4,085 research outputs found
Dynamic Behavior in Piezoresponse Force Microscopy
Frequency dependent dynamic behavior in Piezoresponse Force Microscopy (PFM)
implemented on a beam-deflection atomic force microscope (AFM) is analyzed
using a combination of modeling and experimental measurements. The PFM signal
comprises contributions from local electrostatic forces acting on the tip,
distributed forces acting on the cantilever, and three components of the
electromechanical response vector. These interactions result in the bending and
torsion of the cantilever, detected as vertical and lateral PFM signals. The
relative magnitudes of these contributions depend on geometric parameters of
the system, the stiffness and frictional forces of tip-surface junction, and
operation frequencies. The dynamic signal formation mechanism in PFM is
analyzed and conditions for optimal PFM imaging are formulated. The
experimental approach for probing cantilever dynamics using frequency-bias
spectroscopy and deconvolution of electromechanical and electrostatic contrast
is implemented.Comment: 65 pages, 15 figures, high quality version available upon reques
Direct Measurement of Periodic Electric Forces in Liquids
The electric forces acting on an atomic force microscope tip in solution have
been measured using a microelectrochemical cell formed by two periodically
biased electrodes. The forces were measured as a function of lift height and
bias amplitude and frequency, providing insight into electrostatic interactions
in liquids. Real-space mapping of the vertical and lateral components of
electrostatic forces acting on the tip from the deflection and torsion of the
cantilever is demonstrated. This method enables direct probing of electrostatic
and convective forces involved in electrophoretic and dielectroforetic
self-assembly and electrical tweezer operation in liquid environments
In Silico Comparison of Phase Maps Based on Action Potential and Extracellular Potential
In this work, a computer simulation of the reentrant ventricular tachycardia (VT) was used to investigate the peculiar properties of phase maps based on transmembrane potentials (TP) and extracellular potentials (EP). The simulation approach included the bidomain model with full myocardium-torso coupling, a realistic ionic model of the human cardiomyocytes and a personalized geometry of the heart and torso. The phase mapping pipeline includes a signal detrending and the Hilbert transform. It was demonstrated that TP-based phase maps correlated well with the propagation of cardiac excitation. In contrast, EP-based phase mapping provides some aberrations which can complicate electrophysiological interpretation of the phase maps in terms of cardiac activation sequence. It was also shown that a modification of the phase computation algorithm, including the sign inversion of signals and a special transformation of the phase plot, can partially eliminate these aberrations and make EP-based phase maps resemble TP-based maps. © 2018 Creative Commons Attribution.Russian Foundation for Basic Research, RFBR: 18-31-00401The reported study was funded by RFBR according to the research project No. 18-31-00401. Development of computer model with personalized geometry was funded by IIP UrB RAS theme No AAAA-A18-118020590031-8, RF Government Act #211 of March 16, 2013 (agreement 02.A03.21.0006), Program of the Presidium RAS #27 (project AAAA-A18-118020590030-1)
Domain Dynamics in Piezoresponse Force Microscopy: Quantitative Deconvolution and Hysteresis Loop Fine Structure
Domain dynamics in the Piezoresponse Force Spectroscopy (PFS) experiment is
studied using the combination of local hysteresis loop acquisition with
simultaneous domain imaging. The analytical theory for PFS signal from domain
of arbitrary cross-section is developed and used for the analysis of
experimental data on Pb(Zr,Ti)O3 polycrystalline films. The results suggest
formation of oblate domain at early stage of the domain nucleation and growth,
consistent with efficient screening of depolarization field within the
material. The fine structure of the hysteresis loop is shown to be related to
the observed jumps in the domain geometry during domain wall propagation
(nanoscale Barkhausen jumps), indicative of strong domain-defect interactions.Comment: 17 pages, 3 figures, 2 Appendices, to be submmited to Appl. Phys.
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