Mixed-mode cyclic debonding of adhesively bonded composite joints

A combined experimental-analytical investigation to characterize the cyclic failure mechanism of a simple composite-to-composite bonded joint is conducted. The cracked lap shear (CLS) specimens of graphite/epoxy adherend bonded with EC-3445 adhesive are tested under combined mode 1 and 2 loading. In all specimens tested, fatigue failure occurs in the form of cyclic debonding. The cyclic debond growth rates are measured. The finite element analysis is employed to compute the mode 1, mode 2, and total strain energy release rates (i.e., GI, GII, and GT). A wide range of mixed-mode loading, i.e., GI/GII ranging from 0.03 to 0.38, is obtained. The total strain energy release rate, G sub T, appeared to be the driving parameter for cyclic debonding in the tested composite bonded system

Abundances of Suprathermal Heavy Ions in CIRs during the Minimum of Solar Cycle 23

In this paper we examine the elemental composition of the 0.1-1 MeV/nucleon interplanetary heavy ions from H to Fe in corotating interaction regions (CIRs) measured by the SIT (Suprathermal Ion Telescope) instrument. We use observations taken on board the STEREO spacecraft from January 2007 through December 2010, which included the unusually long solar minimum following solar cycle 23. During this period instruments on STEREO observed more than 50 CIR events making it possible to investigate CIR ion abundances during solar minimum conditions with unprecedented high statistics. The observations reveal annual variations of relative ion abundances in the CIRs during the 2007-2008 period as indicated by the He/H, He/O and Fe/O elemental ratios. We discuss possible causes of the variability in terms of the helium focusing cone passage and heliolatitude dependence. The year 2009 was very quiet in CIR event activity. In 2010 the elemental composition in CIRs were influenced by sporadic solar energetic particle (SEP) events. The 2010 He/H and He/O abundance ratios in CIRs show large event to event variations with values resembling the SEP-like composition. This finding points out that the suprathermal SEPs could be the source population for CIR acceleration.Comment: accepted for publication in Solar Physic

Interaction of mixed mode loading on cyclic debonding in adhesively bonded composite joints

A combined experimental and analytical investigation of an adhesively-bonded composite joint was conducted to characterize the fracture mode dependence of cyclic debonding. The system studied consisted of graphite/epoxy adherends bonded with EC 3445 adhesive. Several types of specimens are tested which provide the cyclic debond growth rate measurements under various load conditions: mode 1, mixed mode 1 to 2, and mostly mode 2. This study shows that the total strain-energy-release rate is the governing factor for cyclic debonding

Characterization of Metal and Metal Alloy Films as Contact Materials in MEMS Switches

This study presents a basic step toward the selection methodology of electric contact materials for microelectromechanical systems (MEMS) metal contact switches. This involves the interrelationship between two important parameters, resistivity and hardness, since they provide the guidelines and assessment of contact resistance, wear, deformation and adhesion characteristics of MEMS switches. For this purpose, thin film alloys of three noble metals, platinum (Pt), rhodium (Rh) and ruthenium (Ru) with gold (Au), were investigated. The interrelationship between resistivity and hardness was established for three levels of alloying of these metals with gold. Thin films of gold (Au), platinum (Pt), ruthenium (Rh) and rhodium (Ru) were also characterized to obtain their baseline data for comparison. All films were deposited on silicon substrates. When Ru, Rh and Pt are alloyed with Au, their hardness generally decreases but resistivity increases. This decrease or increase was, in general, dependent upon the amount of alloying

Nanoindentation Technique for Characterizing Cantilever Beam Style RF Microelectromechanical Systems (MEMS) Switches

A nanoindentation technique was used to mechanically actuate a radio frequency micro-switch along with the measurement of contact resistance to investigate its applicability to characterize deflection and contact resistance behaviors of micro-sized cantilever beam switches. The resulting load–displacement relationship showed a discontinuity in slope when the micro-switch closed. The measured spring constants reasonably agreed with theoretical values obtained from the simple beam models. The change in contact resistance during test clearly indicated micro-switch closure but it did not coincide exactly with the physical contact between two electric contacts due to a resistive contaminated film

Cyclic debonding of adhesively bonded composites

The fatigue behavior of a simple composite to composite bonded joint was analyzed. The cracked lap shear specimen subjected to constant amplitude cyclic loading was studied. Two specimen geometries were tested for each bonded system: (1) a strap adherend of 16 plies bonded to a lap adherend of 8 plies; and (2) a strap adherend of 8 plies bonded to a lap adherend of 16 plies. In all specimens the fatigue failure was in the form of cyclic debonding with some 0 deg fiber pull off from the strap adherend. The debond always grew in the region of adhesive that had the highest mode (peel) loading and that region was close to the adhesive strap interface

Holographic single particle imaging for weakly scattering, heterogeneous nanoscale objects

Single particle imaging (SPI) at X-ray free electron lasers (XFELs) is a technique to determine the 3D structure of nanoscale objects like biomolecules from a large number of diffraction patterns of copies of these objects in random orientations. Millions of low signal-to-noise diffraction patterns with unknown orientation are collected during an X-ray SPI experiment. The patterns are then analyzed and merged using a reconstruction algorithm to retrieve the full 3D-structure of particle. The resolution of reconstruction is limited by background noise, signal-to-noise ratio in diffraction patterns and total amount of data collected. We recently introduced a reference-enhanced holographic single particle imaging methodology [Optica 7,593-601(2020)] to collect high enough signal-to-noise and background tolerant patterns and a reconstruction algorithm to recover missing parameters beyond orientation and then directly retrieve the full Fourier model of the sample of interest. Here we describe a phase retrieval algorithm based on maximum likelihood estimation using pattern search dubbed as MaxLP, with better scalability for fine sampling of latent parameters and much better performance in the low signal limit. Furthermore, we show that structural variations within the target particle are averaged in real space, significantly improving robustness to conformational heterogeneity in comparison to conventional SPI. With these computational improvements, we believe reference-enhanced SPI is capable of reaching sub-nm resolution biomolecule imaging

3He-rich SEP Events Observed by STEREO-A

Using the SIT (Suprathermal Ion Telescope) instrument on STEREO-A we have examined the abundance of the rare isotope 3He during the rising activity phase of solar cycle 24 between January 2010 and December 2011. We have identified six solar energetic particle (SEP) events with enormous abundance enhancements of 3He (3He/4He >1). The events were short lasting, typically ~0.5-1 day and most of them occurred in association with high-speed solar wind streams and corotating interaction regions. With one exception the events were not associated with ~100 keV solar electron intensity increases. The events showed also enhanced NeS/O and Fe/O ratios. The solar images indicate that the events were generally associated with the active regions located near a coronal hole.Comment: accepted for publication in AIP Conference Proceedings for 'Thirteenth International Solar Wind Conference