Influence of austenite stability on predicted cyclic stress-strain response of metastable austenitic steels

AbstractA modeling approach that captures the plastic strain amplitude dependence of strain induced martensite fraction evolution during low cycle fatigue (LCF) loading of metastable austenitic steels has been developed. The model is based on a modified version of the Olson-Cohen kinetic equation that retains connection to the underlying mechanisms of the transformation by relating cyclic austenite stability to monotonic stability. The kinetic model is then input into an evolving composite mechanical model that relies on a simple rule of mixtures formulation to predict cyclic stress-strain behavior, including increases in stress amplitude due to martensitic transformation. Predictions from the modeling approach compare well to fatigue data in the literature for AISI 304 stainless steel

Extreme value statistical analysis to determine the endurance limit of a 1045 induction hardened steel alloy

AbstractSurface hardened components are used in fatigue critical applications such as axles and gears. Inclusions are critical microstructural features where fatigue cracks have been observed to nucleate in these parts. In this investigation, the effect of inclusion populations on fatigue performance of induction hardened 1045 steel was examined. The steel was heat treated to have a tempered martensite starting microstructure and was induction hardened to two different case depths. Utilizing extreme value statistical analysis, the largest inclusion as well as the largest inclusion in each of five categories, MnS, MnCaS, MnAlS, Al2O3, and Al2O3-MgO, was estimated for a critically stressed area in a fully reversed cantilever bending fatigue sample. The inclusion size estimates were used to predict the endurance limit of the sample with a fracture mechanics-based model. This methodology has been traditionally used for homogeneous materials but has been modified here for bending fatigue and inhomogeneous case hardened material. The predicted endurance limits are closely correlated to experimentally measured endurance limits

Thermal and mechanical stability of retained austenite surrounded by martensite with different degrees of tempering

The mechanical and thermal stability of austenite in multiphase advanced high strength steels are influenced by the surrounding microstructure. The mechanisms underlying and the relations between thermal and mechanical stability are still dubious due to the difficulty of isolating other factors influencing austenite stability. In this work, martensite/austenite microstructures were created with the only significant difference being the degree of tempering of the martensite matrix. Hence, the effect of tempering in martensite is isolated from other factors influencing the stability of austenite. The thermal stability during heating of retained austenite was evaluated by monitoring phase fractions as a function of controlled temperature employing both dilatometry and magnetometry measurements. The mechanical stability was studied by performing interrupted tensile tests and determining the remaining austenite fraction at different levels of strain. The thermal stability of this remaining austenite after interrupted tests was studied by subsequent reheating of strained specimens. The results are evidence for the first time that thermal recovery of martensite during reheating assists austenite decomposition through shrinkage and softening of martensite caused by a reduction of dislocation density and carbon content in solid solution. This softening of martensite also leads to a subsequent reduction of austenite mechanical stability. Additionally, remaining austenite after pre-straining at room temperature was thermally less stable than before pre-straining, demonstrating that plastic deformation has opposing effects on thermal and mechanical stability.(OLD) MSE-

Controlling the work hardening of martensite to increase the strength/ductility balance in quenched and partitioned steels

The role of retained austenite on tensile behavior in quenched and partitioned (Q&P) steels has been studied extensively, but the deformation behavior of martensite, which comprises the majority of Q&P microstructures, has received less attention. In this investigation, martensite properties were varied through heat treatment in a low carbon Q&P steel consisting of retained austenite and martensite. Additional conditions were produced by reheating the Q&P steel to 450 °C for 30 min or to 700 °C followed immediately by quenching. The reheated microstructures contained similar fractions of retained austenite as the non-reheated Q&P microstructures, but reheating tempered the martensite, thereby decreasing martensite dislocation density. The reheated conditions had a lower yield stress and initial work hardening rate than the non-reheated Q&P condition. However, the reheated conditions had a greater work hardening rate at larger strains and greater uniform strain due to less stable retained austenite. Furthermore, the tensile strength of the condition reheated to 450 °C was nearly equal to the non-reheated condition. In addition to retained austenite to martensite transformation, the early stage work hardening rate of martensite is critical to ductility and is dependent on martensite dislocation density, which can be decreased through tempering.(OLD) MSE-3(OLD) MSE-

Interplay between metastable phases controls strength and ductility in steels

By means of high-energy synchrotron X-ray diffraction, the interplay between martensite and retained austenite phases in steel during the application of stress has been analyzed. Martensite properties were varied through controlled reheating heat treatments in a low carbon Quenched and Partitioned (Q&P) steel consisting of retained austenite and martensite. The reheating treatments significantly altered martensite strength while keeping the same fractions of retained austenite as the non-reheated Q&P microstructures, resulting in different degrees of stress partitioning and work hardening of the individual microconstituents. Results of this study show that the strength ratio between the different phases in the microstructure plays a crucial role in the onset and rate of mechanically induced decomposition of retained austenite. Consequently, the strength ratio between phases controls the yielding and work-hardening of the material.(OLD) MSE-3(OLD) MSE-

Influence of selected alloying variations on liquid metal embrittlement susceptibility of quenched and partitioned steels

In this work, the influence of selected alloying variations on Zn-assisted liquid metal embrittlement (LME) susceptibility of Zn-coated advanced high strength steels (AHSS) is investigated. Cold-rolled AHSS alloys of different carbon (C), manganese (Mn), silicon (Si), and aluminum (Al) concentrations were continuous-annealed to generate a third generation AHSS microstructure (composed of martensite and retained austenite) via quenching and partitioning. High temperature tension tests using simulated spot-weld thermomechanical cycles revealed no significant influence of C and Mn variations on the Zn-LME susceptibility of AHSS. On the other hand, Zn-LME susceptibility was strongly correlated with the Si content of AHSS. A direct comparison of the (reacted) coating microstructures of the Si-alloyed and Low-Si AHSS variants revealed that Si in the AHSS substrate suppresses Fe–Zn alloying reactions and retards the nucleation and growth of Fe-Zn intermetallic phases at the coating-substrate interface in these spot weld simulations. The suppressed intermetallic formation at elevated Si concentrations is consistent with phase equilibria considerations in the Fe-Zn-Si ternary system. In the context of Zn-assisted LME, therefore, Si is hypothesized to aggravate LME behavior by increasing the liquid Zn availability for embrittlement and promoting direct contact between liquid Zn and the AHSS steel substrate