Effect of nanosize BaZrO3 inclusions on vortex parameters in YBaCuO

We report on the field dependence of the microwave complex resistivity data in YBa$_2$Cu$_3$O$_{7-x}$/BaZrO$_3$ films grown by PLD at various BaZrO$_3$ content. The data, analyzed within a recently developed general framework for the mixed-state microwave response of superconductors, yield the field dependence of the fluxon parameters such as the vortex viscosity and the pinning constant. We find that pinning undergoes a change of regime when the BaZrO$_3$ content in the target increases from 2.5 mol.% to 5 mol.%. Simultaneously, the vortex viscosity becomes an increasing function of the applied magnetic field. We propose a scenario in which flux lines are pinned as bundles, and a crossover from dilute point pins to dense c-axis correlated defects takes place between 2.5 and 5 mol.% in the BZO concentration. Our data are inconsistent with vortices occupying mainly the BaZrO$_3$ sites at low fields, and suggest instead that vortices occupy both BaZrO$_3$ sites and interstitials in the YBa$_2$Cu$_3$O$_{7-x}$ matrix, even at low fields.Comment: Presented at EUCAS 2009, to be published in J. Phys.:Conf. Serie

Strong Reduction of the Field-Dependent Microwave Surface Resistance in YBCO with BaZrO_3 Inclusions

We present measurements of the magnetic field dependent microwave surface resistance in laser-ablated YBa$_2$Cu$_3$O$_{7-\delta}$ films on SrTiO$_3$ substrates. BaZrO$_3$ crystallites were included in the films using composite targets containing BaZrO$_3$ inclusions with mean grain size smaller than 1 $\mu$m. X-ray diffraction showed single epitaxial relationship between BaZrO$_3$ and YBa$_2$Cu$_3$O$_{7-\delta}$. The effective surface resistance was measured at 47.7 GHz for 60$< T <$90 K and 0$< \mu_0H <$0.8 T. The magnetic field had a very different effect on pristine YBa$_2$Cu$_3$O$_{7-\delta}$ and YBa$_2$Cu$_3$O$_{7-\delta}$/BaZrO$_3$, while for $\mu_0H=$0 only a reduction of $T_c$ in the YBa$_2$Cu$_3$O$_{7-\delta}$/BaZrO$_3$ film was observed, consistent with dc measurements. At low enough $T$, in moderate fields YBa$_2$Cu$_3$O$_{7-\delta}$/BaZrO$_3$ exhibited an intrinsic thin film resistance lower than the pure film. The results clearly indicate that BaZrO$_3$ inclusions determine a strong reduction of the field-dependent surface resistance. From the analysis of the data in the framework of simple models for the microwave surface impedance in the mixed state we argue that BaZrO$_3$ inclusions determine very steep pinning potentials.Comment: LaTeX, 6 pages, 4 figures, uses jpconf.cls and jpconf11.clo class files, talk given at EUCAS 2007, submitted to J. Phys.: Conf. Serie

Directional pinning and anisotropy in YBa2Cu3O7-x with BaZrO3 nanorods: intrinsic and nanorods-induced anisotropy

We present a study of the anisotropic vortex parameters as obtained from measurements of the microwave complex resistivity in the vortex state with a tilted applied magnetic field in YBa2Cu3O7-x thin films with BaZrO3 nanorods. We present the angular dependence of the vortex viscosity $\eta$, the pinning constant k_p and the upper limit for the creep factor \chi_M. We show that the directional effect of the nanorods is absent in \eta, which is dictated by the mass anisotropy \gamma. By contrast, pinning-mediated properties are strongly affected by the nanorods. It is significant that the pinning and creep affected by the nanorods is detectable also at our very high operating frequency, which implies very short-range displacements of the vortices from their equilibrium position.Comment: Proceedings of VORTEX VIII Conference, to be published in Physica

Reduction of the field-dependent microwave surface resistance in YBa_2Cu_3O_7 with sub-micrometric BaZrO_3 inclusions as a function of BaZrO_3 concentration

In order to study the vortex pinning determined by artificially introduced pinning centers in the small-vortex displacement regime, we measured the microwave surface impedance at 47.7 GHz in the mixed state of YBa$_{2}$Cu$_{3}$O$_{7-\delta}$ thin films, where sub-micrometric BaZrO$_3$ particles have been incorporated. As a function of the BaZrO$_3$ content, we observe that the absolute losses slightly decrease up to a BaZrO$_3$ content of 5%, and then increase. We found that the magnetic-field-induced losses behave differently, in that they are not monotonic with increasing BaZrO$_3$ concentration: at small concentration (2.5%) the field-induced losses increase, but large reduction of the losses themselves, by factors up to 3, is observed upon further increasing the BaZrO$_3$ concentration in the target up to 7%. Using measurements of both surface resistance and surface reactance we estimate vortex pinning-related parameters. We find that BaZrO$_3$ inclusions introduce deep and steep pinning wells. In particular, the minimum height of the energy barrier for single vortices is raised. At larger BaZrO$_3$ content (5% and 7%) the phenomenon is at its maximum, but it is unclear whether it shows a saturation or not, thus leaving room for further improvements.Comment: 7 pages, 7 figure

Strong reduction of field-dependent microwave surface resistance in YBa2_{2}Cu3_{3}O7−δ_{7-\delta} with sub-micrometric BaZrO3_3 inclusions

We observe a strong reduction of the field induced thin film surface resistance measured at high microwave frequency ($\nu=$47.7 GHz) in YBa$_{2}$Cu$_{3}$O$_{7-\delta}$ thin films grown on SrTiO$_3$ substrates, as a consequence of the introduction of sub-micrometric BaZrO$_3$ particles. The field increase of the surface resistance is smaller by a factor of $\sim$3 in the film with BaZrO$_3$ inclusions, while the zero-field properties are not much affected. Combining surface resistance and surface reactance data we conclude (a) that BaZrO$_3$ inclusions determine very deep and steep pinning wells and (b) that the pinning changes nature with respect to the pure film.Comment: RevTeX; 4 pages, 3 figures; submitted to Applied Physics Letter

Anisotropy and directional pinning in YBaCuO with BaZrO3 nanorods

Measurements of anisotropic transport properties (dc and high-frequency regime) of driven vortex matter in YBa$_2$Cu$_3$O$_{7-x}$ with elongated strong-pinning sites (c-axis aligned, self-assembled BaZrO$_3$ nanorods) are used to demonstrate that the effective-mass angular scaling takes place only in intrinsic physical quantities (flux-flow resistivity), and not in pinning-related Labusch parameter and critical currents. Comparison of the dynamics at different time scales shows evidence for a transition of the vortex matter toward a Mott phase, driven by the presence of nanorods. The strong pinning in dc arises partially from a dynamic effect.Comment: 4 pages, 4 figures. Accepted for publication on Applied Physics Letters. With respect to v1: changed title, slightly shortene

Microwave properties of DyBa_2Cu_3O_(7-x) monodomains and related compounds in magnetic fields

We present a microwave characterization of a DyBa$_{2}$Cu$_{3}$O$_{7-x}$ single domain, grown by the top-seeded melt-textured technique. We report the (a,b) plane field-induced surface resistance, $\Delta R_s(H)$, at 48.3 GHz, measured by means of a cylindrical metal cavity in the end-wall-replacement configuration. Changes in the cavity quality factor Q against the applied magnetic field yield $\Delta R_s(H)$ at fixed temperatures. The temperature range [70 K ; T_c] was explored. The magnetic field $\mu_0 H <$ 0.8 T was applied along the c axis. The field dependence of $\Delta R_s(H)$ does not exhibit the steep, step-like increase at low fields typical of weak-links. This result indicates the single-domain character of the sample under investigation. $\Delta R_s(H)$ exhibits a nearly square-root dependence on H, as expected for fluxon motion. From the analysis of the data in terms of motion of Abrikosov vortices we estimate the temperature dependences of the London penetration depth $\lambda$ and the vortex viscosity $\eta$, and their zero-temperature values $\lambda(0)=$165 nm and $\eta(0)=$ 3 10$^{-7}$ Nsm$^{-2}$, which are found in excellent agreement with reported data in YBa$_{2}$Cu$_{3}$O$_{7-x}$ single crystals. Comparison of microwave properties with those of related samples indicate the need for reporting data as a function of T/T_c in order to obtain universal laws.Comment: 6 pages, 4 figures, LaTeX, submitted to Journal of Applied Physic

Microwave properties of Nb/PdNi/Nb trilayers. Observation of flux flow in excess of Bardeen-Stephen theory

We combine wideband (1-20 GHz) Corbino disk and dielectric resonator (8.2 GHz) techniques to study the microwave properties in Nb/PdNi/Nb trilayers, grown by UHV dc magnetron sputtering, composed by Nb layers of nominal thickness $d_S$=15 nm, and a ferromagnetic PdNi layer of thickness $d_F$= 1, 2, 8 and 9 nm. We focus on the vortex state. Magnetic fields up to $H_{c2}$ were applied. The microwave resistivity at fixed $H/H_{c2}$ increases with $d_F$, eventually exceeding the Bardeen Stephen flux flow value.Comment: 6 pages. Submitted to Journal of Superconductivity and Novel Magnetis