19 research outputs found

    An extended semi-analytical formulation for fast and reliable mode I/II stress analysis of adhesively bonded joints

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    The Finite Element (FE) method is able to address the stress analysis of adhesively bonded joints. However, analyses based on FE models are computationally expansive and it would be profitable to develop simplified approaches enabling extensive parametric studies. Firstly, a 1D-beam simplified model for the bonded joint stress analysis assuming a linear elastic adhesive material is presented. This model, derived from an approach inspired by the Finite Element (FE) method and based on the semi-analytical formulation of a 4-nodes macro-element, is able to simulate entire bonded overlaps at low computational costs. Secondly, a numerical procedure allowing for non-linear adhesive stress–strain relationships to be accounted for is presented. This procedure allows for various non-linear adhesive behaviors (ie. softening, plastic, etc.) to be accounted for with no restriction on the specimen geometry. The possible mixed-mode I/II response of the adhesive layer is introduced through an extension of the classical Cohesive Zone Modeling (CZM) procedure. The aforementioned procedure is then illustrated using a bi-linear softening adhesive behavior. However the procedure is not limited to this particular behavior only. The results obtained are finally compared to those of more time-consuming 2D FE strength predictions. Good agreement is shown

    Caractérisation des propriétés d'adhésion et de frottement de quelques matériaux : influence des conditions opératoires

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    L'objectif de cette thÚse était d'analyser les forces d'interaction en milieu liquide à l'aide de la microscopie à force atomique (AFM) et d'utiliser les résultats des mesures, pour expliquer le frottement mesuré dans le cadre de la microtribologie (charge de 200 mN). Les expériences ont été menées dans différents électrolytes (eau, éthanol, éthylÚne glycol, formamide) et à pH variable. L'étude de l'influence de la nature de l'électrolyte sur les interactions entre la pointe de l'AFM (Si3N4) et différentes surfaces (verre, Si, films TiN et DLC) a montré une forte corrélation entre le frottement commençant et l'hystérésis d'adhésion mesurée par AFM. L'étude de l'influence du pH sur les forces d'interaction entre la pointe et différents matériaux (SiC, Ni, Cu) a montré que selon la valeur du pH, les matériaux testés présentent des interactions de type attractif ou répulsif dues à leur charge portée en surface qui se manifestent aussi bien sur les propriétés d'adhésion que de frottement.The aim of this thesis was to analyze the interaction in liquid environment with an atomic force microscope (AFM) and to use the results of the measurements to explain the friction measured in microtribology (load of 200 mN). The experiments have been led in different electrolytes (water, ethanol, ethylene glycol, formamide) and as a function of pH. The study of the influence of the nature of the electrolyte on the interactions between the tip of the AFM (Si3N4) and different surfaces (glass, Si, TiN and DLC coatings) showed a strong relationship between the early friction and the hysteresis of adhesion measured by AFM. The study of the influence of the pH on the interactions between the tip and different materials (SiC, Ni, Cu) showed that according to the value of the pH, the tested materials present attractive or repulsive interactions due to their surface charge that has an impact as well on the adhesion that friction.BESANCON-BU Sciences Staps (250562103) / SudocSudocFranceF

    Etude de systÚmes ternaires à base de Cr et N pour applications mécaniques sur outils de coupe destinés à la transformation du bois

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    Les actes de ce colloque francophone ont Ă©tĂ© mis sur un CD-Rom, pas en version papier.Le prĂ©sent travail se propose d'Ă©tudier les propriĂ©tĂ©s physico-chimiques et mĂ©caniques de revĂȘtements PVD nanocristallins ou nanocomposites (CrAlN, CrSiN) obtenus sur diffĂ©rents substrats et destinĂ©s Ă  la premiĂšre et seconde transformation du bois une fois leur optimisation effectuĂ©e. Pour cela, les couches de CrAlN obtenues par magnĂ©tron RF ont subit des observations au MEB afin de dĂ©terminer la morphologie des couches alors que de la microanalyse EDS a dĂ©fini leur composition. La structure des couches a Ă©tĂ© dĂ©terminĂ©e par diffraction de rayons X. Nous avons alors mesurĂ© l’épaisseur des couches par profilomĂ©trie et par interfĂ©romĂ©trie puis on en a dĂ©duit les contraintes internes de celles-ci. L’adhĂ©rence et la duretĂ© des couches ont Ă©tĂ© obtenues par scratch-tests et nanoindentation. Enfin, des analyses plus fines telles que de l’XPS et du SIMS ont Ă©tĂ© rĂ©alisĂ©es afin de dĂ©terminer les phases en prĂ©sence dans ces couches. La co-pulvĂ©risation rĂ©active des cibles de Cr et Si en position confocale, est un procedĂ© sĂ©duisant pour l’élaboration de films de CrSiN avec une structure nanocomposite du type nc-CrN/a-SiNx. Les analyses EDS et les caractĂ©risations par DRX et nanoindentation confirment dans ces films la prĂ©sence de phase cristallisĂ©e de type CrN et la possibilitĂ© de faire varier leur teneur en silicium corrĂ©lĂ©e avec des changements de duretĂ©.Conseil RĂ©gional de Bourgogne ainsi que le Conseil RĂ©gional de Franche-ComtĂ© dans le cadre de ce projet transrĂ©gional intitulĂ© « ROBUS », CTBA cofinanceur de la thĂšse de C. Labid

    Tantalum Oxide Thin Films Sputter-Deposited by Oxygen Gas Pulsing

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    International audienceantalum oxide thin films are deposited by DC reactive magnetron sputtering from a tantalum metallic target and argon + oxygen. The oxygen gas is pulsed during the deposition with a constant pulsing period T = 10 s, whereas the introduction time of the reactive gas, namely the tON injection time, is systematically changed from 0 to 100% of T. Therefore, composition of as-deposited TaOx films is continuously changed from pure metallic tantalum to the over-stoichiometric Ta2O5 material. Films adopt the body-centered cubic structure (metallic Ta) for the lowest tON injection time values (oxygen stoichiometry x < 1.0) and become amorphous for the longest ones. It is shown that the tON injection time is a key parameter to deposit either homogeneous tantalum oxides, or periodic Ta/TaOx multilayers with alternations close to 3 nm. Optical transmittance in the visible region of the film/glass substrate system and electrical conductivity vs. temperature both exhibit a gradual evolution from metallic (σ300K = 8.17 × 105 S m−1^{−1} with an opaque behavior) to semiconducting (σ300K = 1.97 × 103 S m−1^{−1} with a semi-transparent transmittance) and finally to dielectric properties (σ300K < 10−5^{−5} S m−1^{−1} for interferential films) as a function of the oxygen concentration in the film

    Tuning the Optical Properties of WO3Films Exhibiting a ZigzagColumnar Microstructure

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Priority="60" Name="Light Shading Accent 1"/&gt <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/&gt <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/&gt <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/&gt <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/&gt <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/&gt <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/&gt <w:LsdException Locked="false" Priority="34" QFormat="true" Name="List Paragraph"/&gt <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/&gt <w:LsdException Locked="false" Priority="30" QFormat="true" Name="Intense Quote"/&gt <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/&gt <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/&gt <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/&gt <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/&gt <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/&gt <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/&gt <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/&gt <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/&gt <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/&gt <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/&gt <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/&gt <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/&gt <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/&gt <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/&gt <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/&gt <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/&gt <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/&gt <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/&gt <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/&gt <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/&gt <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/&gt <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/&gt <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/&gt <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/&gt <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/&gt <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/&gt <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/&gt <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/&gt <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/&gt <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/&gt <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/&gt <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/&gt <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/&gt <w:LsdException Locked="false" Priority="71" Name="Colorful Shading A
    corecore