1,637 research outputs found
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Direct iminization of PEEK
Semi-crystalline poly(ether ketone)s are important high-temperature engineering thermoplastics, but are difficult to characterize at the molecular level because of their insolubility in conventional organic solvents. Here we report that polymers of this type, including PEEK, react cleanly at high temperatures with low-volatility aralkyl amines to afford stable, noncrystalline poly(ether-imine)s, which are readily soluble in solvents such as chloroform, THF and DMF and so characterizable by conventional size-exclusion chromatography
The Decay with Highly Improved Staggered Quarks and NRQCD
We report on progress of a lattice QCD calculation of the and
semileptonic form factors. We use a relativistic staggered
action (HISQ) for light and charm quarks, and an improved non-relativistic
(NRQCD) action for bottom, on the second generation MILC ensembles.Comment: Presented at Lattice 2017, the 35th International Symposium on
Lattice Field Theory at Granada, Spain (18-24 June 2017
Υ and Υ′ leptonic widths, abμ, and mb from full lattice QCD
We determine the decay rate to leptons of the ground-state ϒ meson and its first radial excitation in lattice
QCD for the first time. We use radiatively improved nonrelativistic QCD for the b quarks and include u, d,
s and c quarks in the sea with u=d masses down to their physical values. We find Γðϒ → eþe−Þ ¼
1.19ð11Þ keV and Γðϒ0 → eþe−Þ ¼ 0.69ð9Þ keV, both in good agreement with experimental results. The
decay constants we obtain are included in a summary plot of meson decay constants from lattice QCD
given in the Conclusions. We also test time moments of the vector current-current correlator against values
determined from the b-quark contribution to σðeþe− → hadronsÞ and calculate the b-quark piece of the
hadronic vacuum polarization contribution to the anomalous magnetic moment of the muon,
ab
μ ¼ 0.271ð37Þ × 10−10. Finally we determine the b-quark mass, obtaining in the MS scheme, ¯
m¯ bðm¯ b; nf ¼ 5Þ ¼ 4.196ð23Þ GeV, the most accurate result from lattice QCD to date
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Synthesis, x-ray structure and anion binding properties of a cryptand-like hybrid calixpyrrole
The novel cryptand in/out-3, containing two tripyrrolemethane units briged by three 1,3- diisopropylidenbenzene arms was readily synthesized by a convergent three-step synthesis. It binds fluoride by inclusion with excellent selectivity with respect to a number of other tested anions. The structure of the free receptor and that of its fluoride complex were investigated in solution by NMR spectroscopy. The solid state X-ray structure of the free cryptand 3 was also determined
B-meson decay constants: a more complete picture from full lattice QCD
We extend the picture of -meson decay constants obtained in lattice QCD
beyond those of the , and to give the first full lattice QCD
results for the , and . We use improved NonRelativistic QCD
for the valence quark and the Highly Improved Staggered Quark (HISQ) action
for the lighter quarks on gluon field configurations that include the effect of
, and quarks in the sea with quark masses going down to
physical values. For the ratio of vector to pseudoscalar decay constants, we
find = 0.941(26), = 0.953(23) (both
less than 1.0) and = 0.988(27). Taking correlated
uncertainties into account we see clear indications that the ratio increases as
the mass of the lighter quark increases. We compare our results to those using
the HISQ formalism for all quarks and find good agreement both on decay
constant values when the heaviest quark is a and on the dependence on the
mass of the heaviest quark in the region of the . Finally, we give an
overview plot of decay constants for gold-plated mesons, the most complete
picture of these hadronic parameters to date.Comment: 20 pages, 9 figures. Minor updates to the discussion in several
places and some additional reference
Ascanius Project: MECH 401/402 Senior Capstone Experience
This report describes the analysis, design, and test, and launch of a high power reusable rocket. The design goals were to reach a target altitude of 3000’, deploy a payload module containing an egg that can be safely recovered, and record flight video. The rocket was 62.13 in long fully assembled, had a dry mass of 2.764 kg (3.077 kg wet), and was propelled using an I-class solid fuel rocket motor (Cesaroni I-216-CL). The nose cone and tail cone were fabricated by the team from carbon fiber reinforced polymer (CFRP) via wet layup and vacuum bagging. The fins were constructed from a carbon fiber-balsawood sandwich structure and designed to optimize aerodynamic performance (minimize drag and maximize lift). The motor mount consisted of an innovative “tubeless” design utilizing three centering rings and a 3D-printed ABS engine block. In order to ensure reusability, this design includes a dual deployment recovery system that uses a barometric altimeter to trigger flight events. A 15” drogue chute was set to deploy at apogee, which would control the initial descent while minimizing drift, and a 60” parachute deployed at 800’ was used to slow the rocket to a safe ground-hit velocity. At 900’, a self-contained egg module was deployed with its own parachute. The rocket achieved an apogee of 3556’, however a failure in the recovery system resulted in catastrophic fuselage damage on main parachute deployment. Design objectives, analyses, specifications, testing, and results are discussed in detail
Diffusive hidden Markov model characterization of DNA looping dynamics in tethered particle experiments
In many biochemical processes, proteins bound to DNA at distant sites are
brought into close proximity by loops in the underlying DNA. For example, the
function of some gene-regulatory proteins depends on such DNA looping
interactions. We present a new technique for characterizing the kinetics of
loop formation in vitro, as observed using the tethered particle method, and
apply it to experimental data on looping induced by lambda repressor. Our
method uses a modified (diffusive) hidden Markov analysis that directly
incorporates the Brownian motion of the observed tethered bead. We compare
looping lifetimes found with our method (which we find are consistent over a
range of sampling frequencies) to those obtained via the traditional
threshold-crossing analysis (which can vary depending on how the raw data are
filtered in the time domain). Our method does not involve any time filtering
and can detect sudden changes in looping behavior. For example, we show how our
method can identify transitions between long-lived, kinetically distinct states
that would otherwise be difficult to discern
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