FORMULATION AND CHARACTERIZATION OF POLOXAMER 407 (R): THERMOREVERSIBLE GEL CONTAINING POLYMERIC MICROPARTICLES AND HYALURONIC ACID

The influence of the composition and preparation method on the sol-gel transition temperature (Tsol-gel) and rheological response of poloxamer-based formulations was determined. Manual and more complex mechanical stirring were found to provide similar results. In addition, a linear dependence of Tsol-gel on the poloxamer content was observed in the range of concentrations analyzed, and a Poloxamer 407® concentration of 18% was selected. The addition of hyaluronic acid did not lead to significant changes in the Tsol-gel values. In contrast, the addition of microparticles caused a reduction in Tsol-gel without a significant reduction in gel strength, and pseudoplastic characteristics were observed, indicating that a thermoreversible gel was obtained with a rheology suitable for application in the treatment of burn wounds

Rheological, Textural and Flavour Properties of Yellow Mustard Sauce as Affected by Modified Starch, Xanthan and Guar Gum

Influence of a modified starch-gum thickening system on the rheological, textural and flavour properties of yellow mustard sauce was studied. The rheological measurements indicated that the sauces exhibited a weak gel-like, strong shear thinning behaviour. Dynamic viscoelasticity measurements showed that the sauces with modified starch (MS) and xanthan gum (XG) presented superior viscoelastic properties to those with MS and guar gum (GG) samples. All tested sauces showed non-Newtonian, pseudoplastic and thixotropic fluids characteristics. Parameters such as hardness, springiness, cohesiveness, gumminess and spreadability were used to evaluate the textural properties, and the results indicated that MS/XG was more influential than MS/GG on the textural properties. Sensory analysis suggested that 0.4 % MS/0.3 % XG, 0.4 % MS/0.4 % XG and 0.4 % MS/0.4 % GG were superior thickeners for the yellow mustard sauces. The flavours of these three sample groups with the highest sensory scores and a sample with only MS were analysed by an electronic nose, which showed that the electronic nose was able to distinguish their differences

Aroma, Sugar and Anthocyanin Profile of Fruit and Seed of Mahlab (Prunus mahaleb L.): Optimization of Bioactive Compounds Extraction by Simplex Lattice Mixture Design

In the present study, bioactive properties of black mahlab fruit and seed were investigated. Simplex lattice mixture design was used to determine the best solvent composition for the extraction of bioactive compounds of the samples. The content of total phenolics, total flavonoids, condensed tannins, total anthocyanins, and antiradical efficiency of mahlab fruit and seed extracts were investigated by spectrophotometric methods. Moreover, major sugar composition, individual anthocyanins, fatty acids, and aroma profile of the samples were determined by chromatographic methods. Effect of temperature on degradation of anthocyanins was also investigated, and degradation kinetic model parameters were calculated. Finally, the constructed simplex lattice mixture design model was optimized to estimate the optimum solvent mixtures that would yield maximum total phenolic content. The best solvent mixture was found to be 36% of acetone and 64% of water. It was concluded that the experimental and predicted values were in good agreement. Total phenolics and flavonoids of the fruit were 2,266 mg gallic acid equivalent/100 g of dry sample and 946.57mg catechin equivalent/100 g of dry sample, respectively. Total anthocyanin content of the fruit was 505.7 mg/100 g of dry sample. Temperature showed a significant degradation effect on the anthocyanins