Center, and touch on communication and outreach activities, the consortium organisation, and finally on the life cycle assessment of X-IFU aiming at minimising the environmental footprint, associated with the development of the instrument. It is expected that thanks to the studies conducted so far on X-IFU, along the design-to-cost exercise requested by ESA, the X-IFU will maintain flagship capabilities in spatially resolved high resolution X-ray spectroscopy, enabling most of the original X-IFU related scientific objectives of the Athena mission to be retained (abridged)