225 research outputs found

    Peculiarities of training foreign students in the masters program «International business in the field of trade and services»

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    Nowadays more and more foreigners choose Russia as a country where they can get education in a prestige University, knowledge o f Russian being not obligatory. Thus, to deliver lectures for foreign students Russian specialists should both professionally master English and consider their national and vocational peculiaritiesВ последние годы все больше иностранных граждан выбирают Россию в качестве страны, где можно получить образование в престижном университете, причем без знания русского языка. В этой связи для российских преподавателей важным является не только хорошее владение английским языком, а также профессиональных и национальных особенностей магистранто

    Effect of anodic oxygen evolution on cell morphology of sulfuric acid anodic alumina films

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    The purpose of this work was to study and analyze the effect of electrolyte temperature and anodization voltage on cell morphology of thin films of sulfuric acid anodic alumina formed on substrates of different nature, such as SiO2/Si, glass-ceramic, glass substrates, and polished aluminum. The data obtained demonstrated that the thermal conductivity of the substrate in the voltage range from 12 to 14 V affected a pore diameter (dpore) in anodic films. Depending on the substrate type, dpore increased in the following order: glass > glass- ceramic > SiO2/Si > aluminum. It was found that the anodizing voltage (Ua) of 16 V was a turning point for anodic films obtained in sulfuric acid after which the slope of the lines for both dpore and Dinter (interpore distance) vs. Ua changed. This behavior might be explained by the occurrence of the overpotential enough for the beginning of the oxygen evolution reaction. We assumed that the oxygen evolution on aluminum oxide surface at the pore bottom at Ua> 16 V results in an increase in acid concentration in the solution and, consequently, in rise in acidic nature of the electrolyte and increase in the dissolution rate of the oxide layer of pore walls

    Photoluminescence and its damping kinetics of nanoporous alumina m embranes formed in solutions of various carboxylic acids

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    The article is devoted to the study of the photoluminescence of carbon-containing anodic alumina obtained in various electrolytes based on carboxylic (tartaric and oxalic) acids. We studied the emission and excitation spectra of luminescence, as well as the PL decay of nanostructured anodic alumina membranes. It is shown that such membranes exhibit photoluminescence (excitation wavelength 330 nm) in the wavelength range 350-600 nm with a maximum at 460 nm. They have two PL centers with maxima at 440 and 490 nm and lifetimes of 0.2 and 4.0 ns, respectively. It is shown that the PL peak at 440 nm can be related to the emission of COO– - ions, and the peak at 490 nm can be related to the PL of defects in partially oxidized amorphous carbon

    The sorption of water molecules in the pores of anodic alumina films during aluminum anodizing in oxalic acid

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    The thermogravimetric analysis of membranes of anodic aluminum oxide (AAO) was carried out. The results showed that in the process of anodic growth, water molecules are adsorbed in the pores of Al2O3, the amount of which is determined by the anodizing voltage of aluminum. The relationship is revealed and the graphs of the relationship between anodizing voltage, annealing temperature, and weight loss of nanostructured membranes of AAO are presented. It has been established that the adsorption of water molecules on the surface of AAO is explained by the presence of a surface charge, which disappears after annealing at 200–300 °C. An increase in the amount of adsorbed water with an increase in the anodizing voltage from 20 to 40 V indicates a decrease in the surface charge density

    Stored charge and its influence on properties of anodic alumina films

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    In porous and barrier-type anodic alumina films, the stored charge has electronic nature and it plays a significant role in the process of aluminum anodizing. The charge stored can modify the distribution of local field generated by a voltage applied and thus it can affect the oxide growth. The method for the investigation of thermally activated defects in anodic alumina films by reanodizing technique was also described. It was applied for computation of activation energy of electron traps in barrier layer for sulfuric and oxalic acid alumina films and concentration of the traps

    Investigation of the features of the porous morphology of anodic alumina films at the initial stage of anodization

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    The work is devoted to the study of the porous structure formation of anodic alumina films at the initial stage of aluminium anodizing. SEM images of the surface morphology of the oxalic acid anodic films were analyzed. It was shown that at the initial stage, both major and minor pores are formed, the diameter ratio of which is about 1.16 and does not depend on the anodizing voltage. The results obtained indicate that the minor pores in the anodic films are located inside hexagonal cells composed of the major pores

    Scientific Performance of the ISDC Quick Look Analysis

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    The INTEGRAL Science Data Centre (ISDC) routinely monitors the Near Real Time data (NRT) from the INTEGRAL satellite. A first scientific analysis is made in order to check for the detection of new, transient or highly variable sources in the data. Of primary importance for this work is the Interactive Quick Look Analysis (IQLA), which produces JEM-X and ISGRI images and monitors them for interesting astrophysical eventsComment: 4 pages, 3 figures. Proceedings of 5th INTEGRAL Workshop: The INTEGRAL Universe, Munich, 16-20 February 2004. Accepted for publication in European Space Agency Special Publication 552. See paper for institute affiliation

    Study of microstructure of porous anodic alumina films formed in malonic acid in the wide range of aluminium anodizing voltages

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    In present paper the microstructure parameters of porous anodic alumina films formed by the anodizing of aluminum in the aqueous solution of malonic acid at different anodizing voltages was studied. The morphology of structured surface of aluminum film was studied using a scanning electron microscope after selective removal of anodic film. The results obtained for anodic films formed in malonic acid during anodizing in the range of 15-80 V allowed to determine that change in the interpore distance with the anodizing voltage is linear function with a slope of 1.45. The key conclusion was made that mechanical stress in anodic alumina layer is the main factor responsible for formation of the nanoporous structure of anodic alumina films

    Monitoring of Electrode Temperature in Exothermic Electrochemical Process

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    In this paper the features of temperature control of aluminum electrode during the anodization are discussed. Temperature monitoring in this exothermic process is a necessary condition for obtaining a high ordered nanoporous structure. A new electrochemical cell with a Peltier device working in cooling or heating mode was proposed. Time dependences of the electrolyte and Peltier element temperatures without and during anodizing process were presented. The results demonstrated that the cell construction allows precise control of the electrode temperature
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