Simulations of precipitation kinetics in Ti2AlNb-based multiphase alloys synthesized by laser powder bed fusion

High-temperature Ti2AlNb-based alloys are structural candidate materials for weight reduction in engines and aircraft. The precipitation kinetics underlying the complex microstructure observed in Ti2AlNb-based alloys was investigated using computational tools for simulating diffusion controlled precipitation processes. The microstructure of alloys processed by laser powder bed fusion (LPBF) was investigated using electron microscopy. The phase fractions were determined by high-energy X-ray diffraction during in situ annealing of the samples. Precipitation reaction models were used as implemented in the Thermo-Calc PRISMA software in combination with a well-developed thermodynamic database, Thermo-Calc Software TCTI/Ti-alloys database version 3. In particular the volume fractions of strengthening phases were quantified during the simulations and final phase fractions tailored as a function of temperature and alloy composition. Different nucleation and growth mechanisms were simulated and correlated with experimental observations at relative early stages of the precipitation process. Moreover, we identify models’ limitations and key model parameters through a sensitivity analysis of the adjustable parameters using the parametric optimization software Optislang

Kinetics of the α→γ′α → γ′ stress-induced martensitic transformation in a Fe–Mn–Al–Ni shape memory bicrystal

The Fe–Mn–Al–Ni pseudoelastic system has garnered interest for diverse engineering applications owing to its promising characteristics. The poor pseudoelasticity in polycrystals is generally attributed to activation of new martensite variants and the high density of dislocations close to austenite/martensite interface. High-energy synchrotron X-ray diffraction and microscopy studies on a Fe–Mn–Al–Ni bicrystal reveal the sequence of transformation, deformation mechanisms, and grain boundary effects on martensite nucleation, shedding light on its limited pseudoelasticity in polycrystalline configurations. The results highlight challenges in achieving pseudoelasticity in polycrystalline configurations due to disparities in deformation between grains and at grain boundaries

Combining Atom-Probe Tomography and Synchrotron Methods to Investigate In-Situ Precipitation in AM-Produced Alloys

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