Rapid method for determining nitrogen in tantalum and niobium alloys

Adaptation of commercial instrument which measures nitrogen and oxygen in steel gave results in less than four minutes. Sample is heated in helium atmosphere in single-use graphite crucible. Platinum flux facilitates melting of sample. Released gases are separated chromatographically and measured in thermal-conductivity cell

Procedure for rapid determination of nickel, cobalt, and chromium in airborne particulate samples

A rapid, selective procedure for the determination of 1 to 20 micrograms of nickel, chromium, and cobalt in airborne particulates is described. The method utilizes the combined techniques of low temperature ashing and atomic absorption spectroscopy. The airborne particulates are collected on analytical filter paper. The filter papers are ashed, and the residues are dissolved in hydrochloric acid. Nickel, chromium, and cobalt are determined directly with good precision and accuracy by means of atomic absorption. The effects of flame type, burner height, slit width, and lamp current on the atomic absorption measurements are reported

Galaxy Tracers and Velocity Bias

This paper examines several methods of tracing galaxies in N-body simulations and their effects on the derived galaxy statistics, especially measurements of velocity bias. Using two simulations with identical initial conditions, one following dark matter only and the other following dark matter and baryons, both collisionless and collisional methods of tracing galaxies are compared to one another and against a set of idealized criteria. None of the collisionless methods proves satisfactory, including an elaborate scheme developed here to circumvent previously known problems. The main problem is that galactic overdensities are both secularly and impulsively disrupted while orbiting in cluster potentials. With dissipation, the baryonic tracers have much higher density contrasts and much smaller cross sections, allowing them to remain distinct within the cluster potential. The question remains whether the incomplete physical model introduces systematic biases. Statistical measures determined from simulations can vary significantly based solely on the galaxy tracing method utilized. The two point correlation function differs most on sub-cluster scales with generally good agreement on larger scales. Pairwise velocity dispersions show less uniformity on all scales addressed here. All tracing methods show a velocity bias to varying degrees, but the predictions are not firm: either the tracing method is not robust or the statistical significance has not been demonstrated. Though theoretical arguments suggest that a mild velocity bias should exist, simulation results are not yet conclusive.Comment: ApJ, in press, 23 pages, plain TeX, 8 of 13 figures included, all PostScript figures (4.8 MB) available via anonymous ftp from ftp://astro.princeton.edu/summers/tracers . Also available as POPe-616 on http://astro.princeton.edu/~library/prep.htm

Instrument Systems Analysis and Verification Facility (ISAVF) users guide

The ISAVF facility is primarily an interconnected system of computers, special purpose real time hardware, and associated generalized software systems, which will permit the Instrument System Analysts, Design Engineers and Instrument Scientists, to perform trade off studies, specification development, instrument modeling, and verification of the instrument, hardware performance. It is not the intent of the ISAVF to duplicate or replace existing special purpose facilities such as the Code 710 Optical Laboratories or the Code 750 Test and Evaluation facilities. The ISAVF will provide data acquisition and control services for these facilities, as needed, using remote computer stations attached to the main ISAVF computers via dedicated communication lines

Zeolite phi: a physical mixture of chabazite and offretite

Zeolite Phi is synthesized by two methods reported previously. Results from X-ray powder diffraction and scanning electron microscopy suggest that the materials are physical mixtures of chabazite and offretite; one sample has a small amount of phillipsite. The X-ray powder diffraction data from these samples, and those reported previously, are indexed and their unit-cell parameters compare well to those obtained from a physical mixture of chabazite and offretite. These samples show multiple particle morphologies that are indicative of physical mixtures. Zeolite Phi is concluded to be a physical mixture of chabazite and offretite and we suggest that the use of the name zeolite Phi be discontinued

The development and properties of the support needs questionnaire

Abstract: The Support Needs Questionnaire (SNQ) measures the support people with severe mental illness need to attain valued social roles as a route to social inclusion. Its design derives from Wolfensberger’s Social Role Valorisation theory. It is a clinical tool comprising a comprehensive lifestyle inventory of “universal basic” and “disability” needs; and ‘revalorisation needs’ arising from social devaluation and deep exclusion. The SNQ comprises eight discreet sub-scales based on O’Brien’s Five Service Accomplishments, the domains of which include Community Presence, Community Participation, Choice and Control, Social Roles and Respect, Skills and Competencies, and Finance. There are also two descriptive sub-scales: Physical and Mental Health. The item set was developed collaboratively with service users. This paper introduces the SNQ, its design rationale and development, and investigates aspects of its reliability, validity and utility. Care co-ordinators in a Community Mental Health Team rated eighty-two service users’ support needs at a two week interval using the SNQ, the Global Assessment Scale and the MARC-2. The SNQ is shown to have high test-retest reliability, good construct and concurrent validity, and good discriminatory power. It exhibited no floor or ceiling effects with the reference population. It could be used with a more diverse population. The descriptive sub-scales were weakest. The population profile showed moderate support was required for physical integration but high levels for social integration which is consistent with previous research. The SNQ has some good psychometric properties. Future research should address internal consistency and potential item redundancy, determine inter-rater reliability and change sensitivity

The genomics of neonatal abstinence syndrome

Significant variability has been observed in the development and severity of neonatal abstinence syndrome (NAS) among neonates exposed to prenatal opioids. Since maternal opioid dose does not appear to correlate directly with neonatal outcome, maternal, placental, and fetal genomic variants may play important roles in NAS. Previous studies in small cohorts have demonstrated associations of variants in maternal and infant genes that encode the μ-opioid receptor (OPRM1), catechol-O-methyltransferase (COMT), and prepronociceptin (PNOC) with a shorter length of hospital stay and less need for treatment in neonates exposed to opioids in utero. Consistently falling genomic sequencing costs and computational approaches to predict variant function will permit unbiased discovery of genomic variants and gene pathways associated with differences in maternal and fetal opioid pharmacokinetics and pharmacodynamics and with placental opioid transport and metabolism. Discovery of pathogenic variants should permit better delineation of the risk of developing more severe forms of NAS. This review provides a summary of the current role of genomic factors in the development of NAS and suggests strategies for further genomic discovery