Effects of Dissolved Air on Subcooled Flow Boiling of a Dielectric Coolant in a Microchannel Heat Sink

The effects of dissolved air in the dielectric liquid FC-77 on flow boiling in a microchannel heat sink containing ten parallel channels, each 500 mircometers wide and 2.5 mm deep, were experimentally investigated. Experiments were conducted before and after degassing, at three flow rates in the range of 30–50 ml/min. The dissolved air resulted in a significant reduction in wall temperature at which bubbles were first observed in the microchannels. Analysis of the results suggests that the bubbles observed initially in the undegassed liquid were most likely air bubbles. Once the boiling process is initiated, the wall temperature continues to increase for the undegassed liquid, whereas it remains relatively unchanged in the case of the degassed liquid. Prior to the inception of boiling in the degassed liquid, the heat transfer coefficients with the undegassed liquid were 300–500 % higher than for degassed liquid, depending on the flow rate. The heat transfer coefficients for both cases reach similar values at high heat fluxes (\u3e120 KW/m^2) the boiling process with the degassed liquid was well established. The boiling process induced a significant increase in pressure drop relative to single-phase flow; the pressure drop for undegassed liquid was measured to be higher than for degassed liquid once the boiling process became well established in both cases. Flow instabilities were induced by the boiling process, and the magnitude of the instability was quantified using the standard deviation of the measured pressure drop at a given heat flux. It was found that the magnitude of flow instability increased with increasing heat flux in both the undegassed and degassed liquids, with greater flow instability noted in the undegassed liquid

Flow Patterns During Convective Boiling in Microchannels

To develop a flow regime map for convective boiling in microchannels and to propose flow pattern-based models to predict the corresponding heat transfer coefficients, a thorough understanding of the existing flow patterns and their transitions is necessary. In the present study, high-speed photography is employed to observe the flow patterns in flow boiling of a dielectric liquid, FC-77, in parallel silicon microchannels of depth 400 μm and widths ranging from 100 to 5850 μm. In each test, liquid mass flux and inlet subcooling are fixed at 250 kg/m2s and 5°C, respectively, while the heat flux to the bottom of the heat sink is increased form zero to a value near the critical heat flux. Temperature and pressure are measured at several locations. A high-speed digital video camera is used to observe boiling patterns at frame rates ranging from 2000 to 24000 frames per second (fps). The images presented show a top view of the horizontal microchannels, at a location along the heat sink centerline and near the flow exit

Thermal Resistance Measurement across a Wick Structure using a Novel Thermosyphon Test Chamber

Microfluidics-based cell assays offer high levels of automation and integration, and allow multiple assays to be run in parallel, based on reduced sample volumes. These characteristics make them attractive for studies associated with drug discovery. Controlled delivery of drug molecules or other exogenous materials into cells is a critical issue that needs to be addressed before microfluidics can serve as a viable platform for drug screening and studies. In this study, we report the application of hydrodynamic focusing for controlled delivery of small molecules into cells immobilized on the substrate of a microfluidic device. We delivered calcein AM which was permeant to the cell membrane into cells, and monitored its enzymatic conversion into fluorescent calcein during and after the delivery. Different ratios of the sample flow to the side flow were tested to determine how the conditions of hydrodynamic focusing affected the delivery. A 3D numerical model was developed to help understand the fluid flow, molecular diffusion due to hydrodynamic focusing in the microfluidic channel. The results from the simulation indicated that the calcein AM concentration on the outer surface of a cell was determined by the conditions of hydrodynamic focusing. By comparing the results from the simulation with those from the experiment, we found that the calcein AM concentration on the cell outer surface correlated very well with the amount of the molecules delivered into the cell. This suggests that hydrodynamic focusing provides an effective way for potentially quantitative delivery of exogenous molecules into cells at the single cell or subcellular level. We expect that our technique will pave the way to high-throughput drug screening and delivery on a microfluidic platform

Analysis and Prediction of Constriction Resistance between Coated Surfaces

Well-controlled and well-characterized experimental measurements are obtained during the melting of a moderate-Prandtl-number material (n-eicosane) in a cylindrical enclosure heated from the side. The study aims to provide benchmark experimental measurements for validation of numerical codes. Experimental results in terms of measured temperatures and melt front locations are reported in both graphical and tabular forms. The melt front was captured photographically and its location ascertained using digital image processing techniques. To facilitate numerical validation exercises, a complete set of experimental results have been made available on a website for public access. An illustrative numerical comparison exercise was also undertaken using a multiblock finite volume method and the enthalpy method for a range of Stefan numbers. The experimental boundary conditions can be adequately represented with a constant and uniform side wall temperature, a constant and uniform lower surface temperature, and an adiabatic top wall. Very good agreement was obtained between the predictions and the experiment for Stefan numbers of up to 0.1807. The experimental results for a Stefan number of 0.0836 are recommended as being the most suitable for numerical benchmarking, since the boundary conditions are best controlled in this set of experiments

Enabling Highly Effective Boiling from Superhydrophobic Surfaces

Avariety of industrial applications such as power generation, water distillation, and high-density cooling rely on heat transfer processes involving boiling. Enhancements to the boiling process can improve the energy efficiency and performance across multiple industries. Highly wetting textured surfaces have shown promise in boiling applications since capillary wicking increases the maximum heat flux that can be dissipated. Conversely, highly nonwetting textured (superhydrophobic) surfaces have been largely dismissed for these applications as they have been shown to promote formation of an insulating vapor film that greatly diminishes heat transfer efficiency. The current Letter shows that boiling from a superhydrophobic surface in an initial Wenzel state, in which the surface texture is infiltrated with liquid, results in remarkably low surface superheat with nucleate boiling sustained up to a critical heat flux typical of hydrophilic wetting surfaces, and thus upends this conventional wisdom. Two distinct boiling behaviors are demonstrated on both micro- and nanostructured superhydrophobic surfaces based on the initial wetting state. For an initial surface condition in which vapor occupies the interstices of the surface texture (Cassie- Baxter state), premature film boiling occurs, as has been commonly observed in the literature. However, if the surface texture is infiltrated with liquid (Wenzel state) prior to boiling, drastically improved thermal performance is observed; in this wetting state, the three-phase contact line is pinned during vapor bubble growth, which prevents the development of a vapor film over the surface and maintains efficient nucleate boiling behavior

The Petal Effect of Parahydrophobic Surfaces offers Low Receding Contact Angles that Promote Effective Boiling

Despite extensive study of boiling processes and their widespread use in industry, critical interactions between the fluid and surface during boiling remain poorly understood. Simplistic, static descriptions of the contact angle are still relied upon to describe the effects of surface wettability on dynamic interfacial processes that govern boiling. This work demonstrates the critical role of the dynamic wettability characteristics of a surface on bubble growth dynamics and boiling performance. In spite of their superior nucleation behavior, hydrophobic surfaces have received little attention for boiling applications due to their typically premature transition from efficient nucleate boiling to inefficient film boiling. Evaluation of hydrophobic surfaces with high contact angle hysteresis reveals that the heat transfer efficacy of these surfaces can be exploited in boiling, so long as the receding contact angle of the surface is sufficiently small to mitigate vapor spreading and thereby extend the nucleate boiling regime. A new paradigm of textured boiling surfaces – parahydrophobic surfaces that exhibit the “petal effect” and mimic the wetting behavior of a rose petal – are shown to have untapped potential in boiling applications resulting from highly hydrophobic behavior coupled with low receding contact angles

High‐Frequency Thermal‐Fluidic Characterization of Dynamic Microchannel Flow Boiling Instabilities: Part 1 ‐ Rapid‐Bubble‐Growth Instability at the Onset of Boiling

Dynamic flow boiling instabilities are studied experimentally in a single, 500 μm-diameter glass mi- crochannel subjected to a uniform heat flux. Fluid flow is driven through the microchannel in an open- loop test facility by maintaining a constant pressure difference between a pressurized upstream reservoir and a reservoir at the exit that is open to the ambient; the working fluid is HFE-7100. This hydrodynamic boundary condition resembles that of an individual channel in a parallel-channel heat sink where the channel mass flux can vary in time. Simultaneous high-frequency measurement of reservoir, inlet, and outlet pressures, pressure drop, mass flux, inlet and outlet fluid temperatures, and wall temperature is synchronized to high-speed flow visualizations enabling transient characterization of the thermal-fluidic behavior. Part 1 of this study investigates the rapid-bubble-growth instability at the onset of boiling; the effect of flow inertia and inlet liquid subcooling is assessed. The mechanisms underlying the rapid- bubble-growth instability, namely, a large liquid superheat and a large pressure spike, are quantified; this instability is shown to cause flow reversal and can result in large temperature spikes. Low flow inertia exacerbates the rapid-bubble-growth instability by starving the heated channel of liquid replenishment for longer durations and results in severe temperature increases. In the case of high flow inertia or high inlet liquid subcooling, flow reversal is still observed at the onset of boiling, but results in a minimal wall temperature rise because liquid quickly replenishes the heated channel. A companion paper (Part 2) investigates the effect of flow inertia, inlet liquid subcooling, as well as heat flux on the thermal-fluidic oscillations during time-periodic flow boiling that follows the initial incipience at the onset of boiling considered here

Time-Resolved Characterization of Microchannel Flow Boiling During Transient Heating: Part 2 – Dynamic Response to Time-Periodic Heat Flux Pulses

Flow boiling in microchannels is an effective method for dissipating high heat fluxes. However, two- phase heat sink operation during transient heating conditions remains relatively unexplored. In Part 1 of this two-part study, the dynamic response of flow boiling to a single heat flux pulse was experimentally studied. In this Part 2, the effect of heating pulse frequency on microchannel flow boiling is explored when a time-periodic series of pulses is applied to the channel. HFE-7100 is driven through a single 500 μm-diameter glass microchannel using a constant pressure reservoir. A thin indium tin oxide layer on the outside surface of the microchannel enables simultaneous transient heating and flow visualization. High-frequency measurements of heat flux, wall temperature, pressure drop, and mass flux are synchro- nized to the flow visualizations to characterize the boiling process. A square-wave heating profile is used with pulse frequencies ranging from 0.1 to 100 Hz and three different heat fluxes levels (15, 75, and 150 kW/m 2 ). Three different time-periodic flow boiling fluctuations were observed for the heat flux lev- els and pulse frequencies investigated in this study: flow regime transitions, pressure drop oscillations, and heating pulse propagation. For heat flux pulses between 15 and 75 kW/m 2 and heating pulse fre- quencies above 1 Hz, time-periodic flow regime transitions between single-phase and two-phase flow are reported. For heating profiles involving 150 kW/m 2 heat flux pulses, fluid in the microchannel is al- ways boiling and thus the flow regime transitions are eliminated. For heating pulse frequencies between approximately 1 and 10 Hz, the thermal and flow fluctuations are heavily coupled to the heating char- acteristics, forcing the pressure drop instability frequency to match the heating frequency. Outside this heating pulse frequency range, the pressure drop instability occurs at the intrinsic frequency of the sys- tem. For heating pulse frequencies above 25 Hz, the microchannel wall attenuates the transient heating profile and the fluid essentially experiences a constant heat flux

The Effect of Lateral Thermal Coupling Between Parallel Microchannels on Two‐Phase Flow Distribution

Evaporating flows in parallel channels occurring in a variety of industrial heat exchange processes can encounter non-uniform flow distribution between channels as a result of two-phase flow instabilities. Such flow maldistribution can have a negative impact on the performance, robustness and predictability of these systems. Two-phase flow modeling can assist in understanding the mechanistic behavior of this flow maldistribution, as well as determine parametric trends and identify safe operating conditions. The work described in this paper expands on prior two-phase flow distribution modeling efforts by including and assessing the effect of thermal conduction in the walls surrounding the parallel channels. This thermal conduction has a critical dampening effect on wall temperature gradients. In particular when a channel is significantly starved of flow rate and risks dryout, channel-to-channel thermal coupling can redistribute the heat load from the flow-starved channel to neighboring channels. The model is used to simulate the two-phase flow distribution in a system of two parallel channels driven by a constant flow rate pump. A comparison between thermally isolated and coupled channels indicates that thermally coupled channels are significantly less susceptible to maldistribution. Furthermore, a parametric study reveals that flow maldistribution is only possible in thermally coupled systems beyond a certain critical heat flux threshold. This threshold heat flux increases as the lateral wall conductance is increased, converging to a constant value in the limit of very high lateral conductance

Time-Resolved Characterization of Microchannel Flow Boiling During Transient Heating: Part 1 – Dynamic Response to a Single Heat Flux Pulse

Microchannel flow boiling is an attractive approach for the thermal management of high-heat-flux elec- tronic devices that are often operated in transient modes. In Part 1 of this two-part study, the dynamic response of a heated 500 μm channel undergoing flow boiling of HFE-7100 is experimentally investigated for a single heat flux pulse. Three heat flux levels exhibiting highly contrasting flow behavior under con- stant heating conditions are used: a low heat flux corresponding to single-phase flow (15 kW/m 2 ), an intermediate heat flux corresponding to continuous flow boiling (75 kW/m 2 ), and a very high heat flux which exceeds critical heat flux and would cause dryout if applied continuously (150 kW/m 2 ). Transient testing is conducted by pulsing between these three heat flux levels and varying the pulse duration. High-frequency measurements of heat flux, wall temperature, pressure drop, and mass flux are synchro- nized to high-speed flow visualizations to characterize the boiling dynamics during the pulses. At the onset of boiling, the dynamic response resembles that of an underdamped mass-spring-damper system subjected to a unit step input. During transitions between single-phase flow and time-periodic flow boil- ing, the wall temperature temporarily over/under-shoots the eventual steady operating temperature ( e.g. , by up to 20 °C) thus demonstrating that transient performance can extend beyond the bounds of steady performance. It is shown that longer duration high-heat-flux pulses (up to ~50% longer in some cases) can be withstood when the fluid in the microchannel is initial boiling, relative to if it is initially in the single-phase flow regime, despite being at an initially higher heat flux and wall temperature prior to the pulse