105 research outputs found

    2-(4-Iodo­phen­yl)-1,2,3,4-tetra­hydro­isoquinoline-1-carbonitrile

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    In the title compound, C16H13IN2, the benzene ring of the tetra­hydro­isoquinoline moiety makes a dihedral angle of 45.02 (9)° with the benzene ring of the 4-iodo­phenyl fragment. The N atom and the adjacent unsubstituted C atom of the tetra­hydro­isoquinoline unit are displaced by 0.294 (2) and 0.441 (3) Å, respectively, from the plane through the remaining eight C atoms. In the crystal, pairs of adjacent mol­ecules are linked into dimers by weak inter­molecular C—H⋯π inter­actions

    2-(4-Bromo­phen­yl)-3,4-dihydro­isoquinolin-2-ium thio­cyanate hemihydrate

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    In the title hemihydrated salt, C15H13BrN+·NCS−·0.5H2O, the two benzene rings are aligned at a dihedral angle of 46.9 (1)°. The six-membered heterocycle of the dihydro­isoquinoline unit adopts a half-chair conformation. The water mol­ecule and thio­cyanate ion are linked by O—H⋯N hydrogen bonds, generating a four-membered ring motif. In addition, C—H⋯O and C—H⋯S inter­actions link the components into a chain along the c axis. π–π inter­actions [centroid–centroid distance = 3.974 (2) Å] link the chains into sheets and further π—π [centroid–centroid distance = 3.746 (2) Å] and C—H⋯π inter­actions give rise to a three-dimensional nework

    2-(2-Hy­droxy­phen­yl)-3,4-dihydro­iso­quinolin-1(2H)-one

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    There are two independent mol­ecules in the asymmetric unit of the title compound, C15H13NO2, in both the six-membered dihydro­pyridine rings adopt a half-chair conformation. The two benzene rings make dihedral angles of 43.66 (10) and 62.22 (10)° in the two mol­ecules. In the crystal, the two independent mol­ecules are linked alternately by inter­molecular O—H⋯O hydrogen bonds, forming a zigzag chain along the c axis. Furthermore, inter­molecular C—H⋯π inter­actions link the chains into a three-dimensional network

    Optical thermal filters for eXTP: Manufacturing and characterization

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    In order to ensure the effective detection of X-ray astronomical detectors by blocking ultraviolet, visible and infrared light, adding optical thermal filter in front of the load is an effective method. According to the scientific requirements of eXTP, optical thermal filters with aluminized polyimide (PI) film structure had been designed and tested in this paper, the results of mechanical tests including burst pressure, vibration and acoustic tests, also the transparent properties of optics in UV, Vis and IR lights are presented. The mechanical test results show that the filters for LAD and SFA can't pass the acoustic tests, causing the thickness of PI should be increased or a nickel mesh structure should be added. Furthermore, the transmission test results indicate that a single-sided Al deposited structure is more suitable than a double-sided one
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