Mechanical property evaluation of an Al-2024 alloy subjected to HPT processing

An aluminum-copper alloy (Al-2024) was successfully subjected to high-pressure torsion (HPT) up to five turns at room temperature under an applied pressure of 6.0 GPa. The Al-2024 alloy is used as a fuselage structural material in the aerospace sector. Mechanical properties of the HPT-processed Al-2024 alloy were evaluated using the automated ball indentation technique. This test is based on multiple cycles of loading and unloading where a spherical indenter is used. After two and five turns of HPT, the Al-2024 alloy exhibited a UTS value of ~1014 MPa and ~1160 MPa respectively, at the edge of the samples. The microhardness was measured from edges to centers for all HPT samples. These results clearly demonstrate that processing by HPT gives a very significant increase in tensile properties and the microhardness values increase symmetrically from the centers to the edges. Following HPT, TEM examination of the five-turn HPT sample revealed the formation of high-angle grain boundaries and a large dislocation density with a reduced average grain size of ~80 nm. These results also demonstrate that high-pressure torsion is a processing tool for developing nanostructures in the Al-2024 alloy with enhanced mechanical propertie

Effect of processing condition and composition on the microhardness of Cu-(2.5-10)vol.%Al₂O₃ nanocomposite powder particles produced by high energy mechanical milling

Nanostructured Cu-(2.5-10vol.%)Al₂O₃ nanocomposites were produced using high energy mechanical milling. For the as-milled Cu- Al₂O₃ composite powder particles having Al₂O₃ volume fractions of 2.5% and 5%, the increase in average microhardness is significant with the increase of milling time from 12 hours to 24 hours. With the increase of the content of Al₂O₃ nanoparticles the microhardness increases and in the range of 255HV-270HV. The milled nanocomposite powders were heat treated at 150, 300, 400 and 500°C for 1 hour, respectively, to determine the thermal stability of the powder particles as a function of annealing temperature. The average microhardness increased/decreased for the Cu- Al₂O₃ composites after annealing at 150°C due to the dislocation density, while increasing the annealing temperature to 300°C and 400°C the average microhardness almost remained mostly unchanged. Further increasing the annealing temperature to 500°C causes significant decrease in average microhardness due to reduction in dislocation density and coarsening of Cu grains of the Cu- Al₂O₃ composite powders produced after 24 hours of milling. This paper is to report and discuss the changes of the microhardness of the material, caused by the compositions and processing conditions, used to fabricate the Cu-(2.5-10)vol.% Al₂O₃ nanocomposite powders

Microstructural Characterization of Shrouded Plasma-Sprayed Titanium Coatings

Titanium and its alloys are often used for corrosion protection because they are able to offer high chemical resistance against various corrosive media. In this paper, shrouded plasma spray technology was applied to produce titanium coatings. A solid shroud with an external shrouding gas was used to plasma spray titanium powder feedstock with aim of reducing the oxide content in the as-sprayed coatings. The titanium coatings were assessed by optical microscope, scanning electron microscopy, X-ray diffraction, LECO combustion method and Vickers microhardness testing. The results showed that the presence of the shroud and the external shrouding gas led to a dense microstructure with a low porosity in the plasma-sprayed titanium coatings. The oxygen and nitrogen contents in the titanium coating were kept at a low level due to the shielding effect of the shroud attachment and the external shrouding gas. The dominant phase in the shrouded titanium coatings was mainly composed of α-Ti phase, which was very similar to the titanium feedstock powders. The shrouded plasma-sprayed titanium coatings had a Vickers microhardness of 404.2 ± 103.2 HV

Hardening mechanism of commercially pure Mg processed by high pressure torsion at room temperature

Coarse-grained Mg in the as-cast condition and fine-grained Mg in the extruded condition were processed by high pressure torsion (HPT) at room temperature for up to 16 turns. Microstructure observation and texture analysis indicate that to fulfil the Von Mises criterion, the non-basal slip is activated in the as-cast Mg and tension twinning is activated in the as-extruded Mg. Although the deformation mechanism is different in the as-cast Mg and the as-extruded Mg during HPT, their hardening evolutions are similar, i.e. after 1/8 turn of HPT, microhardness of the as-cast Mg and the extruded Mg both show a significant increase and further HPT processing does not significantly further increase the microhardness. Texture strengthening can explain the rapid hardening. Hardness anisotropy and texture data results suggest that texture strengthening plays an important role for both types of samples. Texture strengthening weakens with decreasing grain size

Dimensional effects on magnetic properties of Fe-Si steels due to laser and mechanical cutting

Microstructural deterioration near the cut line and presence of residual stresses both affect the magnetic properties of cut parts. In this paper, the differences between microstructural deterioration resulting from mechanical and laser cutting as well as the sample size effects observed upon hysteresis will be discussed. It will be shown that the underlying mechanism for changes in magnetic properties due to mechanical cutting is distinct from that of laser cutting

A multidisciplinary approach to study precipitation kinetics and hardening in an Al-4Cu (wt. %) alloy

A multidisciplinary approach is presented to analyse the precipitation process in a model Al-Cu alloy. Although this topic has been extensively studied in the past, most of the investigations are focussed either on transmission electron microscopy or on thermal analysis of the processes. The information obtained from these techniques cannot, however, provide a coherent picture of all the complex transformations that take place during decomposition of supersaturated solid solution. Thermal analysis, high resolution dilatometry, (high resolution) transmission electron microscopy and density functional calculations are combined to study precipitation kinetics, interfacial energies, and the effect of second phase precipitates on the mechanical strength of the alloy. Data on both the coherent and semi-coherent orientations of the {\theta}"/Al interface are reported for the first time. The combination of the different characterization and modelling techniques provides a detailed picture of the precipitation phenomena that take place during aging and of the different contributions to the strength of the alloy. This strategy can be used to analyse and design more complex alloys

Effect of pulsed magnetic field pre-treatment of AISI 52100 steel on the coefficient of sliding friction and wear in pin-on-disk tests

Disc specimens manufactured from commercial bearing rollers (AISI 52100 steel, 62–63 HRC) in initial state and after pre-treatment by pulsed magnetic field (PMF) with a magnetic field strength of 1–7 MA/m were tested with sunflower oil using pin-on-disk apparatus. According to the obtained results the treatment causes a reduction in the coefficient of friction and wear. To explain the results, nano- and microhardness tests as well as optical and atomic force microscopy were used. Reasons of the effect of PMF on the friction and wear were discussed.Peer reviewe

Characterisation of dispersions within annealed HVOLF thermally sprayed AlSnCu coatings

High velocity oxy-liquid fuel (HVOLF) AlSnCu coatings are characterised following annealing for up to 5 hours at 300°C. A combination of statistical analysis of BSE images and TEM observations demonstrate the decrease in the number of sub-micron and nanoscale Sn particles with annealing, commensurate with a decrease in the coating microhardness. TEM evidence further suggests the coarsening of nanoscale Sn through a mechanism of a liquid phase migration within the Al matrix. EELS and EFTEM additionally allow the identification of the precipitation of theta'

Excimer laser treatment of ZE41 magnesium alloy for corrosion resistance and microhardness improvement

We would like to acknowledge the financial support of the ‘‘Conseil regional de PACA’’ and Protection des Metaux d’Arenc). The authors are grateful to PMA’s engineers Ms. E. Castellan, Ms. A. Gonthier and Mr. F. Miretti for their help and assistance with the salt-spray testsA laser surface melting treatment (LSMT) was performed on a ZE41 Mg-alloy using an excimer KrF laser. The laser-melted layer depth depends on the laser scan speed. The morphology and the microstructure of the laser-melted surface were characterized, thanks to the scanning electron microscopy (SEM). The melted Mg-alloy presented a homogenous distribution of the alloying elements in the magnesium matrix. The laser surface melting treatment increased the microhardness of the ZE41 Mg-alloy and improved its corrosion resistance

Morphology and Properties of Zn-Al-TiO2 Composite on Mild Steel

The influence of TiO2 composite and dispersed pure Al particle on zinc alloy electrodeposited on mild steel was studied from chloride bath solution.Microstructural and mechanical properties of the alloy were investigated. The structure, surface morphology, and surface topography of the deposited alloys were characterized by scanning electron microscopy (SEM) and atomic force microscope (AFM).In addition, hardness of the coated alloys was measured. It was found that the obtained Zn-Al-TiO2 alloyexhibited more preferred surface morphology and mechanical strength compared tothe substrate. The result shows the existence of interaction between TiO2 compounds and zinc alloy particulate. It also exhibited well bright dominate zinc coating on steel surface