Design of a low-velocity impact framework for evaluating space-grade materials

Material deformation and failure under impact loading is a subject of active investigation in space science and often requires very specialized equipment for testing. In this work, we present the design, operational analysis and application of a low-velocity ($\sim 100$ m/s) projectile impact framework for evaluating the deformation and failure of space-grade materials. The system is designed to be modular and easily adaptable to various test geometries, while enabling accurate quantitative evaluation of plastic flow. Using coupled numerical methods and experimental techniques, we first establish an operating procedure for the system. Following this, its performance in two complementary impact configurations is demonstrated using numerical and experimental analysis. In the first, a Taylor impact test is performed for predicting the deformed shape of a cylindrical projectile impinging on a rigid substrate. In the second, deformation of a plate struck by a rigid projectile is evaluated. In both cases, physics-based models are used to interpret the resulting fields. We present a discussion of how the system may be used both for material property estimation (e.g., dynamic yield strength) as well as for failure evaluation (e.g., perforation and fracture) in the same projectile impact configuration

Onset of the aerobic nitrogen cycle during the Great Oxidation Event

The rise of oxygen on the early Earth (about 2.4 billion years ago)1 caused a reorganization of marine nutrient cycles2, 3, including that of nitrogen, which is important for controlling global primary productivity. However, current geochemical records4 lack the temporal resolution to address the nature and timing of the biogeochemical response to oxygenation directly. Here we couple records of ocean redox chemistry with nitrogen isotope (15N/14N) values from approximately 2.31-billion-year-old shales5 of the Rooihoogte and Timeball Hill formations in South Africa, deposited during the early stages of the first rise in atmospheric oxygen on the Earth (the Great Oxidation Event)6. Our data fill a gap of about 400 million years in the temporal 15N/14N record4 and provide evidence for the emergence of a pervasive aerobic marine nitrogen cycle. The interpretation of our nitrogen isotope data in the context of iron speciation and carbon isotope data suggests biogeochemical cycling across a dynamic redox boundary, with primary productivity fuelled by chemoautotrophic production and a nitrogen cycle dominated by nitrogen loss processes using newly available marine oxidants. This chemostratigraphic trend constrains the onset of widespread nitrate availability associated with ocean oxygenation. The rise of marine nitrate could have allowed for the rapid diversification and proliferation of nitrate-using cyanobacteria and, potentially, eukaryotic phytoplankton

Development of a processing map for the hot working of Ti-25Al-15Nb

A simple condition for metallurgical instability useful in the development of processing maps for analyzing the high temperature forming of metals, is used. This condition is deduced following a criterion based on continuum principles as applied to large plastic flow proposed by Ziegler, which can be applied for any type of flow stress versus strain rate curve. This criterion has been validated using the flow stress data of a alpha (2)/O titanium aluminide alloy Ti-25Al-15Nb with microstructural observations. The optimum hot working conditions are suggested for this material based on the processing map

Development of processing maps and constitutive relationship for thermomechanical processing of Aluminum Alloy AA2219

Isothermal uniaxial compression tests were conducted on aluminum alloy AA2219 to study the evolution of microstructure over a wide range of temperatures (300-500 °C) and strain rates (0.001-100 s−1) with a view to study the flow behavior and concurrent microstructural evolution. True stress-true strain curves showed only a gradual flow softening at all temperatures except at 300 °C where strain hardening was followed by severe flow softening. Processing map delineating the stable ‘safe’ and unstable ‘unsafe’ regions during hot working is developed and validated by comparing the microstructures observed in the deformed compression specimens. Optimum processing parameters (temperature 450 °C and strain rate 0.001 s−1) for hot deformation of AA2219 were proposed based on contour maps of efficiency of power dissipation and strain rate sensitivity parameter. The activation energy value (Qavg) of AA2219 for hot working was computed to be 169 kJ/mol. Finally, a constitutive equation for hot working of AA2219 was established as: ε˙=4.99×109⋅exp(0.06149σ)⋅exp(−168.958/RT)ε˙=4.99×109⋅exp⁡(0.06149σ)⋅exp⁡(−168.958/RT).by S. V. S. Narayana Murty, Aditya Sarkar, P. Ramesh Narayanan, P. V. Venkitakrishnan and Jyoti Mukhopadhya

Generation of Temperature Dependent Transversely Isotropic Properties for Zigzag and Armchair Single-Walled Carbon Nanotubes

Finite element analysis has been carried out to obtain temperature dependent transversely isotropic properties of the single-walled carbon nanotubes (SWCNTs). Finite element models of SWCNTs are generated by specifying the C-C bond rigidities. The five independent transversely isotropic properties for different chiralities are evaluated using the stress fields of thick-walled cylinders and the elastic deformations of SWCNTs subjected to pure extension, internal pressure and pure torsion loads. Empirical relations are provided for the five independent elastic constants useful to armchair and zigzag SWCNTs

Analysis of Microstructure and Texture Evolution in Mg-3Al-1Zn Alloy Processed Through Groove Rolling

The mechanism of grain refinement in a AZ31 Mg alloy subjected to hot groove rolling is investigated up to large strain (epsilon(t) similar to 2.5). The alloy shows enhanced yield strength without compromising ductility. The change in strain path during rolling has resulted in significant weakening of basal texture. The microstructure analyses show that dynamic recrystallization (DRX) contributed significantly to grain refinement and hence to the observed mechanical properties. The combined effects of DRX and texture evolution on mechanical properties have been addressed

High-Temperature Deformation Processing Map Approach for Obtaining the Desired Microstructure in a Multi-component (Ni-Ti-Cu-Fe) Alloy

An equiatomic NiTiCuFe multi-component alloy with simple body-centered cubic (bcc) and face-centered cubic solid-solution phases in the microstructure was processed by vacuum induction melting furnace under dynamic Ar atmosphere. High-temperature uniaxial compression experiments were conducted on it in the temperature range of 1073 K to 1303 K (800 degrees C to 1030 degrees C) and strain rate range of 10(-3) to 10(-1) s(-1). The data generated were analyzed with the aid of the dynamic materials model through which power dissipation efficiency and instability maps were generated so as to identify the governing deformation mechanisms that are operative in different temperature-strain rate regimes with the aid of complementary microstructural analysis of the deformed specimens. Results indicate that the stable domain for the high temperature deformation of the multi-component alloy occurs in the temperature range of 1173 K to 1303 K (900 degrees C to 1030 degrees C) and (epsilon) over dot range of 10(-3) to 10(-1.2) s(-1), and the deformation is unstable at T = 1073 K to 1153 K (800 degrees C to 880 degrees C) and (epsilon) over dot = 10(-3) to 10(-1.4) s(-1) as well as T = 1223 K to 1293 K (950 degrees C to 1020 degrees C) and (epsilon) over dot = 10(-1.4) to 10(-1) s(-1), with adiabatic shear banding, localized plastic flow, or cracking being the unstable mechanisms. A constitutive equation that describes the flow stress of NiTiCuFe multi-component alloy as a function of strain rate and deformation temperature was also determined. (C) The Minerals, Metals & Materials Society and ASM International 201