Low-Cycle Fatigue of Ultra-Fine-Grained Cryomilled 5083 Aluminum Alloy

The cyclic deformation behavior of cryomilled (CM) AA5083 alloys was compared to that of conventional AA5083-H131. The materials studied were a 100 pct CM alloy with a Gaussian grain size average of 315 nm and an alloy created by mixing 85 pct CM powder with 15 pct unmilled powder before consolidation to fabricate a plate with a bimodal grain size distribution with peak averages at 240 nm and 1.8 μm. Although the ultra-fine-grain (UFG) alloys exhibited considerably higher tensile strengths than those of the conventional material, the results from plastic-strain-controlled low-cycle fatigue tests demonstrate that all three materials exhibit identical fatigue lives across a range of plastic strain amplitudes. The CM materials exhibited softening during the first cycle, similar to other alloys produced by conventional powder metallurgy, followed by continual hardening to saturation before failure. The results reported in this study show that fatigue deformation in the CM material is accompanied by slight grain growth, pinning of dislocations at the grain boundaries, and grain rotation to produce macroscopic slip bands that localize strain, creating a single dominant fatigue crack. In contrast, the conventional alloy exhibits a cell structure and more diffuse fatigue damage accumulation

A Novel 2D Folding Technique for Enhancing Fermi Surface Signatures in the Momentum Density: Application to Compton Scattering Data from an Al-3at%Li Disordered Alloy

We present a novel technique for enhancing Fermi surface (FS) signatures in the 2D distribution obtained after the 3D momentum density in a crystal is projected along a specific direction in momentum space. These results are useful for investigating fermiology via high resolution Compton scattering and positron annihilation spectroscopies. We focus on the particular case of the (110) projection in an fcc crystal where the standard approach based on the use of the Lock-Crisp-West (LCW) folding theorem fails to give a clear FS image due to the strong overlap with FS images obtained through projection from higher Brillouin zones. We show how these superposed FS images can be disentangled by using a selected set of reciprocal lattice vectors in the folding process. The applicability of our partial folding scheme is illustrated by considering Compton spectra from an Al-3at%Li disordered alloy single crystal. For this purpose, high resolution Compton profiles along nine directions in the (110) plane were measured. Corresponding highly accurate theoretical profiles in Al-3at%Li were computed within the local density approximation (LDA)-based Korringa-Kohn-Rostoker coherent potential approximation (KKR-CPA) first-principles framework. A good level of overall accord between theory and experiment is obtained, some expected discrepancies reflecting electron correlation effects notwithstanding, and the partial folding scheme is shown to yield a clear FS image in the (110) plane in Al-3%Li.Comment: 24 pages, 8 figures, to appear in Phys. Rev.

Relationship Between the Thermodynamic Parameters, Structure, and Anticorrosion Properties of Al-Zr-Ni-Fe-Y Alloys

The influence of the chemical composition on the crystallization process, amorphous phase formation, and the anticorrosion properties of Al-Zr-Ni-Fe-Y alloys are presented. To reduce the number of experiments, a thermodynamic approach was applied in which the entropy and Gibbs free energy of representative alloys were optimized. The low glass-forming ability of Al-Zr-Ni-Fe-Y alloy systems was related to the crystallization of the Al3Zr phase from the melt. The structural analysis showed that phases containing Ni and Fe, such as Al19Ni5Y3, Al10Fe2Y, and Al23Ni6Y4, played a key role in the formation of amorphous alloys. According to this, the simultaneous addition of Ni/Fe and Y is important to prevent the crystallization of Al-based alloys in the melt. The formation of an amorphous phase in Al80Zr5Ni5Fe5Y5 alloys and the complete amorphization of Al85Ni5Fe5Y5 alloys were responsible for the high corrosion resistance compared with fully crystalline alloys. Moreover, the addition of Y had a significant impact on the anticorrosion properties. The XPS results showed that the alloys tended to form a passive Al2O3 and Y2O3 layer on the surface

Effect of preparation methods on the incorporation/distribution of ceramic particulates in metal based composite powders

Materials Transactions, JIM363451-457MTJI

Effect of processing on the microstructural variation and heat-treatment response of a hypercutectic AlSi alloy

Journal of Materials Processing Tech.541-4261-270JMPT

Synthesis and microstructural characterization of metal based composite powders

Scripta Metallurgica et Materiala30111377-138

TEM investigation on microstructural characteristics in nanostructured Al-Mg alloy

The microstructural evolution in a nanostructured Al-Mg alloy fabricated by cryogenic mechanical alloying (cryomilling), was investigated using transmission electron microscopy (TEM). Nanostructured Al-Mg powders were first synthesized by a mechanical alloying under liquid nitrogen media (cryomilling), and the powders were Subsequently degassed, hot isostatically pressed, and extruded into a full dense, bulk form. The results showed that Si containing phases and (Fe,Ni)Al intermetallics existed in as-extruded Al-Mg alloy. In addition, the extrusion temperature has a strong influence on the formation of microstructural anisotropy. A lower extrusion temperature yields a microstructure that is more anisotropic relative to that present at the higher extrusion temperature. More specifically, at the lower temperature, the nano-sized Al grains have a tendency to rotate towards the direction, along the extrusion direction.11sciescopu

Wear of a spray-deposited hypereutectic aluminium-silicon alloy

Journal of Materials Processing Technology631-3865-870JMPT