The influence of containerless undercooling and rapid solid-state quenching on the superconductive and magnetic properties of some clustering alloy systems

The properties of clustering alloy systems and the manner in which they are influenced by rapid quenching from a containerless undercooled melt are discussed. It was postulated that rapid quenching under such conditions would result in highly disordered metastable alloys, and furthermore, that alloys in such conditions would possess physical properties characteristically different from those of alloys in the annealed equilibrium state. The scope of the program is essentially to gauge the influence of containerless undercooling on the submicrostructure of clustering-type alloys, using certain physical properties as diagnostic tools. Microstructures and macrostructures were to be examined using optical- and scanning-electron microscopy

Analytical study of space processing of immiscible materials for superconductors and electrical contacts

The results of a study conducted to determine the role space processing or materials research in space plays in the superconductor and electrical contact industries are presented. Visits were made to manufacturers, users, and research organizations connected with these products to provide information about the potential benefits of the space environment and to exchange views on the utilization of space facilities for manufacture, process development, or research. In addition, space experiments were suggested which could result in improved terrestrial processes or products. Notable examples of these are, in the case of superconductors, the development of Nb-bronze alloys (Tsuei alloys) and, in the electrical contact field, the production of Ag-Ni or Ag-metal oxide alloys with controlled microstructure for research and development activities as well as for product development. A preliminary experimental effort to produce and evaluate rapidly cooled Pb-Zn and Cu-Nb-Sn alloys in order to understand the relationship between microstructure and superconducting properties and to simulate the fine structure potentially achievable by space processing was also described

Increases in the Irreversibility Field and the Upper Critical Field of Bulk MgB2 by ZrB2 Addition

In a study of the influence of ZrB2 additions on the irreversibility field, Birr and the upper critical field Bc2, bulk samples with 7.5 at. % ZrB2 additions were made by a powder milling and compaction technique. These samples were then heated to 700-900C for 0.5 hours. Resistive transitions were measured at 4.2 K and Birr and Bc2 values were determined. An increase in Bc2 from 20.5 T to 28.6 T and enhancement of Birr from 16 T to 24 T were observed in the ZrB2 doped sample as compared to the binary sample at 4.2 K. Critical field increases similar to those found with SiC doping were seen at 4.2 K. At higher temperatures, increases in Birr were also determined by M-H loop extrapolation and closure. Values of Birr which were enhanced with ZrB2 doping (as compared to the binary) were seen at temperatures up to 34 K, with Birr values larger than those for SiC doped samples at higher temperatures. The transition temperature, Tc, was then measured using DC susceptibility and a 2.5 K drop of the midpoint of Tc was observed. The critical current density was determined using magnetic measurements and was found to increase at all temperatures between 4.2 K and 35 K with ZrB2 doping.Comment: 15 pages, 5 figs, 1 tabl

AC Loss and Contact Resistance In Copper-Stabilized Nb3Al Rutherford Cables with and without a Stainless Steel Core

Calorimetric measurements of AC loss and hence interstrand contact resistance (ICR), were measured on three samples of Rutherford cable wound with Cu-stabilized jelly-roll type unplated Nb3Al strand. One of the cable types was furnished with a thin core of AISI 316L stainless steel and the other two were both uncored but insulated in different ways. The cables were subjected to a room-temperature-applied uniaxial pressure of 12 MPa that was maintained during the reaction heat treatment (RHT), then vacuum impregnated with CTD 101 epoxy, and repressurized to 100 MPa during AC-loss measurement. The measurements were performed at 4.2 K in a sinusoidal field of amplitude 400 mT at frequencies of 1 to 90 mHz (no DC-bias field) that was applied both perpendicular and parallel to the face of the cable (the face-on, FO, and edge-on, EO, directions, respectively). For the cored cable the FO-measured effective ICR (FO-ICR), was 5.27 . Those for the uncored cables were less than 0.08 . As shown previously for NbTi- and Nb3Sn-based Rutherford cables, the FO-ICR can be significantly increased by the insertion of a core, although in this case it is still below the range recommended for accelerator-magnet use. Post-measurement dissection of one of the cables showed that the impregnating resin had permeated between the strands and coated the core with a thin, insulating layer excepting for some sintered points of contact. In the uncored cables the strands were coated with resin except for the points of interstrand contact. It is suggested that in the latter case this tendency for partial coating leads to a processing-sensitive FO-ICR.Comment: Four pages, with two figure

Transport and magnetic Jc of MgB2 strands and small helical coils

The critical current densities of MgB2 monofilamentary strands with and without SiC additions were measured at 4.2 K. Additionally, magnetic Jc at B = 1 T was measured from 4.2 K to 40 K. Various heat treatment times and temperatures were investigated for both short samples and small helical coils. SiC additions were seen to improve high field transport Jc at 4.2 K, but improvements were not evident at 1 T at any temperature. Transport results were relatively insensitive to heat treatment times and temperatures for both short samples and coils in the 700C to 900C range.Comment: 8 text pages, 1 table, 4 fig

Stability mechanical considerations, and AC loss in HTSC monoliths, coils, and wires

For monolithic high-T(sub c) superconductors (HTSC's) calculations are presented of: (1) the initial flux jump field, H(sub fj), in melt-processed YBCO based on a field and temperature dependent J(sub c), and (2) the radial and circumferential stresses in solid and hollow cylinders containing trapped magnetic flux. For model multi filamentary (MF) HTSC/Ag strands calculations are presented of: (1) the limiting filament diameters for adiabatic and dynamic stability, and (2) the hysteretic and eddy current components of AC loss. Again for MF HTSC/Ag composite strands the need for filamentary subdivision and twisting is discussed