Torque Measurements and DEM Simulations in a Couette-type Device with Application to Particle Size Measurements

A continuously operating modified Cuette-type shearing device has been developed for in-situ measurements to estimate the average particle size during size enlargement processes in fluidized bed granulator. It was proven by experiments that well-defined correlation exists between the mean torque and the average particle size being in the device. DEM simulations revealed interesting aspects of this method

Computer Tomograph Measurements in Shear and Gravity Particle Flows

The paper reports the recent results obtained on the applicability of cross-sectional digital imaging method to study particle flow characteristics in 3D particle beds forced to move by gravity or shear. X-ray CT imaging technique is widely used in medical diagnostics and, during the last decades, its spatial and temporal resolution has been improved significantly. In this study, an attempt was made to use this technique for engineering purposes. Two experimental set-ups with different types of particle flows were investigated using Siemens Somatom Plus type CT equipment. A series of trials were carried out in a small model hopper with flat bottom and almost cylindrical side wall slightly deviating from verticality. Non steady-state flow was studied during the outflow of particulate material from this vessel, through a central hole at the bottom. Further investigation was fulfilled in a modified Cuette-type shearing device to study steady-state shear flow. This equipment consisted of an almost cylindrical vessel identical to that used for gravity flow measurements, and a smaller inner cylinder rotating within this vessel concentrically, around its vertical axis. The surface of the inner cylinder was notched vertically, i.e. perpendicularly to the direction of rotation to increase wall friction between the particles and the cylinder. Almost spherical sucrose granules, also used for gravity flow measurements, were filled into the gap between the rotating cylinder and the outer wall of the equipment. Movement of particles took place due to shear, generated within the particle bed. By using X-ray CT technique, cross-sectional digital images were obtained in every two seconds for both types of particle flows. For this, the cross-sectional variation of the local Hounsfield density values were measured in a matrix of 0.1x0.1x2.0 mm space elements. It was proved that the applied non-invasive crosssectional imaging technique was suitable to distinguish the stationary and moving particle regions, and by this, to estimate the location of the boundary zone between them

The effects of leaching from alkaline red mud on soil biota: modelling the conditions after the Hungarian red mud disaster

A soil column experiment was set up to investigate the effect of red mud from Ajka (Hungary) on a typical soil profile from the concerned area. The chemical changes caused by the leachate of the red mud and the effects of these changes on living organisms were assessed. Ecotoxicological tests with Vibrio fischeri, Sinapis alba and Folsomia candida were performed and the number of aerobic heterotrophic microorganisms was determined. The total, plant available, exchangeable and water soluble fractions of Na, Mo, Cu, and Cr increased in the soil mostly due to their leaching from the red mud layer and partly to the increase of the pH and DOC concentration. The chemical changes had significant effects on the test organisms only in the 0 – 30 cm soil layer except for F. candida that had a lower survival rate also in the 30 – 50 cm soil layer. There were no severe toxic effects detected on the test organisms. Furthermore in case of the aerobic heterotrophic cell number and S. alba germination a stimulating effect was revealed. However, the red mud itself was toxic, therefore the performed ecotoxicology tests have justified the removal of red mud from the soil surface after the disaster

Structure-property and composition-property relationships for poly(ethylene terephthalate) surfaces modified by helium plasma-based ion implantation

The surfaces of untreated and helium plasma-based ion implantation (He PBII) treated poly(ethylene terephthalate) (PET) samples were characterised by reflectance colorimetry, contact angle studies and measurements of surface electrical resistance. The results were related to the structural and compositional data obtained by the authors earlier on parallel samples by XPS and Raman spectroscopy. Inverse correlations between lightness and ID/IG ratio and between chroma and ID/IG ratio were obtained, suggesting that the PBII-treated PET samples darken and their colourfulness decreases with the increase of the portion of aromatic sp2 carbon rings in the chemical structure of the modified layer. Direct correlation between water contact angle and the ID/IG ratio and inverse correlations between surface energy and ID/IG ratio and between dispersive component of surface energy and ID/IG ratio were found, reflecting that surface wettability, surface energy and its dispersive component decrease with the formation of surface structure, characterised again by enhanced portion of aromatic sp2 carbon rings. The surface electrical resistance decreased with the increase of the surface C-content determined by XPS and also with the increase of the surface concentration of conjugated double bonds, reflected by the increase of the pi-pi* shake-up satellite of the C 1s peak