In vitro effects of hydrogen peroxide combined with different activators for the in-office bleaching technique on enamel

The aim of this study was to evaluate the alteration of human enamel bleached with high concentrations of hydrogen peroxide associated with different activators. Fifty enamel/ dentin blocks (4 x 4 mm) were obtained from human third molars and randomized divided according to the bleaching procedure (n = 10): G1 = 35% hydrogen peroxide (HP -Whiteness HP Maxx); G2 = HP + Halogen lamp (HL); G3 = HP + 7% sodium bicarbonate (SB); G4 = HP + 20% sodium hydroxide (SH); and G5 = 38% hydrogen peroxide (OXB - Opalescence Xtra Boost). The bleaching treatments were performed in three sessions with a 7-day interval between them. The enamel content, before (baseline) and after bleaching, was determined using an FT-Raman spectrometer and was based on the concentration of phosphate, carbonate, and organic matrix. Statistical analysis was performed using two-way ANOVA for repeated measures and Tukey's test. The results showed no significant differences between time of analysis (p = 0.5175) for most treatments and peak areas analyzed; and among bleaching treatments (p = 0.4184). The comparisons during and after bleaching revealed a significant difference in the HP group for the peak areas of carbonate and organic matrix, and for the organic matrix in OXB and HP+ SH groups. Tukey's analysis determined that the difference, peak areas, and the interaction among treatment, time and peak was statistically significant (p < 0.05). The association of activators with hydrogen peroxide was effective in the alteration of enamel, mainly with regards to the organic matrix737516521FUNDAÇÃO DE AMPARO À PESQUISA DO ESTADO DE SÃO PAULO - FAPESP05/60082-4 01/14384-

The effect of curing light and chemical catalyst on the degree of conversion of two dual cured resin luting cements

The aim of this study was to evaluate the influence of different curing lights and chemical catalysts on the degree of conversion of resin luting cements. A total of 60 disk-shaped specimens of RelyX ARC or Panavia F of diameter 5 mm and thickness 0.5 mm were prepared and the respective chemical catalyst (Scotchbond Multi-Purpose Plus or ED Primer) was added. The specimens were light-cured using different curing units (an argon ion laser, an LED or a quartz-tungsten-halogen light) through shade A2 composite disks of diameter 10 mm and thickness 2 mm. After 24 h of dry storage at 37A degrees C, the degree of conversion of the resin luting cements was measured by Fourier-transformed infrared spectroscopy. For statistical analysis, ANOVA and the Tukey test were used, with p a parts per thousand currency signaEuro parts per thousand 0.05. Panavia F when used without catalyst and cured using the LED or the argon ion laser showed degree of conversion values significantly lower than RelyX ARC, with and without catalyst, and cured with any of the light sources. Therefore, the degree of conversion of Panavia F with ED Primer cured with the quartz-tungsten-halogen light was significantly different from that of RelyX ARC regardless of the use of the chemical catalyst and light curing source. In conclusion, RelyX ARC can be cured satisfactorily with the argon ion laser, LED or quartz-tungsten-halogen light with or without a chemical catalyst. To obtain a satisfactory degree of conversion, Panavia F luting cement should be used with ED Primer and cured with halogen light.CAPE

Effect of dimethyl sulfoxide wet-bonding technique on hybrid layer quality and dentin bond strength

This study examined the effect of a dimethyl sulfoxide (DMSO) wet bonding technique on the resin infiltration depths at the bonded interface and dentin bond strength of different adhesive systems. Flat dentin surfaces of 48 human third molars were treated with 50% DMSO (experimental groups) or with distilled water (controls) before bonding using an etch-and-rinse (SBMP: Scotchbond Multi-Purpose, 3M ESPE) or a self-etch (Clearfil: Clearfil SE Bond, Kuraray) adhesive system. The restored crown segments (n = 12/group) were stored in distilled water (24 h) and sectioned for interfacial analysis of exposed collagen using Masson's Trichrome staining and for microtensile bond strength testing. The extent of exposed collagen was measured using light microscopy and a histometric analysis software. Failure modes were examined by SEM. Data was analyzed by two-way ANOVA followed by Tukey Test (alpha = 0.05). The interaction of bonding protocol and adhesive system had significant effects on the extension of exposed collagen matrix (p 0.05). DMSO-wet bonding was effective to improve the quality of resin-dentin bonds of the tested etch-and-rinse adhesives by reducing the extent of exposed collagen matrix at the base of the resin-dentin biopolymer. The improved penetration of adhesive monomers is reflected as an increase in the immediate bond strength when the DMSO-wet bonding technique is used with a water-based etch-and-rinse adhesive316676683CONSELHO NACIONAL DE DESENVOLVIMENTO CIENTÍFICO E TECNOLÓGICO - CNPQCOORDENAÇÃO DE APERFEIÇOAMENTO DE PESSOAL DE NÍVEL SUPERIOR - CAPESAcademy of Finlan

Dispositivo De Controle De FumaÇa E Uso Do Referido Dispositivo

DISPOSITIVO DE CONTROLE DE FUMAÇA E USO DO REFERIDO DISPOSITIVO. A presente invenção refere-se a um dispositivo de controle de fumaça de tabacaria utilizado em testes de pigméntação e depósitos tóxicos oriundos em substratos dentais e materiais odontológicos. Além disso, a presente invenção refere-se ao uso do referido dispositivo.BRPI1101465 (A2)G01N1/22BR2011PI01465G01N1/2

Mechanical and physical properties of silorane and methacrylate-based composites

Made available in DSpace on 2019-09-12T16:53:37Z (GMT). No. of bitstreams: 0 Previous issue date: 2013Objectives: This study measured the degree of conversion (DC), sorption, solubility and microhardness of methacrylate (Filtek Z250 and Filtek Z350XT) and silorane-based composites (Filtek P90). Methods: DC was measured using near infrared spectroscopy immediately and 24 h after the photoactivation. Sorption and solubility measurements were performed after 24 h, 4 weeks and 12 weeks of storage in water. Knoop microhardness was measured after 24 h and after thermal cycling. The data were statistically analyzed using ANOVA followed by Tukey's, Tamhane or paired t-tests (alpha = 0.05). Results: The DC for P90 (37.22 +/- 1.46) was significantly lower than the Z250 (71.44 +/- 1.66) and Z350 (71.76 +/- 2.84). Water sorption was highest in the Z250 and lowest in the P90. All the tested composites exhibited similar values after 24 h of immersion, and no significant differences were observed. No significant differences were observed between the solubilities of the P90 composite (12 weeks) and the Z250 or Z350 composites (4 weeks). KHN values were less elevated for the P90 composite and similar for the Z250 and Z350 composites. An effect of thermal cycling on KHN values was observed for all the composites (p < 0.001). Conclusions: Silorane produced the lowest DC and KHN values and exhibited lower water sorption and solubility compared to methacrylate- based composites. These differences suggest that silorane composites exhibit better hydrolytic stability after 3 months of water immersion compared to conventional methacrylate-based composites. Clinical significance: Silorane had higher hydrolytic stability after 3 months of water immersion than the methacrylate-based resins, despite the lower values of DC and KHN recorded. (c) 2013 Elsevier Ltd. All rights reserved.[Celerino de Moraes Porto, Isabel Cristina] Univ Fed Alagoas, Dept Restorat Dent, BR-57072970 Maceio, Alagoas, Brazil[Baggio de Aguiar, Flavio Henrique] Univ Estadual Campinas, Dept Restorat Dent, BR-13414903 Sao Paulo, Brazil[Brandt, William Cunha] Univ Santo Amaro, Dept Dent, BR-04829300 Sao Paulo, Brazil[Susy Liporoni, Priscila Christiane] Universidade de Taubaté (Unitau), Dept Restorat Dent, BR-12020340 Sao Paulo, Brazi

Evaluation of bond strength, nanoleakage, and marginal adaptation of bulk-fill composites submitted to thermomechanical aging

Purpose: To evaluate the bond strength (BS). nanoleakage, and marginal adaptation (MA) of three bulk-fill and one conventional composite, submitted or not to mechanical and thermal cycling. Materials and Methods: Ninety-six molars were selected and 4-mm-deep class I cavities were prepared and restored. Half of the teeth were submitted to mechanical and thermal cycling (MTC). Teeth were divided into 8 groups (n = 12), according to the composite used - Filtek Z350 XT (Z350), Tetric N-Ceram Bulk Fill (TET), Filtek Bulk Fill Posterior Restorative (FBF) and SonicFill (SF) - and aging, submitted or not to MTC. Fifty-six teeth (n = 7) were used for bond-strength testing, which was performed on stick-shaped specimens obtained from the restored area. Two sticks per tooth were selected to assess nanoleakage. For MA analysis, 40 teeth (n = 5) were sectioned parallel and perpendicular to the occlusal surface and resin-based replicas from the obtained surfaces were prepared. Fracture pattern, nanoleakage, and MA were evaluated using SEM. Quantitative analysis of nanoleakage and MA were performed with Image) software. Data obtained were submitted to two-way ANOVA and Tukey's test (alpha = 0.05). Results: TET presented good MA and higher values of BS when compared to SF. 2350 and FBF presented poorer MA and lower BS, which was statically similar to the other groups. SF obtained the best MA values. Regarding nanoleakage, the highest values were obtained for TEL which differed significantly from the other groups, which presented similar results among themselves. Aging by MTC solely affected MA. Conclusion: Bulk-fill composites presented similar performance to the conventional nanocomposite and remained stable when aged.213255264FUNDAÇÃO DE AMPARO À PESQUISA DO ESTADO DE SÃO PAULO - FAPESP2015/23201-

Effect of diphenyliodonium hexafluorophosphate salt on experimental infiltrants containing different diluents

Non-invasive treatments for caries lesions are increasingly required for oral health; resin infiltration is one possible conservative option. In this study, we evaluated the effects of diphenyliodonium hexafluorophosphate salt (DPI) on experimental resin infiltrants with either (hydroxyethyl)methacrylate (HEMA) or ethanol as the diluent. A monomeric base with diglycidyl methacrylate ethoxylated (BisEMA, 25wt%) and triethylene glycol dimethacrylate (TEGDMA, 75wt%), 0.5mol% of camphorquinone, and 1mol% of ethyl-4-(dimethylamino)benzoate (EDAB) was prepared. The mixtures were divided into 12 groups according to DPI concentration (0; 0.25; 0.5; 1mol%) and diluents (10wt% HEMA, 10wt% ethanol, or none). Degree of conversion (DC), water sorption (Ws), solubility (Sol), contact angle (CA), and cohesive strength (CS) tests were performed and compared to a commercial infiltrant control group (Icon). Only ethanol negatively affected DC and Sol, but both diluents negatively affected Ws and CS. Nevertheless, the presence of DPI, mainly at the 0.5mol% concentration, compensated for the negative effects of the diluents. The commercial control group was less effective only for CS. In conclusion, 0.5% DPI seems to be the most suitable concentration to compensate for the negative effects of diluents1072202208CNPQ - Conselho Nacional de Desenvolvimento Científico e Tecnológico132690/2015-0