Study of the effect of microwave power coupled with hot air drying on orange peel by dielectric spectroscopy

[EN] Monitoring moisture and water activity during drying is crucial for process optimization, avoiding inadequate uses of energy. The main objective of this work was to study the dielectric properties of orange peel during hot air drying at 55 °C (HAD) and microwave power coupled with hot air drying at different power intensities (2 W/g, 4 W/g and 6 W/g). At 5, 15, 40, 60 and 120 min mass, aw, moisture, and permittivity were measured in fresh and dried samples. Results allowed developing a dielectric isotherm technique by adapting the GAB model to predict aw in dried orange peel by using ε'ε' (20 GHz). The physical meaning of the dielectric isotherm parameters (View the MathML sourceε0' and Cd) was studied. The value of View the MathML sourceε0' at 20 GHz (γ-dispersion) represents the induction effect of the minimum quantity of adsorbed water or the monomolecular moisture layer. The parameter Cd is related with isosteric heat, as well as the C parameter of the GAB model. The application of MW power produced an increase of isosteric heat or adsorption energy of the monomolecular layer, improving surface tension of samples and thus the hygroscopicity, explaining the reduction of the View the MathML sourceε0' independently of the quantity of the water molecules adsorbed.The authors would like to acknowledge the Basque Government for the financial support of the project (LasaiFood). The author Marta Castro-Giraldez wants to thanks to the UPV Postdoctoral Program (PAID-10-14) from Universidad Politecnica de Valencia for their support. The authors acknowledge the financial support from the Spanish Ministerio de Ciencia e Innovacion throughout the project AGL2011-30096.Talens Vila, C.; Castro Giraldez, M.; Fito Suñer, PJ. (2016). Study of the effect of microwave power coupled with hot air drying on orange peel by dielectric spectroscopy. LWT - Food Science and Technology. 66:622-628. https://doi.org/10.1016/j.lwt.2015.11.015S6226286

Effect of Microwave Power Coupled with Hot Air Drying on Sorption Isotherms and Microstructure of Orange Pee

[EN] Drying is one of the most cost-effective methods of worthwhile by-product valorisation. This study had two main objectives. The first was to determine the effect of hot air drying (HAD) combined with microwave (MW) irradiation on the treatment kinetics and the macrostructural and microstructural properties of the dried product. The second aim was to develop engineering tools to predict the extent of dehydration. Drying was performed using hot air at 55 A degrees C and the combined (HAD + MW) treatment at different power intensities (2, 4, and 6 W/g). After 5, 15, 40, 60, and 120 min, the mass, surface, volume, water activity and moisture were measured in fresh and dried samples. Sorption isotherms were obtained and fitted to the GAB model, with high correlation coefficients. The macroscopic and microscopic analyses showed shrinkage and swelling in the peel tissue caused by the MW treatment. The HAD + MW methods not only resulted in increased moisture reduction but also induced microstructural changes that generated higher sorption capacity.The authors would like to thank the Basque Government for the financial support of the project (LasaiFood). They also acknowledge the financial support from the Spanish Ministerio de Economia, Industria y Competitividad, Programa Estatal de I+D+i orientada a los Retos de la Sociedad AGL2016-80643-R. This paper is contribution no. 777 from AZTI (Food Research Division). The authors would like to thank the Electronic Microscopy Service of the Universidad Politecnica de Valencia for its assistance in the use of Cryo-SEM.Talens Vila, C.; Castro Giraldez, M.; Fito Suñer, PJ. (2018). Effect of Microwave Power Coupled with Hot Air Drying on Sorption Isotherms and Microstructure of Orange Pee. Food and Bioprocess Technology. 11(4):723-734. https://doi.org/10.1007/s11947-017-2041-xS723734114Al-Muhtaseb, A. H., McMinn, W. A. M., & Magee, T. R. A. (2002). Moisture sorption isotherm characteristics of food products: a review. Food and Bioproducts Processing, 80(2), 118–128. https://doi.org/10.1205/09603080252938753 .Andrade, R. D., Lemus, R., & Pérez, C. E. (2011). Models of sorption isotherms for food: uses and limitations. Vitae, 18(3), 325–334.Bejar, A. K., Ghanem, N., Mihoubi, D., Kechaou, N., & Mihoubi, N. B. (2011). Effect of infrared drying on drying kinetics, color, total phenols and water and oil holding capacities of orange (Citrus sinensis) peel and leaves. International Journal of Food Engineering, 7(5). https://doi.org/10.2202/1556-3758.2222 .Bergese, P. (2006). Specific heat, polarization and heat conduction in microwave heating systems: a nonequilibrium thermodynamic point of view. Acta Materialia, 54(7), 1843–1849. https://doi.org/10.1016/j.actamat.2005.11.042 .Castro-Giráldez, M., Fito, P. J., Chenoll, C., & Fito, P. (2010). Development of a dielectric spectroscopy technique for the determination of apple (Granny Smith) maturity. Innovative Food Science & Emerging Technologies, 11(4), 749–754. https://doi.org/10.1016/j.ifset.2010.08.002 .Castro-Giráldez, M., Fito, P. J., Dalla Rosa, M., & Fito, P. (2011a). Application of microwaves dielectric spectroscopy for controlling osmotic dehydration of kiwifruit (Actinidia deliciosa cv Hayward). Innovative Food Science & Emerging Technologies, 12(4), 623–627. https://doi.org/10.1016/j.ifset.2011.06.013 .Castro-Giráldez, M., Fito, P. J., & Fito, P. (2011b). Application of microwaves dielectric spectroscopy for controlling long time osmotic dehydration of parenchymatic apple tissue. Journal of Food Engineering, 104(2), 227–233. https://doi.org/10.1016/j.jfoodeng.2010.10.034 .Demirel, Y., & Sandler, S. I. (2001). Linear-nonequilibrium thermodynamics theory for coupled heat and mass transport. International Journal of Heat and Mass Transfer, 44(13), 2439–2451. https://doi.org/10.1016/S0017-9310(00)00291-X .Edrisi Sormoli, M., & Langrish, T. A. G. (2015). Moisture sorption isotherms and net isosteric heat of sorption for spray-dried pure orange juice powder. LWT—Food Science and Technology, 62(1, part 2), 875–882. https://doi.org/10.1016/j.lwt.2014.09.064 .Fava, F., Zanaroli, G., Vannini, L., Guerzoni, E., Bordoni, A., Viaggi, D., Robertson, J., Waldron, K., Bald, C., Esturo, A., Talens, C., Tueros, I., Cebrián, M., Sebők, A., Kuti, T., Broeze, J., Macias, M., & Brendle, H. G. (2013). New advances in the integrated management of food processing by-products in Europe: sustainable exploitation of fruit and cereal processing by-products with the production of new food products (NAMASTE EU). New Biotechnology, 30(6), 647–655. https://doi.org/10.1016/j.nbt.2013.05.001 .Fernández-López, J., Sendra-Nadal, E., Navarro, C., Sayas, E., Viuda-Martos, M., & Alvarez, J. A. P. (2009). Storage stability of a high dietary fibre powder from orange by-products. International Journal of Food Science and Technology, 44(4), 748–756. https://doi.org/10.1111/j.1365-2621.2008.01892.x .Ghanem, N., Mihoubi, D., Kechaou, N., & Mihoubi, N. B. (2012). Microwave dehydration of three citrus peel cultivars: effect on water and oil retention capacities, color, shrinkage and total phenols content. Industrial Crops and Products, 40, 167–177. https://doi.org/10.1016/j.indcrop.2012.03.009 .Gómez, A., López, R., Esturo, A., Bald, C., Tueros, I., Talens, C., & Raynaud, C. (2015). From waste products to raw materials for the development of new foods. Proceedings of the Institution of Civil Engineers: Waste and Resource Management, 168(2), 55–62. https://doi.org/10.1680/warm.13.00038 .Hossain, M. D., Bala, B. K., Hossain, M. A., & Mondol, M. R. A. (2001). Sorption isotherms and heat of sorption of pineapple. Journal of Food Engineering, 48(2), 103–107. https://doi.org/10.1016/s0260-8774(00)00132-1 .Igual, M., Contreras, C., & Martinez-Navarrete, N. (2010). Non-conventional techniques to obtain grapefruit jam. Innovative Food Science & Emerging Technologies, 11(2), 335–341. https://doi.org/10.1016/j.ifset.2010.01.009 .Kowalski, S. J., Rajewska, K., & Rybicki, A. (2005). Stresses generated during convective and microwave drying. Drying Technology, 23(9–11), 1875–1893. https://doi.org/10.1080/07373930500210226 .Labuza, T. P., & Altunakar, B. (2007). Water activity prediction and moisture sorption isotherms. In G. V. Barbosa-Cánovas, A. J. Fontana, S. J. Schmidt, & T. P. Labuza (Eds.), Water Activity in Foods: Fundamentals and Applications (Vol. 109–154). Iowa: IFT Press and Blackwell Publishing. https://doi.org/10.1002/9780470376454.ch5 .Larrauri, J. A. (1999). New approaches in the preparation of high dietary fibre powders from fruit by-products. Trends in Food Science & Technology, 10(1), 3–8. https://doi.org/10.1016/S0924-2244(99)00016-3 .Martín, M. E., Martínez-Navarrete, N., Chiralt, A., & Fito, P. (2003). Diseño y construcción de una instalación experimental para el estudio de la cinética de secado combinado por aire caliente y microondas. Alimentación Equipos y Tecnología, 22(181), 101–107.Quirijns, E. J., van Boxtel, A. J. B., van Loon, W. K. P., & van Straten, G. (2005). Sorption isotherms, GAB parameters and isosteric heat of sorption. Journal of the Science of Food and Agriculture, 85(11), 1805–1814. https://doi.org/10.1002/jsfa.2140 .Rizvi, S. S. H., & Benado, A. L. (1984). Thermodynamic properties of dehydrated foods. Food Technology, 38(3), 83–92.Robertson, J. A., de Monredon, F. D., Dysseler, P., Guillon, F., Amado, R., & Thibault, J.-F. (2000). Hydration properties of dietary fibre and resistant starch: a European collaborative study. Lebensmittel-Wissenschaft und -Technologie, 33(2), 72–79. https://doi.org/10.1006/fstl.1999.0595 .Schieber, A., Stintzing, F. C., & Carle, R. (2001). By-products of plant food processing as a source of functional compounds—recent developments. Trends in Food Science & Technology, 12(11), 401−+.Schiffmann, R. (2001). Microwave processes for the food industry. In A. Datta & R. Anantheswaran (Eds.), Handbook of microwave Technology for Food Applications (pp. 299–352). New York: Marcel Dekker.Talens, C., Castro-Giráldez, M., & Fito, P. J. (2016a). A thermodynamic model for hot-air microwave drying of orange peel. Journal of Food Engineering, 175, 33–42. https://doi.org/10.1016/j.jfoodeng.2015.12.001 .Talens, C., Castro-Giráldez, M., & Fito, P. J. (2016b). Study of the effect of microwave power coupled with hot air drying on orange peel by dielectric spectroscopy. LWT - Food Science and Technology, 66, 622–628. https://doi.org/10.1016/j.lwt.2015.11.015 .Talens, C., Arboleya, J. C., Castro-Giraldez, M., & Fito, P. J. (2017). Effect of microwave power coupled with hot air drying on process efficiency and physico-chemical properties of a new dietary fibre ingredient obtained from orange peel. LWT - Food Science and Technology, 77, 110–118. https://doi.org/10.1016/j.lwt.2016.11.036 .Traffano-Schiffo, M. V., Castro-Giráldez, M., Fito, P. J., & Balaguer, N. (2014). Thermodynamic model of meat drying by infrared thermography. Journal of Food Engineering, 128, 103–110. https://doi.org/10.1016/j.jfoodeng.2013.12.024 .Traffano-Schiffo, M. V., Castro-Giráldez, M., Colom, R. J., & Fito, P. J. (2015). Study of the application of dielectric spectroscopy to predict the water activity of meat during drying process. Journal of Food Engineering, 166, 285–290. https://doi.org/10.1016/j.jfoodeng.2015.06.030 .van den Berg, C., & Bruin, S. (1981). Water activity and its estimation in food systems—theoretical aspects. In L. B. Rockland & G. F. Stewart (Eds.), Water Activity: Influences on Food Quality (pp. 1–61). New York: Academic Press. https://doi.org/10.1016/B978-0-12-591350-8.50007-3 .Waldron, K. W. (2009). Part III exploitation of co-products as food and feed ingredients. In K. W. Waldron (Ed.), Handbook of waste management and co-product recovery in food processing (pp. 255–265). UK: Elsevier Science. https://doi.org/10.1533/9781845697051 .Yan, Z., Sousa-Gallagher, M. J., & Oliveira, F. A. R. (2008). Sorption isotherms and moisture sorption hysteresis of intermediate moisture content banana. Journal of Food Engineering, 86(3), 342–348. https://doi.org/10.1016/j.jfoodeng.2007.10.009

Development of a methodology to categorize poultry meat affected by deep pectoral myopathy

[EN] The growth of poultry production has led to an increase in the incidence of internal defects in chicken and turkey broilers, such as Deep Pectoral Myopathy (DPM). DPM is an ischemic hemorrhage or necrosis caused by the inadequate blood supply of Pectoralis minor and major muscles. Currently, visual appearance is the only parameter used to categorize the damage level. The aim of this research was to develop a scientific methodology to determine the level of damage in poultry breast tenders affected by this myopathy. For this purpose, microstructure, pH, protein and ion contents, and color were studied. Results allowed identifying three damage levels: normal, hemorrhagic samples with hematomas and blood clots, and necrotic tissues, based on significant variables (p < .05) measured in Pectoralis minor (pH, L* and a*), where muscles with myopathy presented L* values lower than 47, and necrotic muscles presented pH values higher than 6.05. Practical applications The appearance of defects in chicken meat is a growing problem due to the intensive genetic selection and the fast growth rate that the poultry industry demands. This research provides a scientific methodology, based on biochemical and physicochemical parameters of muscle tissue metabolism, and develops and validates a categorization for deep pectoral myopathy in broilers based on the level of muscle damage. This work, provides an objective and scientific methodology, and coupled with the work published in Traffano-Schiffo et al. (2018) and patented, will allow detecting, identifying, and characterizing chickens that have suffered deep pectoral myopathy and the degree of damage.Ministerio de Economia, Industria y Competitividad, Gobierno de Espana, Grant/Award Number: AGL2016-80643-R; European Regional Development FundTraffano-Schiffo, MV.; Chuquizuta, T.; Castro Giraldez, M.; Fito, PJ. (2021). Development of a methodology to categorize poultry meat affected by deep pectoral myopathy. Journal of Food Processing and Preservation. 45(3):1-9. https://doi.org/10.1111/jfpp.15226S1945

Encapsulation of lactase in Ca(II)-alginate beads: Effect of stabilizers and drying methods

[EN] The purpose of the present work was to analyze the effect of trehalose, arabic and guar gums on the preservation of beta-galactosidase activity in freeze-dried and vacuum dried Ca(II)-alginate beads. Freezing process was also studied as a first step of freeze-drying. Trehalose was critical for beta-galactosidase conservation, and guar gum as a second excipient showed the highest conservation effect (close to 95%). Systems with T-g values similar to 40 degrees C which were stables at ambient temperature were obtained, being trehalose the main responsible of the formation of an amorphous matrix. Vacuum dried beads showed smaller size (with Feret's diameter below 1.08 +/- 0.09 mm), higher circularity (reaching 0.78 +/- 0.06) and large cracks in their surface than freeze-dried beads, which were more spongy and voluminous. Ice crystallization of the beads revealed that the crystallization of Ca(II)-alginate system follows the Avrami kinetics of nucleation and growth. Particularly, Ca(II)-alginate showed an Avrami index of 2.03 +/- 0.07, which means that crystal growing is bidimensional. Neither the addition of trehalose nor gums affected the dimension of the ice growing or its rate. These results open an opportunity in the development of new lactic products able to be consumed by lactose intolerance people.This work was supported by Universidad de Buenos Aires (UBACyT 20020130100610BA), Agencia Nacional de Promoción Científica y Tecnológica (ANPCyT PICT 2013 0434 and 2013 1331), CIN-CONICET (PDTS 2015 n° 196). The author María Victoria Traffano Schiffo wants to thank Programa para la Formación de Personal Investigador (FPI) Pre-doctoral Program of the Universitat Politècnica de València (UPV) for support her PhD studies and also her mobility to Argentina.Traffano-Schiffo, MV.; Castro Giraldez, M.; Fito Suñer, PJ.; Santagapita, P. (2017). Encapsulation of lactase in Ca(II)-alginate beads: Effect of stabilizers and drying methods. Food Research International. 100(1):296-303. https://doi.org/10.1016/j.foodres.2017.07.020S296303100

New sensor to measure the microencapsulated active compounds released in an aqueous liquid media based in dielectric properties in radiofrequency range

[EN] In recent years, the general and scientific interest in nutrition, digestion, and what role they play in our body has increased, and there is still much work to be carried out in the field of developing sensors and techniques that are capable of identifying and quantifying the chemical species involved in these processes. Iron deficiency is the most common and widespread nutritional disorder that mainly affects the health of children and women. Iron from the diet may be available as heme or organic iron, or as non-heme or inorganic iron. The absorption of non-heme iron requires its solubilization and reduction in the ferric state to ferrous that begins in the gastric acid environment, because iron in the ferric state is very poorly absorbable. There are chemical species with reducing capacity (antioxidants) that also have the ability to reduce iron, such as ascorbic acid. This paper aims to develop a sensor for measuring the release of encapsulated active compounds, in different media, based on dielectric properties measurement in the radio frequency range. An impedance sensor able to measure the release of microencapsulated active compounds was developed. The sensor was tested with calcium alginate beads encapsulating iron ions and ascorbic acid as active compounds. The prediction and measurement potential of this sensor was improved by developing a thermodynamic model that allows obtaining kinetic parameters that will allow suitable encapsulation design for subsequent release.This research was funded by Spanish AGENCIA ESTATAL DE INVESTIGACIÓN, grant number PID2020-116816RB-I00.Tomas-Egea, JA.; Fito, PJ.; Colom Palero, RJ.; Castro Giraldez, M. (2021). New sensor to measure the microencapsulated active compounds released in an aqueous liquid media based in dielectric properties in radiofrequency range. Sensors. 21(17):1-15. https://doi.org/10.3390/s21175781S115211

Innovative photonic system in radiofrequency and microwave range to determine chicken meat quality

[EN] Nowadays, one of the most important challenges of poultry industry is to determine individually the meat quality class (pale, soft and exudative, normal and dark, firm and dry meats) by non-invasive, accurate and fast technique. For this purpose, dielectric spectra in radiofrequency and microwave ranges were studied. In radiofrequency range, the permittivity was measured by a non-destructive sensor conformed by three points with blunt-ended electrodes connected to an Agilent 4294A impedance analyser, and in microwave range an Agilent 85070E open-ended coaxial probe connected to an Agilent E8362B Vector Network Analyser were used. This work demonstrates the direct relation between the pH evolution and the dielectric constant at ¿-dispersion, and also, that the main structural proteins degradation has direct relation with the dielectric constant at ßdispersion, being possible to segregate meat depending on the level of protein degradation. Finally, this paper ends with a classification model for quality poultry meat based on a photonic analysis at radiofrequency range by using the Traffano-Schiffo modelThe authors acknowledge the financial support from: the Spanish Ministerio de Economia, Industria y Competitividad, Programa Estatal de I + D + i orientada a los Retos de la Sociedad AGL2016-80643-R, Agencia Estatal de Investigacion (AEI) and Fondo Europeo de Desarrollo Regional. The author Maria Victoria Traffano Schiffo wants to thank the FPI Predoctoral Program of the Universidad Politecnica de Valencia for its support.Traffano-Schiffo, MV.; Castro Giraldez, M.; Colom Palero, RJ.; Fito Suñer, PJ. (2018). Innovative photonic system in radiofrequency and microwave range to determine chicken meat quality. Journal of Food Engineering. 239:1-7. https://doi.org/10.1016/j.jfoodeng.2018.06.029S1723

Hot Air and Microwave Combined Drying of Potato Monitored by Infrared Thermography

[EN] Hot air drying (HAD) at temperatures below the spontaneous evaporation temperature could be combined with microwave (MW) radiation as a thermal energy source in order to reduce the drying time. A photon flux in the microwave range interacts with dipolar molecules (water) through orientation and induction, producing electrical energy storage and thermal energy accumulation and generating an increase in the internal energy of food. The different mechanisms involved in water transport could change when the microwave penetration depth exceeds the sample characteristic dimension of mass transport. The aim of this paper is to determine the effect of MW in the combined HAD-MW drying of raw potato in order to obtain the real driving forces and mechanisms involved in the water transport, with the purpose of optimizing the MW power used. For this purpose, combined drying was carried out on potato samples (0, 4 and 6 W/g). The sample surface temperature was monitored by infrared thermography, and the sample mass was measured continuously through a precision balance. In parallel with continuous drying, another drying treatment was performed at different times (20, 40, 60, 90, 120, 180, 420 min) and conditions (0, 4 and 6 W/g) to analyze the dielectric properties, mass, moisture, volume and water activity. The results show that it is possible to monitor combined drying by infrared thermography, and it can be concluded that the convection heating is mostly transformed into surface water evaporation, with negligible thermal conduction from the surface, and microwave radiation is mostly transformed into an increase in the potato's internal energy.The authors acknowledge the financial support from THE SPANISH MINISTERIO DE ECONOMÍA, INDUSTRIA Y COMPETITIVIDAD, Programa Estatal de I+D+i orientada a los Retos de la Sociedad AGL2016-80643-R, Agencia Estatal de Investigación (AEI) and Fondo Europeo de Desarrollo Regional (FEDER). Juan Ángel Tomás-Egea wants to thank the FPI Predoctoral Program of the Universitat Politècnica de València for its support.Tomas-Egea, JA.; Traffano-Schiffo, MV.; Castro Giraldez, M.; Fito Suñer, PJ. (2021). Hot Air and Microwave Combined Drying of Potato Monitored by Infrared Thermography. Applied Sciences. 11(4):1-12. https://doi.org/10.3390/app11041730S112114Traffano-Schiffo, M. V., Castro-Giráldez, M., Fito, P. J., & Balaguer, N. (2014). Thermodynamic model of meat drying by infrarred thermography. Journal of Food Engineering, 128, 103-110. doi:10.1016/j.jfoodeng.2013.12.024Dehghannya, J., Kadkhodaei, S., Heshmati, M. K., & Ghanbarzadeh, B. (2019). Ultrasound-assisted intensification of a hybrid intermittent microwave - hot air drying process of potato: Quality aspects and energy consumption. Ultrasonics, 96, 104-122. doi:10.1016/j.ultras.2019.02.005Turkan, B., Canbolat, A. S., & Etemoglu, A. B. (2019). Numerical Investigation of Multiphase Transport Model for Hot-Air Drying of Food. Tarım Bilimleri Dergisi, 518-529. doi:10.15832/ankutbd.441925Cuibus, L., Castro-Giráldez, M., Fito, P. J., & Fabbri, A. (2014). Application of infrared thermography and dielectric spectroscopy for controlling freezing process of raw potato. Innovative Food Science & Emerging Technologies, 24, 80-87. doi:10.1016/j.ifset.2013.11.007Castro-Giráldez, M., Fito, P. J., & Fito, P. (2011). Nonlinear thermodynamic approach to analyze long time osmotic dehydration of parenchymatic apple tissue. Journal of Food Engineering, 102(1), 34-42. doi:10.1016/j.jfoodeng.2010.07.032Talens, C., Castro-Giraldez, M., & Fito, P. J. (2016). A thermodynamic model for hot air microwave drying of orange peel. Journal of Food Engineering, 175, 33-42. doi:10.1016/j.jfoodeng.2015.12.001Markx, G. H., & Davey, C. L. (1999). The dielectric properties of biological cells at radiofrequencies: applications in biotechnology. Enzyme and Microbial Technology, 25(3-5), 161-171. doi:10.1016/s0141-0229(99)00008-3Miraei Ashtiani, S.-H., Sturm, B., & Nasirahmadi, A. (2017). Effects of hot-air and hybrid hot air-microwave drying on drying kinetics and textural quality of nectarine slices. Heat and Mass Transfer, 54(4), 915-927. doi:10.1007/s00231-017-2187-0Dehghannya, J., Bozorghi, S., & Heshmati, M. K. (2017). Low temperature hot air drying of potato cubes subjected to osmotic dehydration and intermittent microwave: drying kinetics, energy consumption and product quality indexes. Heat and Mass Transfer, 54(4), 929-954. doi:10.1007/s00231-017-2202-5Swain, S., Samuel, D. V. K., Bal, L. M., Kar, A., & Sahoo, G. P. (2012). Modeling of microwave assisted drying of osmotically pretreated red sweet pepper (Capsicum annum L.). Food Science and Biotechnology, 21(4), 969-978. doi:10.1007/s10068-012-0127-9Talens, C., Castro-Giraldez, M., & Fito, P. J. (2017). Effect of Microwave Power Coupled with Hot Air Drying on Sorption Isotherms and Microstructure of Orange Peel. Food and Bioprocess Technology, 11(4), 723-734. doi:10.1007/s11947-017-2041-xWang, Q., Li, S., Han, X., Ni, Y., Zhao, D., & Hao, J. (2019). Quality evaluation and drying kinetics of shitake mushrooms dried by hot air, infrared and intermittent microwave–assisted drying methods. LWT, 107, 236-242. doi:10.1016/j.lwt.2019.03.020Glowacz, A. (2021). Fault diagnosis of electric impact drills using thermal imaging. Measurement, 171, 108815. doi:10.1016/j.measurement.2020.108815Gonçalves, B. J., Giarola, T. M. de O., Pereira, D. F., Vilas Boas, E. V. de B., & de Resende, J. V. (2015). Using infrared thermography to evaluate the injuries of cold-stored guava. Journal of Food Science and Technology, 53(2), 1063-1070. doi:10.1007/s13197-015-2141-4Gowen, A. A., Tiwari, B. K., Cullen, P. J., McDonnell, K., & O’Donnell, C. P. (2010). Applications of thermal imaging in food quality and safety assessment. Trends in Food Science & Technology, 21(4), 190-200. doi:10.1016/j.tifs.2009.12.002Costa, N., Stelletta, C., Cannizzo, C., Gianesella, M., Lo Fiego, P., & Morgante, M. (2007). The use of thermography on the slaughter-line for the assessment of pork and raw ham quality. Italian Journal of Animal Science, 6(sup1), 704-706. doi:10.4081/ijas.2007.1s.704Tao, Y. (2000). Combined IR imaging-neural network method for the estimation of internal temperature in cooked chicken meat. Optical Engineering, 39(11), 3032. doi:10.1117/1.1314595J. G. Ibarra, Y. Tao, A. J. Cardarelli, & J. Shultz. (2000). COOKED AND RAW CHICKEN MEAT: EMISSIVITY IN THE MID-INFRARED REGION. Applied Engineering in Agriculture, 16(2), 143-148. doi:10.13031/2013.5060Gan-Mor, S., Regev, R., Levi, A., & Eshel, D. (2011). Adapted thermal imaging for the development of postharvest precision steam-disinfection technology for carrots. Postharvest Biology and Technology, 59(3), 265-271. doi:10.1016/j.postharvbio.2010.10.003Baranowski, P., Mazurek, W., Wozniak, J., & Majewska, U. (2012). Detection of early bruises in apples using hyperspectral data and thermal imaging. Journal of Food Engineering, 110(3), 345-355. doi:10.1016/j.jfoodeng.2011.12.038Zhou, X., Ramaswamy, H., Qu, Y., Xu, R., & Wang, S. (2019). Combined radio frequency-vacuum and hot air drying of kiwifruits: Effect on drying uniformity, energy efficiency and product quality. Innovative Food Science & Emerging Technologies, 56, 102182. doi:10.1016/j.ifset.2019.102182Su, D., Lv, W., Wang, Y., Li, D., & Wang, L. (2019). Drying characteristics and water dynamics during microwave hot-air flow rolling drying of Pleurotus eryngii. Drying Technology, 38(11), 1493-1504. doi:10.1080/07373937.2019.1648291Wei, S., Wang, Z., Wang, F., Xie, W., Chen, P., & Yang, D. (2019). Simulation and experimental studies of heat and mass transfer in corn kernel during hot air drying. Food and Bioproducts Processing, 117, 360-372. doi:10.1016/j.fbp.2019.08.006Pu, Y.-Y., Zhao, M., O’Donnell, C., & Sun, D.-W. (2018). Nondestructive quality evaluation of banana slices during microwave vacuum drying using spectral and imaging techniques. Drying Technology, 36(13), 1542-1553. doi:10.1080/07373937.2017.141592

Gums induced microstructure stability in Ca(II)-alginate beads containing lactase analyzed by SAXS

[EN] Previous works show that the addition of trehalose and gums in ß-galactosidase (lactase) Ca(II)-alginate encapsulation systems improved its intrinsic stability against freezing and dehydration processes in the pristine state. However, there is no available information on the evolution in microstructure due to the constraints imposed by the operational conditions. The aim of this research is to study the time course of microstructural changes of Ca(II)-alginate matrices driven by the presence of trehalose, arabic and guar gums as excipients and to discuss how these changes in¿uence the di¿usional transport (assessed by LF-NMR) and the enzymatic activity of the encapsulated lactase. The structural modi¿cations at di¿erent scales were assessed by SAXS. The incorporation of gums as second excipients induces a signi¿cant stabilization in the microstructure not only at the rod scale, but also in the characteristic size and density of alginate dimers (basic units of construction of rods) and the degree of interconnection of rods at a larger scale, improving the performance in terms of lactase activity.This work was supported by the Brazilian Synchrotron Light Laboratory (LNLS, Brazil, proposal SAXS1-20160278), Universidad de Buenos Aires (UBACyT 20020130100610BA), Agencia Nacional de Promocion Cientifica y Tecnologica (ANPCyT PICT 2013 0434 and 2013 1331), CIN-CONICET (PDTS 2015 no 196), and Consejo Nacional de Investigaciones Cientificas y Tecnicas. The author Maria Victoria Traffano-Schiffo wants to thank "Programa para la Formacion de Personal Investigador (FPI)" Pre-doctoral Program of the Universitat Politecnica de Valencia (UPV) for support her PhD studies and also her mobility to Argentina.Traffano-Schiffo, MV.; Castro Giraldez, M.; Fito Suñer, PJ.; Perullini, M.; Santagapita, PR. (2018). Gums induced microstructure stability in Ca(II)-alginate beads containing lactase analyzed by SAXS. Carbohydrate Polymers. 179:402-407. https://doi.org/10.1016/j.carbpol.2017.09.096S40240717

Effect of pulsed electric fields pre-treatment on mass transport during the osmotic dehydration of organic kiwifruit

[EN] Recently, some authors have applied pulsed electric fields (PEF) as a pre-treatment of osmotic dehydration, showing a faster kinetics of dehydration. Osmotic dehydration of fruit tissue shows complex mass transfer mechanism associated with active and passive transports of the vegetal matrix, usually driven by electrolytes. The aim of this work was to analyze the effect of different PEF values (100, 250, 400 V/cm) as a pre-treatment of the osmotic dehydration (61.5°Brix, up to 120 min) on mass transport mechanism of organic kiwifruit. A thermodynamic model able to describe the mass transfer and tissue deformation in kiwifruit was developed. It was possible to conclude that pulsed electric field as a pre-treatment, remove a part of the native electrolytes, reducing the activity of protein active pumps, leaving alone the passive protein channels as a main mass transmembrane transport and therefore affecting to the regular functionality of cell homeostasis system.The authors Urszula Tylewicz and Marco Dalla Rosa want to thank for the financial support of this project provided by funding bodies within the FP7 ERA-Net CORE Organic Plus, and with cofunds from the European Commission (this project has received funding from the European Union's 7th Framework Programme under grant agreement No 618107.). The author Marta Castro-Giraldez wants to thank the UPV Postdoctoral Program (PAID-10-14) of the Universidad Politecnica de Valencia for its support. The author Maria Victoria Traffano Schiffo wants to thank the FPI Predoctoral Program of the Universidad Politecnica de Valencia for support her PhD studies, ERASMUS PRACTICAS program to finance her mobility to Italy and also Silvia Tappi and Wei Luo for their cooperation during the experiment.Traffano-Schiffo, MV.; Tylewicz, U.; Castro Giraldez, M.; Fito Suñer, PJ.; Ragni, L.; Dalla Rosa, M. (2016). Effect of pulsed electric fields pre-treatment on mass transport during the osmotic dehydration of organic kiwifruit. Innovative Food Science & Emerging Technologies. 38:243-251. https://doi.org/10.1016/j.ifset.2016.10.011S2432513

Development of a non-destructive detection system of Deep Pectoral Myopathy in poultry by dielectric spectroscopy

[EN] The trend in meat consumption has changed drastically in the last years, mainly due to the relationship of red and processed meats with cancer and cardiovascular diseases, which has caused a substantial growth in poultry meat consumption, 8% in 2016. Therefore, poultry production has suffered an intensification that has led to an increase in the incidence of internal malformations in chickens and turkeys for fattening, especially in the pectoral muscles, as Deep Pectoral Myopathy (DPM). Currently, industry is not able to detect DPM breasts when sold as whole carcasses. In this context, the use of dielectric spectroscopy, complemented by a deep study of the chemical, biochemical and microstructural transformations of the muscle and the effect that these changes have on the electrical dispersions in radiofrequency range, may become feasible for online DPM detection. For this paper, non-damaged and affected by DPM chicken breasts (pectoralis major and pectoralis minor) was analysed. Permittivity in radiofrequency and microwave ranges were measured in the different tissues: pectoralis minor, major and skin in order to characterize them. Moreover, proteins content, ion content and pH were measured. With this data, a sensor for measuring the permittivity of chicken whole carcass with skin was developed; it consists of two pairs of two flat plates sensor connected to an impedance Agilent analyzer 4294A and can measure the permittivity from 40 Hz to 1 MHz. The results demonstrated the feasibility of the permittivity in radiofrequency range as an potential identification technique of chicken breasts affected by DPM.The authors acknowledge the financial support from: the Spanish Ministerio de Economia, Industria y Competitividad, Programa Estatal de I+D+i orientada a los Retos de la Sociedad AGL2016-80643-R, Agencia Estatal de Investigacion (AEI) and Fondo Europeo de Desarrollo Regional (FEDER). Maria Victoria Traffano Schiffo wants to thank the FPI Predoctoral Program of the Universidad Politecnica de Valencia for its support. The authors would like to thank the Electronic Microscopy Service of the Universidad Politecnica de Valencia for its assistance in the use of Cryo-SEM and Nutreco corporation for their collaboration with the research.Traffano-Schiffo, MV.; Castro Giraldez, M.; Herrero Bosch, V.; Colom Palero, RJ.; Fito Suñer, PJ. (2018). Development of a non-destructive detection system of Deep Pectoral Myopathy in poultry by dielectric spectroscopy. Journal of Food Engineering. 237:137-145. https://doi.org/10.1016/j.jfoodeng.2018.05.023S13714523