Steel nitriding optimization through multi-objective and FEM analysis☆

Abstract Steel nitriding is a thermo-chemical process leading to surface hardening and improvement in fatigue properties. The process is strongly influenced by many different variables such as steel composition, nitrogen potential, temperature, time, and quenching media. In the present study, the influence of such parameters affecting physic-chemical and mechanical properties of nitride steels was evaluated. The aim was to streamline the process by numerical–experimental analysis allowing defining the optimal conditions for the success of the process. Input parameters–output results correlations were calculated through the employment of a multi-objective optimization software, modeFRONTIER (Esteco). The mechanical and microstructural results belonging to the nitriding process, performed with different processing conditions for various steels, are presented. The data were employed to obtain the analytical equations describing nitriding behavior as a function of nitriding parameters and steel composition. The obtained model was validated, through control designs, and optimized by taking into account physical and processing conditions. Highlights The paper shows the development of a model based on very broad experimental activity. The data were employed to provide a provisional tool for nitrided steel mechanical and microstructural behavior. A very good experimental–numerical correlation was found

Effect of welding parameters on mechanical and microstructural properties of AA6082 jointsproduced by friction stir welding

The effect of processing parameters on mechanical and microstructural properties of AA6082 joints produced by friction stir welding was analysed in the present study. Different welded specimens were produced by employing a fixed rotating speeds of 1600rpm and by varying welding speeds from 40 to 460 mm/min. The joints mechanical properties were evaluated by means of tensile tests at room temperature. In addition, fatigue tests were performed by using a resonant electro-mechanical testing machine under constant amplitude control up to 250 Hz sinusoidal loading. The fatigue tests were conducted in axial control mode with R = min/max = 0.1, for all the welding and rotating speeds used in the present study. The microstructural evolution of the material was analysed according to the welding parameters by optical observations of the jointed cross-sections and SEM observations of the fractured surfaces were done to characterize the weld performances

Water Electrolysis for the Production of Hydrogen to Be Employed in the Ironmaking and Steelmaking Industry

The way to decarbonization will be characterized by the huge production of hydrogen through sustainable routes. Thus, the basic production way is water electrolysis sustained by renewable energy sources allowing for obtaining "green hydrogen". The present paper reviews the main available technologies for the water electrolysis finalized to the hydrogen production. We describe the fundamental of water electrolysis and the problems related to purification and/or desalinization of water before electrolysis. As a matter of fact, we describe the energy efficiency issues with particular attention to the potential application in the steel industry. The fundamental aspects related to the choice of high-temperature or low-temperature technologies are analyzed. Keywords: water electrolysis; ironmaking; steelmaking;

Mechanical and microstructural behaviour of 2024–7075 aluminium alloy sheets joined by friction stir welding

The aim of the present work is to investigate on the mechanical and microstructural properties of dissimilar 2024 and 7075 aluminium sheets joined by friction stir welding (FSW). The two sheets, aligned with perpendicular rolling directions, have been successfully welded; successively, the welded sheets have been tested under tension at room temperature in order to analyse the mechanical response with respect to the parent materials. The fatigue endurance (S–N) curves of the welded joints have been achieved, since the fatigue behaviour of light welded sheets is the best performance indicator for a large part of industrial applications; a resonant electro-mechanical testing machine load and a constant load ratio RZsmin/smaxZ0.1 have been used at a load frequency of about 75 Hz. The resulted microstructure due to the FSW process has been studied by employing optical and scanning electron microscopy either on ‘as welded’ specimens and on tested specimen after rupture occurred

Thermoelasticity and CCD analysis of crack propagation in AA6082 friction stir w elded joints

The advantages of friction stir welding (FSW) process compared to conventional fusion welding technologies have been clearly demonstrated in recent years. In the present study, AA6082 FSW joints were produced by employing different welding parameters. The principal aim of this work is to apply thermoelastic stress analysis (TSA) to study crack propagation characteristics of friction stir welded aluminum sheets, during cyclic fatigue tests. The crack propagation experiments were performed by employing single edge notched specimens; fatigue tests were performed under tension with load ratio R = 0.1. All the mechanical tests were conducted up to failure. The TSA measurement system allowed crack evolution to be observed in real-time during fatigue cycles and stress fields to be derived on the specimens from the measured temperature variation. The thermoelastic data were used to analyse principal stresses and principal strains on the specimens surface and the crack growth rate during tests. In addition, it was possible to evaluate all the joints defects effects, as a function of welding parameters, correlating effects on different crack growth rate and instabilities. The achieved results were compared with those obtained by classical CCD camera monitoring of crack front propagation during cyclic loading and all the results were validated by employing finite element analysis performed with ABAQUS software