Effect of different artificial aging protocolson fluorescence of resin composites

This study evaluated the effect of different artificial aging on fluorescence of resin composites. Forty-fivecylindrical specimens (6mm in diameter and 1mm thick) were made of each resin composite: IPS EmpressDirect, Filtek™ Z350 XT, and Durafill. A baseline measurement of fluorescence by the direct method usingthe fluorescence spectrophotometer RF-5301 PC was performed. After, resin specimens were divided into 3groups according to artificial aging protocol to be submitted: (1) aging by mechanical brushing: 30,000cycles were performed, with fluorescence measurements after 10,000, 20,000 and 30,000 cycles; (2)chemical aging by ethanol: the samples were immersed in ethanol for 15 days, with measurements after 5, 10and 15 days of immersion; (3) light aging: resin specimens were subjected to UV radiation for 216h withfluorescence readings after 72, 144, 216h. Data were submitted to one-way repeated measures ANOVA andTukey’s test (α=0.05). Baseline fluorescence of the tested resins was ranked in this ascending order: Durafill Filtek Z350 XT IPS Empress Direct. Simulated toothbrushing and ethanol immersion reduced fluorescence,except for Z350 XT. For light exposition, fluorescence was reduced after 100h for Empress Direct andDurafill, while a reduction after 100h and 200h was detected for Z350 XT. Artificial aging protocolsinfluenced the fluorescence and that this phenomenon is material dependent. In general, the fluorescence isreduced with aging.Keywords: composite resin, aging, fluorescence

Influence of cavosurface angle on the stress concentration and gaps formation in class V resin composite restorations

The study aimed to evaluate the influence of cavosurface angle on stress concentration and gap formation in class V restorations. Cylindrical cavities 3 mm in diameter were prepared in forty-five bovine incisors, changing only the angle of the bur in relation to the flat surface of the tooth. The cavities maintained the same volume (17.67 mm³). The samples were divided according to the cavosurface angle, into three groups (n = 15): 90°, 120°, 135°. After adhesive application (Futurabond U, VOCO), the cavity was filled with bulk placement of a resin composite (GrandioSO, VOCO). The teeth were analyzed with stereomicroscopy. Data of marginal gap formation were statistically analyzed with a one-way analysis of variance (ANOVA) followed by Tukey tests (significance level: α = 0.05). Finite element analysis (FEA) was used to study residual stress in these geometries and to correlate those stresses with experimentally measured gap formation. The elastic modulus and polymerization shrinkage were determined for FEA. Residual shrinkage stresses were expressed in maximum principal stress (MPS). There was a significant difference in the gap formation among the groups (p = 0.001). A significantly lower marginal gap formation was found for 120° and 135° angles, with no significant difference between them. The cavosurface angle at 90° caused substantially higher stresses, in the restoration interface, with greater marginal gap. For the 120° and 135° angles, the stress concentrations were smaller and were located in the dental structure. The cavosurface angle influenced the marginal gap formation and stress concentration

Polymerization shrinkage stresses in different restorative techniques for non-carious cervical lesions

Objective This study evaluated the effect of different restorative techniques for non-carious cervical lesions (NCCL) on polymerization shrinkage stress of resins using three-dimensional (3D) finite element analysis (FEA). Methods 3D-models of a maxillary premolar with a NCCL restored with different filling techniques (bulk filling and incremental) were generated to be compared by nonlinear FEA. The bulk filling technique was used for groups B (NCCL restored with Filtek™ Bulk Fill) and C (Filtek™ Z350 XT). The incremental technique was subdivided according to mode of application: P (2 parallel increments of the Filtek™ Z350 XT), OI (2 oblique increments of the Filtek™ Z350 XT, with incisal first), OIV (2 oblique increments of the Filtek™ Z350 XT, with incisal first and increments with the same volume), OG (2 oblique increments of the Filtek™ Z350 XT, with gingival first) and OGV (2 oblique increments of the Filtek™ Z350 XT, with gingival first and increments with the same volume), resulting in 7 models. All materials were considered isotropic, elastic and linear. The results were expressed in maximum principal stress (MPS). Results The tension stress distribution was influenced by the restorative technique. The lowest stress concentration occurred in group B followed by OG, OGV, OI, OIV, P and C; the incisal interface was more affected than the gingival. Conclusion The restoration of NCCLs with bulk fill composite resulted in lower shrinkage stress in the gingival and incisal areas, followed by incremental techniques with the initial increment placed on the gingival wall. Clinical significance The non-carious cervical lesions (NCCLs) restored with bulk fill composite have a more favorable biomechanical behavior

Cianoacrilato na colagem de Bráquetes ortodônticos em resina acrílica: há maior adesão?

Pacientes em tratamento ortodôntico apresentam restaurações provisórias com frequência. No entanto, poucos estudos avaliam a influência dos adesivos na resistência ao cisalhamento dos bráquetes nessas superfícies. A resina acrílica é comumente indicada para colagem de bráquetes, porém o uso do cianoacrilato como adesivo ortodôntico é uma opção analisada. O objetivo do presente trabalho foi avaliar o desempenho do cianoacrilato associado aos materiais comumente utilizados para a fixação de bráquetes metálicos em restaurações provisórias de resina acrílica. Quarenta amostras em resina acrílica foram preparadas e as superfícies homogeinizadas com lixas de carboneto de silício (320 e 600). Em seguida, as amostras foram divididas aleatoriamente em quatro grupos (n=10) com base no tratamento de superfície e agente de união: G1 - bráquetes colados com resina acrílica; G2 - bráquetes colados com resina acrílica e aplicação de cianoacrilato; G3 - bráquetes colados com Transbond(tm) XT; G4 - bráquetes colados com Transbond(tm) XT e aplicação de cianoacrilato. Foram utilizados bráquetes ortodônticos de aço inoxidável, prescrição Roth, Kirium (3M/Abzil) para incisivos centrais superiores direitos, slot 022. Após colagem, as amostras foram submetidas ao teste de cisalhamento a uma velocidade de 0,5mm/min em uma máquina de ensaios universal (EMIC DL-1000). Os dados foram coletados e submetidos à análise estatística pelo teste ANOVA com nível de significância de 5%. A associação de resina acrílica ao cianoacrilato (G2) resultou na maior resistência ao cisalhamento (13,76 MPa), mas não significativa em comparação aos valores obtidos para a resina acrílica (G1= 7,76 MPa). O mesmo pôde ser observado para a associação Transbond(tm) XT e cianoacrilato (G4= 4,03 MPa) em relação a utilização da Transbond(tm) XT de forma isolada (G3= 3,87 MPa) e resina acrílica. O tratamento de superfície tem efeito significativo na resistência da união dos bráquetes colados aos materiais provisórios. A associação de cianoacrilato ao monômero de metilmetacrilato apresentou maior resistência ao cisalhamento, sendo mais indicada clinicamente

Efeito da intensidade de fontes de luz e barreiras de cerâmica na microdureza de cimento resinoso dual

ResumoIntroduçãoO cimento resinoso dual é o principal material para cimentação de cerâmicas. Contudo, fatores, como fonte de luz, podem influenciar no desempenho do cimento.ObjetivoAvaliar a influência de duas fontes de luz de diferentes intensidades sobre a microdureza de um cimento resinoso quando fotoativado sob diferentes cerâmicas.Material e métodoForam fotoativados 40 espécimes de cimento resinoso dual (10 mm × 1,0 mm) por meio de duas fontes de luz LED, com intensidades de 1.000 mW/cm² e 800 mW/cm² durante 40 segundos, sob cerâmicas (15 mm × 2 mm) à base de zircônia, espinélio MgAl2O4 e dissilicato de lítio. No grupo controle, foi utilizada uma placa de vidro de mesma dimensão. As amostras tiveram a superfície regularizada com lixa d`água (600 e 1200). Após armazenagem a seco no escuro (24 h), foram realizadas as medidas de microdureza Vickers (HMV Shimadzu - 50g/10 segundos). Os dados foram submetidos à Anova fatorial e ao teste de Tukey com nível de significância de 5%.ResultadoO cimento polimerizado apresentou valor médio de microdureza e desvio padrão para o grupo controle de 43,9±1,5 e 43,4±1,3, para as intensidades de 1.000 mW/cm2 e 800 mW/cm2, respectivamente. O menor valor de microdureza do cimento foi observado para a cerâmica à base de espinélio MgAl2O4, polimerizado a 800 mW/cm², com valor de 34,3±3,3.ConclusãoO tipo de cerâmica e a intensidade da fonte de luz influenciam na microdureza do cimento. A intensidade de 1.000 mW/cm2 sobre as cerâmicas à base de zircônia e espinélio MgAl2O4 resultaram na melhor combinação de valores de dureza do cimento.</sec

Influence of bulk-fill restoration on polymerization shrinkage stress and marginal gap formation in class V restorations

Purpose: This study evaluated the influence of Class V cavity extension and restorative material on the marginal gap formation, before and after aging, and the theoretical polymerization shrinkage stress distribution in a tooth restoration. Methods and Materials: Class V cavities with the depth of 2 mm, cervical/incisal distance of 4 mm, and margins located in the enamel 1 mm above the cementoenamel junction were prepared in 60 bovine incisors in two mesiodistal dimensions (n=30): 2.9-mm large extension cavities (LE) or 1.4-mm small extension cavities (SE). The cavities' depths were validated using a periodontal probe, while the mesiodistal and cervical/incisal distances were measured using a stereomicroscope. After adhesive application (Clearfil SE Bond), each group was randomly divided into two groups (n=15) according to the restorative material: Filtek Z350 XT (N) or Filtek Bulk Fill Posterior (BF). The marginal gap formation between the tooth structure and the restorative material was evaluated using a stereomicroscope before and after thermocycling for 15,000 cycles (58C and 558C). Data were analyzed using repeated-measures analysis of variance (ANOVA) and Tukey test for multiple comparisons (a=0.05). A three-dimensional geometric model with the same dimensions as the experimental test was created for each cavity, and the restorations were modeled for each restorative material. In the analysis software, the finite element mesh was created with tetrahedral quadratic elements, and the polymerization shrinkage was simulated by thermal analogy. The maximum principal stress was used to express the tensile stress in the adhesive interface through colorimetric graphs. Results: For the marginal gap, the repeated-measures ANOVA revealed a significant effect only for the factors composite resin (df=1, F=4.09, p=0.04) and thermal aging (df=1, F=44.35, p,0.001). For all numerical simulations, higher stress concentration occurred at the enamel margin, and the stress peak decreased in the following sequence: LE-N (17.0 MPa). SE-N (15.0 MPa). LE-BF (9.1 MPa). SE-BF (8.2 MPa). Conclusion: Marginal gaps in the specimens fell between approximately 12 and 17 lm; however, the regular bulk-fill composite showed less gap formation and better stress distribution around the cavity margin than the regular nano-filled composite, regardless of the cavity extension